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38 views12 pages

Sem 5

Uploaded by

Yash Tambe
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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114 115

2. Algorithm quadratic equation (for root of). SYLLABUS PRESCRIBED


3. Program for solving ordinary differential equation with initial value FOR BACHELOR OF TECHNOLOGY
of Euler’s method. (CHEMICAL TECHNOLOGY)
4. To find value of unknown of simultaneous by Gauss elimination FOOD TECHNOLOGY, PULP & PAPER TECHNOLOGY,
method. OIL & PAINT TECHNOLOGY AND
5. To find roots of equation using Bisection method.
PETROCHEMICAL TECHNOLOGY
6. Algorithm for Regula-Falsi method.
SEMESTER PATTERN
7. Find the roots of equation by Newton-Raphsons method.
8. Program for modified Newton-Raphson method. FIFTH SEMESTER
9. Design algorithm for regression. 5CT 01 HEAT TRANSFER
10. Algorithm for print the grades of students using if-else-if statement. SECTION-A
11. Design algorithm and flow chart for Runga-Kutta method. Unit I : Importance of heat transfer in chemical process industries.
12. Design algorithm and flow chart to find greatest and smallest Modes of heat transfer, steady state conduction in one
element. dimension.
Note: The students should perform minimum 8 experiments from the Fourier’s law.
list to complete the term. All experiments in this list shall be Heat transfer through plane, cyclindrical and spherical walls,
available in the laboratory. Additional experiments relevant to the compound resistance in series, thermal insulation, critical
syllabus may be added to the main list. and economic thickness. Extended surface equipments,
6PP09 MINOR PROJECT types, their design & operation, introduction to unsteady
The students in a group of not more than four members have to work on a state heat transfer.
topic which is experimental and analytical in the area of POLYMER Unit II : Heat transfer by convection, film concept, individual and
TECHNOLOGY. Each project shall have a guide. On completion of the overall coefficients and factors affecting them. Natural and
work, a project report should be prepared and submitted to the forced convection dimensional analysis applied to heat
Department. The project work and the report will be evaluated by an transfer. Dittus-Boelter equation. Limitations and
internal assessment application.
committee for 25 marks. The university examination for 25 marks will Unit III : Heat transfer by parallel and counter current flow, concept of
be a Viva-Voce examination conducted by a committee of one external log mean tempeature difference, rate of heat transfer. Heat
examiner and one internal examiner /Guide appointed by the University. transfer by film wise and dropwise condensation in horizontal
& vertical tube.
****** SECTION-B
Unit IV : Heat exchange equipments and their design, double pipe,
parallel, counter current, shell and tube heat exchangers,
condensers, fouling factors, concepts of transfer units in
heat exchangers, NTU concept for heat exchangers.
Unit V : Boiling & Evaporators : Classification of types and field
applications of evaporators single and multiple effect
evaporators.
Heat transfer through submerged coils, jacketted vessels.
Unit VI : Heat transfer by radiation, concept of black body, Kirchoff’s
law, Stefan’s law, Black and gray body radiation, view factors
luminous and non-luminous gases. Heat transfer in packed
and fluidised beds.
Recent developments in heat transfer.
116 117
PRACTICALS : Based on above syllabus. Unit V : 1. Centrifuges: Theory, Equipments, types and
calculations.
BOOKS RECOMMENDED :
2. Cyclones: Hydrocyclones, liquid scrubbers and electronic
1) Heat Trasnfer : Mc Adams precipitators.
2) Heat Transfer : Sukhatme Unit VI : 1. Adsorption, theory, type and application, Langmuir’s
3) Basic Heat Transfer : Necati Orisik, McGraw Hill Freundlich’s equation, nature of adsorbents, industrial
Co., Kogakusha. adsorbents.
4) Heat Transfer : J.P.Hokman, McGraw Hill Co., 2. Adsorption on fixed bed, fluidised beds. Adsorption
Kogakusha. equilibria calculations for vapour, gas & liquid adsorption.
5) Unit Operations of : McCab and Smith. Adsorption, operation such as single stage, multi stage, cross
Chemical Engg. current & multistage counter current operation &
6) Introduction to : Bedger and Banchero. equipments.
Chemical Engg. 3. Recent developments in mechanical operation
7) Chemical Engg. : Coulson & Richardson, Vol. I equipments.
(ELBS, Pergamon Press, Latest
Edition) PRACTICALS: based on above syllaubs.
8) Heat Transfer : Gebhart, McGraw Hill,
2nd edition, Latest Edition BOOKS RECOMMENDED:
9) Fundamentals of Engg. : R.C.Sachdeva, Wiley Eastern. 1. Momentum Transfer Operation:S.K.Gupta, TMC, Latest edition.
10) Heat Transfer : R.C.Sachdeva. 2 Unit Operations of Chemical Engineering: McCabe and Smith, TMC
11) Heat & Mass Transfer : S.D.Dawande,Central Techno Pub., 3. Chemical Engineering Vol. I : Coulson & Richardson, Pergamon,
Nagpur Latest edition.
4. Principles of Unit Operations: A.S.Foust, et-al.
5. Unit Operations: C.G.Brown.
5CT 02 MECHANICAL OPERATIONS
6. Introduction to Chemical Engg. : Beder & Bachero.
SECTION - A
7. Mass Transfer Operations: R.E. Treybal
Unit I : Relevance of mechanical operations in industry.
8. Mechanical Operations Vol-I : R.S.Hiremath & A.P.Kulkami.
I. Size reduction, stages of reduction, Equipments operating
variables, laws of energies, energy requirements. 5CT03 CHEMICAL ENGINEERING
2 Screening: Screen analysis, particle size distribution. THERMODYNAMICS

Unit II : 1. Classification: Equal faIling particals, equipments, jigging, SECTION-A


tabling. Unit I : Scope of thermodynamics and its importances to chemical
2 Gravity settling, drag force, terminal settling velocity. Engineers, Basic concepts, extensive & intensive properties.
3. Sedimentation : Continous thickners. state function & chemical systems. Definition, symbols &
interrelation, concepts of Entropy, Enthalpy & internal
Unit III : 1. Storage and handling of solids, transporation energy. First law of thermodynamics, Equations of state,
2 Mixing, Mixers, agitation, types of equipments. critical properties, Vander Wall’s constants, Virial
expansions, Redlich-Kwong equation, Beattie-Bridgeman
SECTION - B equation.
