Soil Testing Methods
Three approaches
Observations in the field
On-site measurements
Laboratory measurements
Observations in the Field
Field observations of properties which can be observed after digging
a soil pit
Semi-quantitative assessments of properties rather than direct
measurements.
On site Measurements
On-site measurements using equipment inserted into soil, without
significant disturbance of the soil.
This approach applies particularly to soil water studies.
Laboratory Analysis
Measurements made in the laboratory on soil samples taken from
the field.
Sub-sampling down to an analytical sample also occurs
Field Analysis of Soils
How can we Analyse Soil in the Field?
Field investigation
soil pits
expose the soil profile and horizons
allow field testing of parameters that would be destroyed by
cores
in-situ testing devices
semi-quantitative assessments
field data minimizes sampling error
does not guarantee reliable or even consistent data
soils have very poor homogeneity
Soil Pit
from [Link]
Choosing Sites for Soil Pits
Avoid
areas close to gateways, paths and tracks
headlands of arable fields (the outer 10 m)
sites where straw or fertilizers have been stored
sites used for localized burning of crop residues or hedge trimmings
old field boundaries where a hedge or bank has been removed and
the land levelled
Choosing Sites for Soil Pits
soil varies spatially (from one place to another)
some properties vary in time
eg nutrient levels, moisture
others are more permanent
horizon depth, texture, stone content and ion exchange capacity
How do we Sample Soil?
Is it just digging holes?
Sampling questions
How many samples do I take?
Do we composite lots of sub samples?
How deep do we take the samples?
Do we replicate the sampling?
What quality control do we need?
What tools do I need?
How do we transport, store and prepare the samples?
Information we need to know
Why are we analysing the soil?
Surveys, chemical analysis etc.
How large is the area of interest?
Large areas require lots of sampling
Do we know the soil profile at all?
If we dont, how deep do we sample?
What are we analysing the soil for?
Physical, chemical or biological parameters
Amount of sample
depends upon;
Time constraints
Topography
Cost factors
Reasons for sampling
There are no specific guidelines
Soil Sampling
undisturbed stratification:
remove a core with all horizon information retained, eg with
auger
disturbed stratification
no attempt to keep the vertical connection between horizons, eg
with a shovel
Soil Sampling
How many samples do we take?
At least 20 single samples per 10 000m2 must be taken with an
earth boring tool (or spade) and combined to a mixed sample.
To what depth do we sample?
The usual sampling depth is up to 20 cm in arable land or 10cm
in pasture. Undisturbed soil samples are obtained with a cutting
cylinder with minimum capacity of 100cm3 .
How do we sample?
random
diagonal line
cross line
test lot
Sampling using Augers
pressed and rotated into the soil to take samples from depth
increments of between 15 and 20cm.
samples are 'disturbed' to varying degrees
observations that can be made on the samples will be restricted
colour, texture, stones, roots and horizon depth can be recorded
soil structure cannot
special coring equipment is required to obtain 'undisturbed' samples
Sampling for lab testing
normal sampling depth for horticultural and tree crops is 0-15 cm
deep sampling down to 60-100 cm may be necessary to better assess
soil salinity, acidity, S, and mineral N status
sampling depth must be recorded
protocols relevant to important crop and soil tests should be
followed
usually involves making a composite from around 15 to 30 subsamples from the area in question
Transportation, preparation
and storage of samples
Now that you have your soil samples, what do you do with
them?
Laboratory Preparation of Samples
should be kept cool or cold between during transport
may be air-dried remote from the laboratory (max. 40C) when
moisture content is not required
breaking up any large cores on a clean surface
remove rocks by hand or sieving
retain a representative portion in a sealed polyethylene bag or
'moisture container' for moisture determination
sample size reduction: coning and quartering or riffler
Laboratory Preparation of Samples
Next spread the soil samples on drying trays (if applicable) and airdry at up to 40C.
When the soil is thoroughly air-dry, mix, roll, and/or grind.
Retain the <2mm fraction, preferably in an air-tight plastic or inert
container, for subsequent laboratory analyses.
Laboratory Preparation of Samples
When required, determine the weight percentage (oven-dry basis) of
the residual >2-20 mm size fraction.
When fine grinding is specified, take a representative sub-sample
(usually around 30g) from the <2 mm portion.
Pass the entire sub-sample through the required mill and store in a
small air-tight container.
Coning & quartering
Riffling