S12 Manual-16
S12 Manual-16
1
DRYING-INTRODUCTION, PRINCIPLE OF DRYING
During drying, the moisture from solids gets vaporised and diffused in dilute environment. Removal of
moisture takes place by high pressure or high temperature conditions. Drying removes the volatile materials
present inside solid matters. In some products, drying is carried to bring down the moisture content to a
predetermined limit
Some amount of moisture present in the pore spaces of grains. Excess amount of moisture remains in
bound form with absorbing materials of the grains. Mutual reaction takes place between absorbing materials
and moisture molecules, finally the moisture chemically bounds with the chemical constituents of the food
grains. Removal of moisture from wet materials by vaporisation depends on the rate of heat and mass
transfer, which is related with the following two basic phenomenon, (1) vaporisation of moisture from
surface of material, and (2) movement of moisture from internal parts of material to its surface. Movement
of moisture takes place because of diffusion, tell contraction and vapour pressure gradient.
Mechanism of Drying
When hot air is blow over a wet food, heat is transferred to the surface and latent heat of
vaporization causes water to evaporate. Water vapours diffuse through a boundary film of air
and is carried away by the moving air. This create a region of lower water vapour pressure
gradient is established from the moist interior of the food to the dry air. The gradient provides the
driving force for water removal from the food.
Schematic diagram of movement of moisture in the interstitial spaces of food cells during
drying in fruits and vegetables
where MC stands for moisture content, and the subscript wb designates “wet basis”.
Dry basis moisture content is the amount of water per unit mass of dry solids:
Note: The value of dry basis moisture content is more than the wet basis moisture content.
Practical No. 2
Drying methods (Thin layer and deep bed drying)-advantages and applications in food
industry
Aim: To know about the thin layer and deep bed drying
Introduction:
Drying and dehydration of fruits and vegetables is an age old method to preserve
these products. Removal of the water (75-90%) present in fresh commodity results in
reduction in the water activity and ultimately resistance against most of the deteriorative
agents. The removal of water is carried out by the application of heat and this heat is usually
supplied in the form of solar energy or artificially generated hot air. Removal of moisture and
exposure of heat often results in poor textural attributes, loss in nutritive value
(vitamins), discolouration and loss of flavouring components. Although both drying and
dehydration are interchangeably used, drying is referred to removal of water to an equilibrium
moisture content while dehydration is removal of water to an almost bone dry condition.
Drying of agricultural products is broadly carried in thin and deep layers.
Thin-layer drying
Deep bed drying
In deep bed dryers, the drying takes place in a drying zone and the layer of grains is more than 15
cm. A typical deep bed dryer is shown in below figure. At heated or drying air entry point, drying of
products starts. A drying zone is formed above the bottom layer which comes in contact of heated air.
Bulk of the drying takes place in the drying zone and this moves along the direction of drying air. In deep
bed system at a particular air flow rate, if the layer of product is more then the layer which comes in
contact with heated air first, may overdry. Therefore, it has been recommended that if the drying air is
43°C, the thickness of grain layer may be limited to 45 cm.
For analysis of deep bed drying method, it is assumed that the deep bed is formed by several thin
layers. In each thin layer, the incoming and outgoing air humidity and temperature change with time and
drying stages. This method is used to determine the drying period and the amount of water-vapour
removed from the products. Additional amount of moisture may be removed from dry layer till it attains the
equilibrium moisture content.
Deep bed drying system has been analysed by Hukill. The Hukill analysis is suitable for correlating the
drying period, product moisture and product depth factors for the solution of drying 'problems
Practical No.3
Types of dryer – Classification (Direct, Indirect and Air dryers)
Direct Dryers
Direct dryers use convection to efficiently transfer heat to the material being dried, enabling
fast and uniform moisture removal. In this method, the heat carrier—such as heated air, inert
gas, or steam—makes direct contact with the product. Hot air dryers are especially common:
hot air is circulated around and through the target material, providing the latent heat
necessary to vaporize adsorbed water, which is expelled with the exhaust air.