UnitIV : 1. Filtration : Theory, operation, types, Flotation agents, Unit II : First law applied to thermodynamic processes & calculation
flotation cells. of Workdone, free energy & heat changes. Maxwell relation
2. Filter Calculations, filtration equation for compressible equation, second law and third law of thermodynamics.
and non-compressible cakes, specific cake resistance. Thermodynamics relations based on second law. Relation
3. Filtration - Constant pressure and constant rate and their between Cp & Cv, compressibility factor & coefficient of
equipments. thermal expansion, concept of residual entropy & entropy
of equilibrium.
118 119
Unit III : Partial molar and apparent molar properties, Gibbs Duhem 6) Chemical Thermodynamic : M.R.Awode, Dattson,
equation, Chemical potential, effect of temperature and Nagpur.
pressure fugacity, excess thermodynamic properties and *****
thermodynamic properties of mixing. Gibbs-Duhem-
Morgules equation, Konovalov laws. Colligative properties.
SPECIAL TECHNOLOGY-II
Ebulliometric constant. Determination of Molecular Weight
of unknown chemical substances. Solubility law. (RELATED TO CONCERNING TECHNOLOGY)
SECTION-B 5FT04 (i) FOOD TECHNOLOGY-II
Unit IV : Vapour liquid equilibrium, T-X-Y diagrams & X-Y diagram for BIO-CHEMlSfRY AND NUTRITION
ideal & non ideal system. Raoult’s law and Henry’s law. Organisation cell and cellular constituents. Introduction and
Deviations from Raoult’s law. Comparision of ideal & non- classification of enzymes, specificity, enzymes Kinetics,
ideal systems. Phase equilibria in non reaching multi- activnetrs and inhabitors. Assay techniques, Isolation of enzymes trom
comonents, Binary, ternary systems. Graphical sources and their application.
representation of L/L, L/S & G/S systems. Right angled Bio-energetics, Digestion and metabolism of carbohydrates,
triangular diagrams. Equilateral triangular diagrams, Janecke proteins and fats. Photosynthesis, Nucleic acids and their functions.
diagram, Effect of temp. & pressure on ternary equilibrium,
Vitamins: Classification, sources, Chemistry, functions and
Phenol-Wafer systems. auiline-water-chlorobenzene
deficiency symptoms. Assay of vitamins.
systems.
Minerals: Macro and micro-minerals, sources, functions and
Unit V : Statistical thermodynamics, thermodynamics probability, its
efficiency symptoms.
relation with Entropy, partition function and its relation with
Nutrition: Functions of foods Energy, value of foods. BMR and its
termodynamics functions, the Boltzman distribution law,
measurement, Energy requirement of individuals. Recommended dietary
Distribution law for chemically reactive system.
allowances of proteins, fats, carbohydrates, vitamins and minerals.
Thermodynamics charts & their uses. Searching of
Nutritional evaluation of proteins. Factors influencing nutritive value of
thermodynamics data.
foods. Loss of nutrients during processing. Enrichment and fortification
Unit VI : Chemical Equilibrium, feasibility of chemical reaction, free
of foods. Formulation of diets and foods for specific needs.
energy change, Reaction co-ordinate, equilibrium constant,
Antinutritional Factors of Foods :
Effect of temp. & pressure, Relation between Kp, Kc & Kv,
Le-Chatelier’s principle, Endo-Exothermic relations, Toxic compounds, enzyme inhabitors, alkaloids etc.
Heterrogeneous equilibria, various methods of calculating Techniques of biochemical analysis like spectrophotometry
free energy charge. Equilibrium conversions, case study of Chromatography, electro-phoresis Light and electro microscopy.
feasibility report for manufacture of industrial chemicals. Histochemical techniques, isotopic methods.
Practicals :- based on above syllabus. Recent Advances in the field.

Books Recommended : Books Recommended :


1) An Introduction to Chemical : R.P.Rastogi, R.R.Misra. 1. Outlines of Biochemistry by E.E.Conn & P.K.Stump, Wiley Eastern
Pvt.Ltd., New DeIhi.
Thermodynamics
2 Biochemistry of Foods by Eskin, N., A.M.Handerson, H.M. & Town
2) Chemical Engineering Process : Houghen-Watson. End RJ., Academic Press, New York.
3) Introduction to Chemical Engg. : J.M.Smith, H.C.Vauhess 3. Cell Physiology by A.C.Giese, Sanders & Company, Toppan, Japan.
Thermodynamics 4. Integrated Biology by L.Hill, D.Bellamy, I Chester, Jones Chapman
4) Thermodynamics for : H.C.Weber, & Hall Ltd., London, EC4.
Chemical Engg. J.P.Meissner 5. Principles of Enzymology for the Food Science by Whitaker J.R.,
5) Engineering Thermodynamics : P.K.Nag. Marcel Dekker, INC, New York.
120 121
6. Applied Nutrition by R.Rajalaxmi, Oxford & IBH Publishing Co., New 4. Hawk’s Physiological Chemistry Edited by Bernard L.Oser, Tata
York. McGraw Hill Pub. Co. Ltd., New Delhi.
7. Heinz Handbook of Nutrition by Benzamin T. Burton, McGraw Hill
. Book Company, New York. SPECIAL TECHNOLOGY-ll
8. Nutrition - An Integrated Approach by R.C.Pyke & M.L. Brown, 5PT04 (ii) PULP & PAPER TECHNOLOGY TECHNOLOGY
Wiley Eastern Pvt.Ltd., New Delhi. OF PULPING PROCESSFS
9. Hawk’s Physiological Chemistry, Edited by Bernard L.Oser, Tata Collection grading and storage of various raw material, wood
McGraw Hill Publishing Co. Ltd., New Delhi. preparation for pulping, units for measuring wood handling wood barking
10. Biochemistry: White A. Handler P., Smit E.L., McGraw Hill, Tokyo. chipping. screening. chip. handling and storage. relationship between wood
11. Text Book of Biochemistry : H.R.Mahler and E.H.Chordes, Harper and quality.
& Row Publisher, New York. Introduction to pulping. Fiber separation commercial processes.
SPECIAL TECHNOLOGY-ll (PRACTICAL)- LAB types of pulping processes. advances and trends in pulping.
5FT10 FOOD TECHNOLOGY Manufacture of mechanical pulp: Types. grades and uses of
A.BIOCHEMISTRY mechanical pulp stone ground wood process, types of grinders. theory of
1. Estimation of carbohydrates and proteins by various methods. grinders. theory of grinding. variable in ground wood process,
2. Estimation of minerals, Phosphorus, Iron, Calcium. characteristics of groundwood pulp, pulp mill operations control, practice
3. Estimation of vitamin C and effect of heat. and testing methods, whole wood fiber manufacture. ground wood from
4. Qualitative demostration of enzyme with salivary amylase. pretreated wood, refiner mechanical pulping scheme, thermomechanical
pulping.
5. Study of rate of enzyme reaction, effect of environmental factors
on rate of enzyme action. Semichemical pulping and Semimechanical pulping; Neutral sulfite
semichemical pulping, bisulfite semichemical pulping, craft semichemical
6. Detection of trypsin inhibitor.
pulping. cold soda semichemical pulping, hot sulfite chemomechanical
7. Chromatographic separation of carbohydrates and aminoacids.
semichemical pulp.
8. Simple histological studies on plant tissue.
Sulfite pulpinp. Description of various sulfite processes, sulfite
B. MICROBIOLOGY liquor preparation. variables in sulfite pulping. mechanics and kinetics of
1. Preparation and sterilisation of nutrient media. sulfite pulping. delignification, digestion in sulfite process. characteristics
2 Cultivation and morphological study of common species of bacteria of sulfite pulp.
yeasts and moulds. Alkaline pulping: General description of alkaline pulping process.
3. Isolation of pure culture from natural sources. alkaline digestion. chemical reactions during alkaline digestion. Variables
in alkaline pulping process, digester operation. material and heat balance
4. Imunelation of bacteria Haemoeytometer, standard plate count
bamboo. reeds. hemp. jute, etc.
MBRT tests for milk.
Recent advances in the field.
5. Bacteriological analysis of water.
6. Microbial spoilage of various foods and effect of extrinsic and BOOKS RECOMMENDED :
intrinsic factors on food spilage. 1. Pulping processes by A.Rydholm. Interscience Pub., John Wiley
&
BOOKS RECOMMENDED:
Sons Inc., New York. London. Sydney.
1. Microbiological Methods, C.H.Collins & P.M. Lyme. Butterworth
Co.Ltd., London. 2 Pulp & Paper: Chemistry & Chemical Technology, 3rd Edn., Vol I
by James P.Casey, John Wiley & Sons, New York.
2 Microbes in Action - A Laboratory Manual of Microbiology;
H.W.Seeley (JR.) and P.J.Von. Denmark - Taraporewala I.,W. Pvt. 3. Pulp and Paper Manufacture, 2nd Edn., Vol I by Ronald G.McDonald.
Ltd., Bombay. 4. Pulp and Paper Science Technology. Vol. I by C.E.Libby. McGraw
3. Introduction to Practical Biochemistry: D.T.Plummer, Tata Hill Co.
McGraw Hill Co., New Dellii. 5. Hand book of Pulp & Paper Technology. 2nd Edn.. by Bitt Van
Nostrad. Reinhold Co.. New York, London.
122 123
SPECIAL TECHNOLOGY -II (PRACTICAL) - LAB Essential fatty acids.
5PC10 PULP & PAPER TECHNOLOGY Recent advances in the field.
Analysis of fibrous materials; Pulp analysis: Determination of
Books Recommended :
moisture ash content, permaganate number, copper number, kappa number
of pulps 2, B, V, cellulose, solubility of pulp in alkali. 1. Industrial Oil and Fat Products: A.E.BaiIey : Interscience
Publishers, New York, Latest Edition.
Analysis of non-fibrous materials: Analysis of black, green and 2 Fatty Acids: K.S. Markley (5 Volumes),lnterscience Publishers,
white liquors, bleaching powder, soda ash, caustic soda, lime stone etc. New York, Edn., Latest Edition.
Books Recommended : 3. Structure and Utilization of Oil Seeds : J.G.Vaughon.
I. Technology of Textile Properties by M.A.Taylor, 4. Melting and Solidification of Fats : A.E.Bailey, Interscience
2. Textile Analysis by S.K. Publishers, New York, Latest Edition..
3. Identification of Textile Materials, 7th Edn., Textile Inc., 5. The Analysis of Fats and Oils: V.C.Mehlenbacher : The Garrard
Manchester,7. Press Champing, Edn., Latest Edition..
4. Analytical methods for a Textile Lab., 2nd Edn., AATCC monog 6. Progress on the Chemistry of Fats and other Lipids: T.T.Homan,
No.3 Research Triangle Park. North Carolina, Printed in U.sA W.O. Lundberg and T.Malkia, Pergamon Press, New York, Latest
5. ISI Standards for Textile Testing Edition (7 Vols.)
6. Textile Testing by Sinkale. 7. The Chemical Constitution Natural Fats: Wiley Books Publishers,
New York, Latest Edition..
5OT04 SPECIAL TECHNOLOGY-ll 8. Vegetable Fats and Oils: G.S.Jamiesan, Renehold Publishers, New
CHEMIS1RY AND BIOCHEMISTRY OF FATS York, Latest Edition..
(iii) (OIL & PAINT TECHNOLOGY) 9. Vegetable Fats and Oils: E. W.Eckey : Renehold Publishers, New
York, Latest Edition..
Techniques of separation of fats and fatty acids : Low temperature 10. Gas-Liquid Chromatography - Theory and Practice: S.Dal Nagore
crystallization, esterification, urea adducts, counter distribution, and R.SJuvent; Interscience Publishers, New York, Latest Edition.
chromatographic methods of separation with special reference to thin- 11. Lipid Chromatographic Analysis: C.V.Marinelt.
layer chromatography and gas-liquid chromatography.