These dryers include rotary dryers, fluid bed dryers, and flash dryers, all of which are widely
deployed in industrial manufacturing for their energy efficiency and ability to scale up for
continuous, high-volume production. Direct continuous dryers typically achieve better heat
transfer rates than their indirect counterparts, increasing throughput, but may lead to higher
operating costs, increased energy consumption, and greater heat loss.
Optimizing the efficiency of direct drying often involves technologies such as lifting flights
—internal blades or vanes within rotary drum dryers—which maximize product contact with
drying gases and improve agitation for superior moisture removal. Recent advances in
process automation and heat recovery systems also help lower energy usage and
environmental impact, making modern direct dryers highly competitive for bulk material
drying.
Indirect Dryers
Indirect dryers operate based on conduction, where thermal energy passes through a solid
barrier—such as drum walls, tubes, or jackets—separating the heat transfer medium (usually
steam, hot oil, or heated surfaces) from the wet material. This indirect heat transfer prevents
contamination between fuel gases and product, making these dryers ideal for drying sensitive
goods, hazardous materials, pharmaceuticals, or food products where air purity is essential.
Classical types of indirect dryers include tray dryers, vacuum dryers, and shelf dryers. Low
airflow and tightly sealed process environments minimize dust, material loss, and risk of
explosion when handling combustible products. Indirect dryers often form part of batch
operations and are prized for their versatile application in research labs, fine chemical
manufacturing, and specialty food production.
Unlike in direct drying, there is no need for mixing flights or complex gas handling mechanisms,
as product never contacts combustion gases or external air streams. This simplifies exhaust
treatment, reduces environmental emissions, and protects final product quality.
Radiant Dryers
Radiant dryers (radiation dryers) utilize electromagnetic waves—such as infrared or microwave
energy—to deliver heat directly to the surface or core of materials. Unlike conventional methods,
radiant drying is a contactless process, minimizing the risk of cross-contamination and enabling
efficient moisture removal with very low environmental impact. These systems offer fast
response times, uniform heating, and the capability to dry heat-sensitive coatings, adhesives, and
specialized industrial products.
Air Dryers
Air dryers, also known as compressed air dryers or dehumidifiers, are engineered to extract
excess moisture from ambient air in industrial settings—particularly from compressed air
systems used in pneumatic machinery, process control, or packaging operations. Ambient air
typically contains 30% to 50% relative humidity, but when compressed, its moisture content can
approach saturation (100%), introducing risks such as water condensation, corrosion, decreased
equipment performance, and contamination of sensitive products.
Efficient air drying is accomplished with technologies and equipment such as refrigerated air
dryers, desiccant dryers, and membrane dryers, among others. Methods may include lowering
the dew point of air via cooling, utilizing absorbent or adsorbent materials (such as silica gel or
activated alumina), or pressure swing adsorption to separate water vapor. Refrigerated dryers use
a heat exchanger to cool the compressed air, causing moisture to condense for removal.
Desiccant dryers pass air through moisture-absorbing materials, while membrane dryers
selectively allow water vapor to permeate through specialized fibers, resulting in ultra-dry
process air.
Routine moisture buildup is an unavoidable result of compressing and processing air, making
reliable moisture removal essential for operational safety, product quality, and regulatory
compliance. Selecting the optimal air dryer—tailored for factors like flow rate, pressure, dew
point requirements, and application-specific contaminants—ensures efficient, uninterrupted
production. Air dryer manufacturers offer expert guidance to help users choose the right
equipment and ensure efficient operation for diverse industries including automotive, electronics,
food processing, and pharmaceuticals.
Conveyor Dryers
Conveyor dryers are state-of-the-art systems for continuous drying of bulk materials, food
products, textiles, granules, and powder. Using a conveyor belt—typically mesh or webbed—
these dryers transport products through zones of controlled temperature, humidity, and air
velocity, ensuring even and rapid moisture removal. The conveyor design permits optimal
airflow both above and below the material, promoting fast drying while limiting product
degradation.
Modern conveyor dryers adopt multi-stage or multi-pass designs. Products may transition from
one belt level to another—often via gravity—to allow for variable residence times, which
enhances the uniformity of drying, especially valuable for sensitive food products and
vegetables. Airflow is carefully engineered through turbine fans or precision nozzles, delivering
adjustable drying profiles for a wide range of materials, from low to high viscosity.