12. Fatty Acid Synthesis and Application: N.E.Bednareyk &
Methods for quantitative investigation on the component, fatty acids W.L.Erickson.
of natural fats and processed fats.
13. The Lipids: H.D.Dauel : Interscience Publishers, New York, Latest
Lipase hydrolysis, X-ray diffraction and polymorphism of Edition.
glycerides and other fatty acids and their derivatives. Dilatimetric
14. Analysis and Characterization of Oil, Fats Products :
measurements and their significance.
H.A.Bookenoogen.
Infrared (IR), Ultraviolet (UV), Unclear Magnetic Resonance
15. Thin-layer Chromatography: Babbit.
(NMR) and mass spectroscopy for the analysis of fatty materials.
Reichert-Missel and Polanske and Krischner values. Advanced SPECIAL TECHNOLOGY - II (PRACTICAL) - LAB
method of analysis of fats, fatty acids and glycerides. . 5OT10 OIL & PAINT TECHNOLOGY
Chemical reactions pertaining to the manufacture of fatty acid Analysis of nickel catalyst and acids oils, Preparation of mixed
derivatives including metal salts other than alkali metals. fatty acids and determination of composition.Analysis of commercial fatty
Quantitative investigation of component triglycerides of natural acids. Preparation of pure fatty acids. Determination of mono, di and tri-
fats. Theories of fatty acid distribution in natural fats. Effect of fatty acid glycerides. Analysis of soaps and detergents. Detection of Adulteration.
distribution on the physical properties. Polymorphism of fats and fatty Analysis of Oils by thin layer and column chromatography.
acids. Biosynthesis of fatty acids, phosphlipids and triglycerides in plants
and animals. Elongation and desaturation of acyl chains. Biological
utilization of fats. Fat assimilation;
124 125
SPECIALTECHNOLOGY-II SPECIALTECHNOLOGY-II (PRACTICAL)- LAB
5PC04 (iv) PETRO CHEMICALTECHNOLOGY-II 5PC10 PETRO-CHEMICAL TECHNOLOGY-II
PETROLEUM REFINING TECHNOLOGY Analysis and testing of petroleum and petroleum products.
Petroleum refining industry in India, practice and prospectus : Commercial petroleum ASTM distillation of motor gasoline, kerosene and high speed diesel,
products, quality requirements.Indian specifications. viscosity index. demulsification number and forming characteristics of
lubricating oils; Existent gum in motor gasoline; oxidation tests for lubricating
Testing methods and their significance: crude assay, refining processes, integration oils, oxidation stability of gasoline, water washout characteristics and roll
of these processes:. typical refining schemes in India. Descriptive account of stability of grease. Ductility of bitumen; Electric strength-transfoer oil, PONA
atmosphere , vaccum distillations, use of process steam, steam stripping vaccum analysis by FIA method, aniline point method liquid vapour pressure, Heat
producing systems.etc. of combustion of liquid hydrocarbon fuels, calorific value of’ gases,
Industrial practice of various conversion processes, such as catalytic cracking, mercaptan sulphur content, salt content, Sulphur by lamp and bomb
hydro-cracking,cooking visbreaking, polymerization, alkylation, hydro- methods, P,Ca and Cl lubricating oils, study of Vapour-Liquid equilibrium
desulphurisation etc. and their role and place in Indian refineries. for binary systems using Othmer still study of ternary equilibrium systems
and representation triangular diagrams.
Production of cube base stocks, solvent extraction, dewazing, finishing and blending;
Finishing processes in a modem refinery. *****
Petroleum speciality products.
Descriptive account of various aspects of a refinery such as instrumentation and 5 FE CT 05 FREE ELECTIVE - I
automatic control, refinery utilities off site facilities refinery layout, corrosion, (2) ECONOMICS AND MANAGEMENT
safety, energy saving, environmental aspects etc; conservation of petroleum SECTION-A
products, Techno-economic aspects of optimum refining schemes. Unit I : Nature and Scope of Economics, introduction to managerial
Recent Advances in the field. economics.
Demand concepts : Demand specification, types of demand.
Books Recommended :
Demand analysis : law of diminishing utility, Consumer’s
1. Petroleum Refinery Engg., W.L. Nelson : Mc Graw Hill Kogakusha, surplus.
4th Edn., Latest Ed.
Demand forecasting : Concept of forecasting, types of
2. Modem Petroleum Technology, Applied Science. G.D.Hobson and forecasts (8)
W.Pol Publisher 4th Edn., Latest Ed.
Unit II : Production Concept, production function, Laws of return,
3. Petroleum Processing, Principles and Applications, RJ scales of production, factors of production, production
.Hengatabes, planning and control : Its meaning, essential factors for the
McGraw Hill, Latest Ed. success of production planning and control. (8)
4. Petroleum Refiing, Technology and Economics: J.H.Gary and G.E., Unit III : Meaning of Management, Principles of management, meaning
Hand-work, Merceidekker, New York, Latest Ed. and principles of scientific management, levels of
5. Petroleum Processing Handbook : W.E.Bland and P.L.Daviason. management, delegation and authority, Organisation, forms
McGraw Hill, Latest Ed. of organisation. (8)
6. Petroleum Refinery Manual : M.M.Noel, Rinebold, New York, 1959.
SECTION-B
7. V.B.Guthrie, Petroleum Products Handbook, McGraw Hill, 1960.
Unit IV : Sources of Finance Banking and Credit structure in India :
Financial institutions, promotional polices and programmes
of industrialisation, functions of Commercial Banks,
functions of Central Bank. (8)
126 127
Unit V : Economic and Social Environment : Brief idea about economic adverbs, prefix and suffix, correct forms of commonly mis-
environment of business, socio-cultural environment, Health spelled words, understanding of the given passage.
hazards of chemical industries, awareness about AIDS & Comprehension - B - Structure study :-
other diseases.
Simple and compound sentences, types of conjunctions, sin-
Brief idea about economic recession & its effect. gular and plural, tenses and their effect on verb forms. Use
Introduction to World Trade, of - not only - but also, if clause, since, may, can, could,
Globalisation, Libertion and their effects. would, too etc.
Introduction to Patenting & intelleatual property protection Active and passive forms, negative and interrogative, punc-
(8) tuation and capitalization. (10 Hours)
Unit VI : Entrepreneur and Entrepreneurship :
Unit II : Theoretical background - importance of communication, its
Entrepreneurial competencies, institutional interface for process, model of communication its components & barri-
small scale enterprises, opportunity scanning and ers.
identification.
Verbal communication, its significance, types of written com-
Market assessment for SSE, choice of technology and
munication, organization of a text (Titles, summaries, head-
selection of site, Ownership structure and organisational
ings, sequencing, signaling, cueing etc.), Important text fac-
framework, preparation of business plan, main features of
tors (length of paragraph, sentences, words, clarification and
Indian factories act & minimum wage act.
text difficulty). Evaluation of written communication for its
Brief idea of Taxation in India. (8)
effectivity and subject content.
BOOKS RECOMMENDED : Non-verbal communication, types of graphics and pictoral
1) Managerial Economics : K.K.Seo, Richard D. Irwin Inc. devices. (10 Hours)
2) Engineering Economics : J.L.Riggs, McGraw Hill, New York, Unit III : Specific formats for written communication like - business
Latest Edition. correspondence, formal reports, technical proposals, re-
3) Managerial Economics : Adhikary M., Khosla Pub. House, New search papers and articles, advertising and graphics. Format
Delhi. for day-to-day written communication like applications,
4) Small Business Management Fundamentals : Dan Strenhoff and notices, minutes, quotations, orders, enquiries etc.
J.F.Burgess, McGraw Hill Book Company. Oral communications - Important objectives of interper-
5) Effective Small Business Management : Richard M.Hodgills, sonal skills, (verbal and non-verbal), face to face commu-
Academic Press Incorporated, Harcourt, Brace Jovanovich. nications, group discussion and personal interviews.
6) Marketing Management for Small Units : Jain Vijay K., Methodology of conduction of meetings, seminars, sympo-
Management Publishing Co., Latest Edition. sia, conference and workshop. (10 Hours)
7) Marketing Management :- Analysis, Planning, Implementation and
Control : Kotler, Phillip, Prentice Hall of India Pvt. Ltd., Latest BOOKS RECOMMENDED :
Edition. 1) Krishna Mohan, Meera Banerjee : Developing Communication
8) Modern Economics Theory : K.K.Dewett. Skills, MacMillan India Limited.
2) Chrissie Wright (Editor) : Handbook of Practical Communication Skills,
***** Jaico Publishing House.
3) Curriculum Development Centre, TTTI WR, Bhopal : A Course in
5 CT 06 COMMUNICATION SKILLS Technical English, Somaiya Publication Pvt. Ltd.
Unit I : Comprehension over an unseen passage.
4) F.Frank Candlin : General English for Technical Students, University
Comprehension - A - word study :- of London Press Ltd.
Synonym, antonym, meanings, matching words, adjectives,
128 129
5 CT 11 COMMUNICATION SKILLS LABORATORY 4. Halogenation: Thermodynamics and Kinetics of halogen.
Objective : Pathohalogenation. Equipment and design for halogenation.
On completion of this laboratory the candidate should be Technical preparation or halogen compounds e.g. allyl chloride.
able to demonstrate adequate skills in oral and written D.D.T...B.H.C....Chlorobenzene dichlorodifluromethane. vinyl
communication for technical English language, actively chloride etc.
participate in group discussions and interviews and exhibit 5. Oxidation : Liquid and Vapour phase oxidation. kinetics and
the evidence of vocabulary building. Candidates should be thermochemistry. apparatus for oxidation. Technical oxidation of
assessed through continuous monitoring and evaluation. isoeurenol. acetaldchyde. Cyclohexane Iso-propylbenzene.
The sample list of experiments is given below. This list can napthaleum refinary, electro-plating, tanning, coat mining and radio
be used as guideline for problem statements but the scope waste.
of the laboratory should not be limited to the same. Aim of 6. Wastewater Treatment : Classification of wastewater. Methods of
the list is to inform about minimum expected outcomes. treatment. sludge treatment and disposal. treatmcnt of effluent
1. Assignments and tests for vocabulary building water from textiles rayon. pulp. dairy, distillery Petroleum refinary,
2. Technical report writing electro-plating, tanning, coal mining and radio active waste.
3. Group discussions 7. Water : Source of water. Impurities in water. Requirements of water
4. Interview techniques by different industrics. treatment of water for industrial and
5. Projects and tasks such as class news letter domestic purpose. boiler feed water treatment. reuse of water.
6. Writing daily diaries and letters Water conservation.
7. Interactive language laboratory experiments. 8. Industrial gases : CO, CO2, CO3, H2,O2, N2, SO2, C2, H2 synthesis gas,
TEXT BOOK : Norman Lewis : Word Power Made Easy rare gases : Helium nitrous oxides.
http://www.teachingenglish.org.uk 9. Industrial Acids : Sulphuric, Nitric and hydrochloric acid.
10. Marine Chemicals : Salt from sea water. by product of salt industry
****** viz, Bromine and Iodine.
11. Fertilizers: Ammonia Nitrogenious of fertilizers. Phosphatic
SIXTH SEMESTER fertilizers. Potassic fertilizers. Compound and complex fertilizers.
FREE ELECTIVE - II Misccllanceous fertilizers,
6 FECT 05 (3) CHEMICAL TECHNOLOGY 12. Electrolytic and Electro-chemical Industries: Chlorates,
perchlorates. Primary and Secondary cells, artificial abrasives.
Study of the following proccsscs : Calcium carbide Refractory carbides. borides, silicides and
nitrides.
1. Nitration: Nitrating agensts. Kinetics and mechanism of aromatic
nitration. Thennodynamics of nitrations. Equipments for nitration. BOOKS RECOMMENDED:
Mixed acids for nitration and typical industrial nitration processes
1. Unit Processes in Organic Synthesis by P.H.Groggins. Vth Edn..
e.g. preparation of nitrabenzene, chloronitronapthalene and
International Students Edn.. McGraw Hill Co.
acetafiline.