Energy savings, minimized labor intervention, scalability, and the ability to integrate with
upstream or downstream conveyors make this category essential for high-throughput industrial
manufacturing, food dehydration, powder coatings, and fabricated parts.
Practical No.4
TRAY DRYER: WORKING PRINCIPLE, ADVANTAGES & DISADVANTAGES; ITS
APPLICATIONS IN FOOD INDUSTRY
Sorting
Washing
Separation of seeds
Peeling
Slicing
Pre-treatment
Drying
Packing
Procedure:
Take fresh fruit/vegetable and sort them and wash to remove the dust particles on the
surface.
Fruits are cut by a special slicing machine into slices at light angles to the core hole and
inch thick.
It is dipped into ascorbic acid solution or if the fruits is sulphured, it should be spread
upon the trays in the cabinet drier to a uniform depth.
This slices are kept in the tray dryer for drying.
The dried fruit slices are stored.
Observation:
Initial weight of fruit :
Temperature in Tray drier (0C) :
Time taken for drying :
Final weight of dried fruit slices :
Moisture content in dried fruit slices :
Initial weight of vegetable :
Temperature in Tray drier (0C) :
Time taken for drying :
Final weight of vegetable slices :
Moisture content in dried vegetable slices :
Practical No.5
CABINET DRYER: WORKING PRINCIPLE, ADVANTAGES & DISADVANTAGES;
ITS APPLICATIONS IN FOOD INDUSTRY
Sorting
Washing
Separation of seeds
Peeling
Slicing
Pre-treatment
Drying
Packing
Procedure:
Take fresh fruit/vegetable and sort them and wash to remove the dust particles on the
surface.
Fruits are cut by a special slicing machine into slices at light angles to the core hole and
inch thick.
It is dipped into ascorbic acid solution or if the fruits is sulphured, it should be spread
upon the trays in the cabinet drier to a uniform depth.
This slices are kept in the cabinet dryer for drying.
The dried fruit slices are stored.
Observation:
i) Initial weight of fruit :
Temperature in cabinet drier (0C) :
Time taken for drying :
Final weight of dried fruit slices :
Moisture content in dried fruit slices :
ii) Initial weight of vegetable :
Temperature in cabinet drier (0C) :
Time taken for drying :
Final weight of vegetable slices :
Moisture content in dried vegetable slices :
Practical No.6
SOLAR DRYER: WORKING PRINCIPLE, ADVANTAGES & DISADVANTAGES; ITS
APPLICATIONS IN FOOD INDUSTRY
Solar drying can only happen on sunny days unless it’s combined with a regular energy-
based system.
Solar dryers are slower than those using conventional fuels due to limited solar energy
collection.
They are typically used for drying at temperatures between 40-50 degrees Celsius.
Poor product quality than other mechanical dryers.
Observations:
1). Initial weight of raw fruit :
Temperature in solar drier (0C) :
Time taken for drying :
Final weight of dried fruit slices :
Moisture content of dried fruit slices :
2). Initial weight of vegetable :
Temperature in solar drier (0C) :
Time taken for drying :
Final weight of dried vegetable slices :
Moisture content in dried vegetable slices :
Practical No. 7
SPRAY DRYER: WORKING PRINCIPLE, ADVANTAGES & DISADVANTAGES; ITS
APPLICATIONS IN FOOD INDUSTRY
Grading
Leaf powder
The drum dryer, a moving bed dryer, is constructed using cast iron and
stainless steel materials.
The MOC of the drum dryer has durability, cleanliness, and resistance to chemical
attacks.
It consists of a hollow steel drum of about 0.75 to 1.5 m in diameter and 2.4 m in
length.
It is heated internally, usually by steam, and rotates in its longitudinal axis.
The external surface of the drum is polished for long sustainability.
For drying purposes, the materials are fed into the pan.
The drum is partially dipped in the pan.
Spreader is used in spreading liquid film eventually on a drum roller.
The drum is rotated continuously and its speed is adjusted so that all the liquid is
fully vaporized.
Dried deposited or material can be scraped off with the help of a knife and
collected in a storage bin.