2. Sulphonation and Sulfation : Sulphonation and sulfating 2. Chemical Technology -Vols I, II, III by D.Venkateswarlu, Chemical
agents:Kinetics, mechanism and thermodynamics. Industrial Engg. Education Development Centre. I.I.T. Madras, Latest Edition.
equipment and techniques. Technical preparation of sulphonates 3. Chemical Process Industries by R. N. Sherve and J. A. Brink. McGraw
and sulphates. Sulphation of lauryl alcohol, dimethyl ether etc. Hill, Co., Latest Edition.
3. Hydrogenation: Catalytic Hydrogenation. Kinetics and thermody- 4. Chemical Technology in two parts. Edited by I.P.Mukhlyanov, Mir
namics of hydrogenation reactions. Apparatus and material of
Publishers Moscow, Latest Edition.
construction, hydrogenation of fatty oils. Synthesis of methanol.
Hydroforming of naptha. Hydrogenation of heavy oils.
130 131
6 CT 01 PROCESS EQUIPMENT -DESIGN & DRAWING Unit II : Measurement of pressure, vacuum, humidity & pH in pro-
cess industry.
SECTION-A
Unit III : Methods for composition analysis. Principle and techniques
of instruments for composition analysis in process indus-
Unit I : Material behaviour under stresses, theories of failures.
try, such as chromatography, spectroscopy, refractrometry
(8)
etc.
Unit II : Fabrication methods and their effects : Design method for
atmospheric storage vessels, unfired pressure vessel SECTION-B
subjected to internal and external pressure. (8) Unit IV : Flow measuring instruments : Flow measuring devices for
Unit III : Vessels for high pressure operations, Agitated vessels. Tail incompressible and compressible fluids. Electro-hydrau-
columns, internals of the reactors. (8) lic valves, hydraulic servomotors, electro-pneumatic valves.
Pneumatic actuators.
SECTION-B Unit V : Introduction to Simple system analysis : Laplace Transfor-
Unit IV : Design of proess equipment accessories and support mation. Block diagrams, linearization. First and higher or-
systems. (8) der system.
Unit V : Complete design and preparation of working drawing Unit VI : Frequency response, distributed parameter system, dead
for typical process equipment, such as large storage vessels, time.
thick wall pressure vessels. Self supported tall columns, Feed back control, servo and regulator control. Time domain
agitated pressure vessels with heat transfer requirements closed loop responses, closed loop frequency response.
etc. (8)
Unit VI : Design and layout of piping system and preparation of piping BOOKS RECOMMENDED :
diagram for a typical process. Material selection and piping 1) Industrial Instrumentation : Eckman, Wiley Eastern
coding. (8) 2) Instrumental Methods of Chemical Analysis : Erwing, McGraw Hill.
3) Instrumentation & Process Measurements : W.Bottom, Orient
PRACTICALS : Based on the above syllabus.
Longman.
BOOKS RECOMMENDED : 4) Industrial Control & Instrumentation : W.Bottom, Orient Longman.
1) Process Equipment Design : I.E.Brownell, E.H.Young, John Wiley,
Latest Edition. 5) Outlines of Chemical Instrumentation & Process Control : A.
2) Process Equipment Design : M.V.Joshi, McMillan, Latest Edition. Suryanarayan, Khanna Pub., New Delhi.
3) Introduction to Chemical Engg. Design, Mechanical Aspects 6) Donald R. Cougha Nowr : Process Systems Analysis and Control,
McGraw Hill Pub., New York.
4) I.S.Code for Unfired Pressure : IS No. 2825 - 1969 pressure vessel.
7) Vyas R.P. : Process Control and Instrumentation, Central Techno
5) Process Equipement Design & Drawing : S.D.Dawande.
Pub., Nagpur.
6) International & Indian Standard codes for Piping. 8) Patranabis D. : Principles of Industrial Instrumentation, 2nd ed., Tata
7) Process Design of Equipments, 3rd Ed, S.D. Dawande, Vol I & II, McGraw Hill Pub. Co., New Delhi.
Central Techno Pub., Nagpur 9) Patranabis D. : Principles of Process Control, Tata McGraw Hill
***** Pub. Co., New Delhi.
10) Gaikwad R.W., Misal S.A. : Process Dynamics & Control, Central
6 CT 0 3 INSTRUMENTATION & CONTROL Techno Pub., Nagpur.
11) Stephanopoulos G. : Chemical Process Control and Introduction to
SECTION-A
Theory & Practice, PHI, Latest Edition.
Unit I : Measuring Instruments : Qualities of measurement, elements 12) Considine D.N. : Process Instrumentation & Control Handbook,
of instrument, static & dynamic characteristics, measurements McGraw Hill.
of temperature and levels.
*****
132 133
SPECIALTECHNOLOGY PAPER-Ill
6 FT04 SPECIAL TECHNOLOGY-III
6 PT 04 (ii) PULP & PAPER TECHNOWGY
(i) FOOD TECHNOLOGY-III
PULPING PROCESSES-II
MICROBIOLOGY AND PRINCIPLES
OF FOOD PRESERVATION Pulp Washing, Bleaching and Recovery of Spent Chemicals :
Brief historical background, classification and terminology of Washing of Pulp : Delibration of sulphate pulp, brown stock washing,
micro-organisms. Study of morphology and physiology of bacteri-yeasts screening and clearing of sulphate pulp, washing of sulphite pulp, screening
moulds and actinomicetes, introduction to viruses and bacteria. Methods and clearing of sulphite pulp, screening and clearing of other pulps.
of isolation, cultivation and enumeration of micro-organisms, Nutrition, Recovery of spent chemical : Liquor recovery in alkaline pulping,
reproduction and metabolism. Synchronised and balanced growth and evaporation of kraft liquors, recovery furnance, recausticizing treatment
continuous cultivation of microorganisms. to digester and evaporator condensates, recovery of alkalining sulphate,
turpentine, tall oil and other alkaline pulping by products.
Control of microorganisms by physical and chemical methods, Recovery process in sulfite pulping, Calcium, Magnesium, Amonia
Sterilisation and disinfection, inadiation antibiotics, evaluation of and Sodium bases recovery, other sulfitex recovery methods, recovery of
antimicrobial agents, Microbiology of air, water and sewage. by-products from sulfite process, whole spent liquor and ligoo sulfonates.
Immunological methods. Bacteriological analysis of foods, Role of Vaniline and alcohol from sulfite spent liquor, fermentation of sulfite spent
microorganisms in food spoilage. liquor to produce proteins.
Principles of food preservation. Preservation of food by means of Bleaching: History of Bleaching, bleaching of mechanical pulps,
low temperature. Freozedrying thermal processing irradiation, dehydration semichemical pulps, chemi-mechanical and chemical pulps, multistage
chemicals antibiotics and C.A.storage. Sources and prevention of bleaching, control procedures in bleaching process, colour reversion of
contamination. Food Production and Microbial toxins, Principles of a bleaching pulps, environmental aspects of Bleaching chemicals.
amitation in food technology and safety of foods. Fermented food like Recent advances inthe field.
bread, cheese, yogurt, vinegar, alcohol, pickles.
Books Recommended:
Recent advances in the field. 1. Pulping Processes by S.A.Rydholm.
BOOKS RECOMMENDED: 2. Pulp & Paper : Chemistry and Chemical Technology, 3rd Edn., Vol.
I. Food Microbiology: W.C.Frazier, Tata McGraw Hill Pub., Co., I by James P.Casay
Bombay. 3. Pulp & Paper Manufacture, 2nd Edn., Vol.-I by R.P.Mc Donald.
2. Microbiology: MJ.Pelkzar, Ried R.D., E.C.S.Chan, Tata McGraw 4. Hand Book of Pulp & Paper Technology, 2nd Edn., by K. W. Britt.
Pub., Co. Ltd., New Delhi.
3. Fundamentals of Microbiology: M.Frobisher, W.B.Saunders Co., 6CT02 COMPUTER PROGRAMMING AND APPLICATIONS
Philadelphia. Note : Application of the following techniques for problems of inter-
4. Microbiology: P.L.Carpenter, W.B.Saunders Co., Philadelphia. est in chemical engineering, writing and testing of programs
5. Microbiological Methods: C.H.Collins & P.M.Lyne, Butterworth written in C Language.
and Co., London. SECTION-A
6. Food Processing Operations: M.A.Goslyn & J.Hold, The AVI Pub.
Co., INC, Westport. Unit I : Numerical solution of first order differential equations with
7. Principles of Food Science, Vol. II : G.Borgestrom the MacMilIan initial condition, Euler’s method, Runge-Kutta method.
Co. Ltd., London. Unit II : Systems of linear equations, solution by the method of de-
8. Technology of Food Preservation: Destosier, Norman W., AVI Pub. terminants, matrix inversion for the solution of linear equa-
Co., INC, London. tions, Gauss elimination method.
9. Practical Food Microbiology and Technology: H.H. Weiser, The Unit III : Roots of algebric and transcendental equation, iteration
AVI Pub. Co., Westport (Coun.) methods, Regula-Falsi method, Newton-Raphson method,
roots of simultaneous and solution set of transcendental
134 135
and algebric equations. Development of equations for heat 3. Soyabeans and Soyabean Products: K.B.NarkIev, Interscience
transfer, fluid mechanics and reaction engineering problems. Publishers, New York, Latest Edition.
SECTION-B 4. Hydrogenation of Fatty Oilseeds : Waterman, Lquosevier
Publishers, New York, Latest Edition.
Unit IV : Regression analysis - Least Square, error approach,
5. Fatty Acids: K.S.Markely (5 Vols.), Interscience Publishers, New
approximation by Chebychev orthogonal polynomial.
York.
Unit V : Elements of optimization techniques, single variable 6. Continuous Processing of Fats : M.K.Schwitzer, Latest Edition.
function, optimization-direct search, with and without 7. Refining of Oils and Fats for Edible Purposes: A.J.C. Anderson,
acceleration, method of regular intervals and fibonacci Academic Press, New York.
search method, gradient methods. 8. Vanaspati Industry: G.S.Hattangadi
Unit VI : Computer programming in modular form, use of subrou- 9. Practical Treaties on Vegetable Ghee Manufacture: Varma & Jaidev.
tine libraries, Block diagrams of preliminary aids in pro- 10. Solvent extraction of Vegetable Oils: H.Y.Parkb.
gramming, capacity optimization. I l. Refining and Technology of Oils and Fats: T.N.Mahatte, Small
PRACTICALS : Based on above theory. Business Publication, New Delhi.
12. Food Oils and their Uses: TJ.Weiss, Latest Edition.
TEXT BOOK : Digital Computation for Chemical Engineering by Leon
13. Bleaching Earths: M.K.H.Siddiqui, Latest Edition.
Lapidas, McGraw Hill, Latest Edition.
14. Progress in the Chemistry of Fats and other Liquids: R.T.Holman,
M.O.Luadberg & T.Malkin, Pergamon Press, New York (7Vols.)
6 OT 04 SPECIAL TECHNOLOGY-III
I5. Vegatable Fats and Oils: E. W.Eckay, Rinehold Publishers, New
(iii) OIL & PAINT TECHNOLOGY OF OIL York,
BEARING MATERIAI:S Latest Edition.
Domestic and World production of oil seeds and oils, storage, 16. The Chemistry, Flavouring and Manufacture in Chocolate,
sampling, Grading of oil seeds and oils. Pre-Extraction treatments of oil Confectionary and Cocoa: H.PJenson, Blackiston Publishers,
seeds. Mechanical expression, solvent extraction and other methods of Philadelphia, Latest Edition.
recovery of oils and fats. Economic aspects of these processes, processes 17. The Butter Industry: O.F.Huzoker, Latest Edition.
and plants employed for refining, bleaching, deororisation and 18. Margarine: A.J.C.Anderson, Academic Press, New York, Latest
hydrogenation of oils and fats. Edition.