Milk powders: While spray drying dominates bulk milk powder production, drum dryers excel
in specialized applications where instant solubility or agglomerated properties are required.
Cheese powder production: Drum dryers can process cheese concentrates into flavorful, easily
dispersible powders for snack seasonings, sauces, and ready meals.
Yogurt powders: The drum drying process preserves many of the sensory properties of yogurt
while creating shelf-stable powder formats.
Dairy-based infant formula components: Certain specialized ingredients benefit from the
unique structural modifications achieved through drum drying.
The ability to handle high-fat dairy products without significant cleaning challenges makes food-
grade drum dryers particularly valuable in cheese processing applications. Modern dairy-focused
drum dryer systems incorporate specialized feeding mechanisms and surface treatments that
prevent protein build-up and facilitate effective cleaning protocols.
Fruit and Vegetable Processing: Preserving Flavor and Nutrition
The fruit and vegetable sector has embraced drum drying technology for multiple applications:
Potato flakes for instant mashed potatoes: Perhaps the most recognized drum-dried food
product, these flakes require precise control of gelatinization and film formation that only drum
drying can efficiently provide.
Fruit purees and powders: Drum drying preserves color, flavor, and nutritional compounds
while creating shelf-stable fruit ingredients for snacks, cereals, and confectionery.
Vegetable powders: From tomato powder to pumpkin and carrot ingredients, drum drying
creates versatile vegetable ingredients with good color retention and reconstitution properties.
Soup and sauce bases: Pre-gelatinized vegetable starches and vegetable concentrates form the
foundation of many convenience food applications.
The drum drying process is particularly valued in fruit applications for its ability to maintain
natural pigmentation and flavor compounds better than some alternative technologies. For
vegetables containing high starch content, the simultaneous gelatinization and drying creates
unique functional properties impossible to achieve with other drying methods.
Pre-gelatinized flours and starches: These instantly soluble ingredients provide thickening and
texture in various food applications without cooking.
Cereal-based baby foods: The controlled gelatinization process creates easily digestible,
instantly reconstitutable baby cereals.
Specialty grain ingredients: Ancient grains and alternative cereal sources can be processed into
highly functional ingredients.
Breakfast cereal components: Many ready-to-eat cereals incorporate drum-dried ingredients for
texture and nutritional enhancement.
The versatility of drum dryers allows manufacturers to process various grain-based slurries with
different viscosities and solids content, making them ideal for product development and
innovation in the cereal category.
Functional Food Ingredients: Supporting Health and Wellness Products
The growing functional food sector leverages drum drying technology for:
Protein concentrates: Plant and dairy proteins can be transformed into more soluble,
application-friendly formats.
Fiber ingredients: Certain dietary fibers benefit from the structural modifications achieved
through drum drying.
Probiotic carriers: When configured for lower-temperature operation, drum dryers can create
protective matrices for probiotic cultures.
Nutritional beverage bases: Instantly dispersible nutritional formulations rely on the unique
properties of drum-dried ingredients.
Observation:
Initial moisture content in food :
Type of roller (single or pair of rollers) :
Gap between pair of rollers (mm) :
Temperature of the roller surface :
RPM of roller :
Final moisture content in dried food :
Practical No. 10
FLUIDIZED BED DRYER: WORKING PRINCIPLE, ADVANTAGES &
DISADVANTAGES; ITS APPLICATIONS IN FOOD INDUSTRY
Aim: To study the drying characteristics of a given material in a fluidized bed dryer.
Introduction:
The fluidised bed drying technique holds an important position among modern drying methods. It is
used mainly for granular materials, nevertheless, it is also applicable in the drying of solutions, pastes and
liquids sprayed onto the fluidised inert bed.
Working principle:
The principle of operation of fluidised bed dryer is to provide sufficient air pressure to fluidise a
thin bed of grain/product, giving excellent air/grain contact Above a certain pressure, related to the weight
per unit area of the grain bed, the pressure drop across the bed becomes constant with volume flow rate, so
that fast drying can occur. The drying method is based on ventilating hot air through the bed of product
kept on the support grid or the gas distributor. When the air velocity becomes higher than the critical
fluidisation velocity, the bed progressively expands until it reaches a state that of boiling liquid. This
phenomenon is called fluidization.