Manufacture of butter, Ghee, margarine, vanaspati and SPECIAL TECHNOLOGY-III
confectionary fats. Transesterified oils, fats, winterization of oils. 6 PC04 (iv) PETROCHEMICAL TECHNOLOGY-Ill
Manufacture and evaluation of ancillary materials such as activated earths, PETROLEUM REFINERY ENGINEERING CALCULATIONS
activated carbons, nickel catalyst for hydrogenation. Cooking and salad ASTM, TBP, EFV distilIation curves, computation of the curves
oils, plastic shortening agents. from any one type by methods such as those or Nelson, Simister etc.
Environmental aspects in Oils seeds and oil processing units. Computation of various properties of petroleum fractions such as
Effective control according to Indian Standard specification. VABP,MABP, thermophysical properteis from refinery engineering chart.
Non Glyceride Constituents, general method of upgrading and Phase behaviour of multicomponent hydrocarbon systems retrograde
utilization of oils and fats, oil-cakes and other products. Synthetic fatty phenomena, K values and their estimate for complex mixtures K values
acids and glycerides. Recent advances in the field. corelations; Flash equilibrium calculation for multi component system by
method of successive approximations and simple methods such as that of
BOOKS RECOMMENDED : McHenry; Calculation of bubbic and dew points for complex mixtures,
1. Cottonseed and Cottonseed Products : A.B.Bailey, Interscience construction of phase diagram, successive flash for complex mixtures,
Publishers, New York, Latest Edition. multicomponent fractionation.
Separation criteria in crude oil fractionation, comparison with the
2. Industrial Oil and Fat Products: A.E.Bailey, Interscience Publishers,
simplest light hydrocarbon fractionation. Watkins method of covering crude
NewYork, Latest Edition. TBP to product TBP curve, concept of overflash.
136 137
Energy balance in a topping tower, types of reflexes and calculations FOUR YEAR DEGREE COURSE IN
involved, estimation of top side draw bottom and stripper temperatures. BACHELOR OF TEXTILE ENGINEERING
Brief account of topping tower design procedures: according to Nelson, SEMESTER - V (CREDIT & GRADE SYSTEM)
Watkins, Van Winkle (psudeo component design method), tray design. 5 TX 01 YARN MANUFACTURING –III
Entrainers and solvents for hydrocarbon separation by azeotropic
and extractive distillations. Types of pipe still heaters, calculation of radiant Section- A
absorption rates, Wilson Lobo, Hetel equation, Labo Evans method piple Unit I : Speed Frame- History of development, object, construction
still design. & working of speed frame. Top arm drafting system,
Problems illustrating the use of solvent extraction, absorption and Construction Flyer, Spindle and presser for twisting & winding
stripping in refinery operations and natural and refinery gas processing; operation. Objects, construction and working of Differential
multicomponent absorbers and strippers, calculation by Kremser-Brown Mechanism and Building Mechanism. Various Parameters
absorption factor procedure. affecting roving quality and production. Gearing and production
Heat exchangers in refinery design and operational problems, fluid calculations of speed frame. Faults in roving. Features of
mechanics and refinery applications. Use of combustion charts. modern speed frame.
Recent advances in the field. Unit-II : Ring Frame- Object, construction & working of ringframe,
(The subject has to be covemed entirely by Numerical) Details of Creel, Drafting system, Balloon control ring, lappet,
Books Recommended: Travelers, Rings, Aprons, top roller cots, spacers of ringframe.
1. Petroleum Refinery Engineering : W.L.Nelson, McGraw Hill, Compact Spinning- Introduction, Pneumatic compact spinning,
Kogakusha, 4th Edn., Latest Edition. Magnetic compact spinning,yarn properties of compact yarn.
2. Petroleum Refinery Distillation: R.N. Watkins, Gulf Pub. Co., Comparison of normal ring and compact yarn.
Texas, Latest Edition.
Unit-III : Ring Frame - Spinning Geometry- Spinning Angle, Spinning
3. Data Book on Hydrocarbons: J.B.Maxwall, K.E.Kriegar Pub. Co.,
triangle, Angle of Wrap.Formation of twist and its effects. Ring
New York, Latest Edition.
and traveler combination effect. Change places in ring frame.
4. Distillation: M. Van Winkle, McGraw Hill, Latest Edition.
Gearing & Building Mechanism of ring frame. Building of cops,
5. Handbook of Natural Gas Engineering: D.L.Katz & Others, McGraw
Types of spindles, Spindle drives. Draft and production
Hill, Latest Edition.
calculation. Development in Ring Spinning.
6. Applied Hydrocarbon Thermodynamics: W.C.Edmister, Gulf Pub.
Section - B
Co., Latest Edition, Vol. I & II.
7. Surface Operations in Petroleum Production: G.Y.Chilingar & Unit-IV : Ring Frame- Drafting, types of drafting system, types of draft.
C.M.Beeson, Elsevier, New York, Latest Edition. Drafting force, Roller slip, Floating fibres, Drafting waves,
8. Petroleum Processing Handbook: W.F.Bland & R.L.Davidson, Drafting capacity. Different Weighing methods, its advantages
McGraw Hill, Latest Edition. & limitation, Factors affecting on roller setting and drafting
9. Chemical Engg. : J.M.Coulson and J.F.Richardson, Pergamon Press performance. End Breakages-Causes, Effect & Control. High
3rd Edn., Vols. I & II, Latest Edition. speed drafting in ring spinning. Hairiness –causes control and
10. Equipment Design Handbook for Refineries and Chemical Plants: effect. Yarn Faults- causes, effects and control.
Frank L.Evans, Jr., Gulf Pub. Co., Houston, Texas, Latest Edition. Unit-V : Doubling- Object of doubling, twist and twist direction
effects, Tension effects, Balanced and unbalanced yarn,
6 CT 09 MINOR PROJECT
Properties of folded yarn,Doubling methods –dry, wet
Students are required to prepare and submit report on mini project
,Doubling machine – Ring doubler , Up twister, Two stage
on Software Development / Market Survey / Design / Fabrication / Site
twisting machine, Two For One twister and Three for One
Visit / Some Experimental Investigation / Validation in the relevant field
twister, Comparison of doubling machines. Fancy yarns-
under the guidence of teacher.
Introduction, types. Method of production, yarn properties, end
********
uses.

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