Advantages:
Fluidity of bed facilitates continuous and easy equipment performance even on very large
scale plants.
Lack of moving parts.
Very good condition for heat and mass transfer.
Provides good mixing i.e. uniformity of drying of the material in the bed.
Disadvantages:
While efficient, the initial energy requirement for fluidizing the bed can be high,
especially in large-scale operations.
The technology is most effective with powders and small particles. Larger or irregularly
shaped materials might not fluidize properly and could lead to uneven drying.
Fine powders or sticky materials can cause clogging of the bed or fouling in the
equipment, which can lead to maintenance issues and lower efficiency.
Fluidized bed dryers can be more complex and costly to install and maintain compared to
other drying methods, like tray or conveyor dryers.
Procedure
Select the vegetable seeds and clean it thoroughly with screen cleaners.
Seeds are pre-conditioned to improve drying quality.
Loading the seeds into fluidized bed dryer.
Adjust the drying parameters of dryer like temperature, air flow rate and humidity.
The air should be heated gradually to the set temperature (usually between 40°C to
50°C).
As the hot air passes through the seeds, they should begin to fluidize, meaning the seeds
will be suspended in the air, moving gently around. This ensures uniform drying.
The drying time varies based on the moisture content of the seeds and the airflow
settings. Generally, the drying process for vegetable seeds can take from 1 to 4 hours,
depending on seed type and moisture content.
The dried seeds are stored.
Observations:
Initial weight of seeds :
Final weight of dried seeds :
Moisture content in dried seeds :
Practical No. 11
PNEUMATIC DRYER: WORKING PRINCIPLE, ADVANTAGES &
DISADVANTAGES; IT’S APPLICATIONS IN FOOD INDUSTRY
Aim: To know about the working of pneumatic dryer.
Introduction:
Drying is a separation process that converts a wet solid, semisolid, or liquid feedstock into a
solid product by evaporation of the liquid into a vapour phase with the application of heat.
Drying is a separation process that converts a wet solid, semisolid, or liquid feedstock
into a solid product by evaporation of the liquid into a vapor phase with the application of
heat. Essential features of the drying process are phase change and production of a solid.
One of the most widely used drying systems is flash drying and is also known as pneumatic
drying. Flash dryers are most commonly direct drying units and are also known as
convective dryers. Pneumatic or flash dryers may be classified as gas–solid transport systems
that are characterized by continuous convective heat and mass transfer processes.
Working principle:
A simple pneumatic flash drying system in which particulate solids are dried during
transport in a hot gas stream (usually air or combustion gases). The simple flash drying
system includes six basic components: the gas heater, the wet material feeder, the drying duct,
the separator, exhaust fan, and a dried product collector. The wet particles are fed into the
hot gas stream sometimes with special mixing devices. The stream flows up the drying tube.
The gas velocity must be greater than the free fall velocity of the largest particle to be dried.
The gas velocity in relation to the particle velocity is high. Thermal contact between the
conveying air and the solids is usually very short and therefore flash dryers are most suitable
for removal of external moisture (surface moisture) and are less suitable for removal of
internal moisture. At the end of the drying process a dust separation arrangement is
installed. It must comply with the regulations for pollution control. For this purpose cyclone
dust sep- arators, fabric filters, electrostatic precipitators, wet scrubbers, and fabric filters
are used.
Advantages
Short contact time and parallel flow make possible to dry thermolabile
materials.
The dryer needs only a very small area and can be installed outside a
building. However, the gas cleaning system should be located inside the
building in order to avoid moisture and dust deposition.
The dryer is easy to control. The low material content in the dryer enables
equilibrium conditions to be reached very quickly.
Due to small number of moving parts the maintenance cost is low.
The capital costs are low in comparison with other types of dryers.
Simultaneous drying and transportation is useful for materials handling
process.
Disadvantages
Practical No.13
HYBRID DRYING-WORKING PRINCIPLE, ADVANTAGES & DISADVANTAGES;
ITS APPLICATIONS IN FOOD INDUSTRY
Aim: To study about the working of hybrid drying.
Introduction:
The main objective of food drying is preservation; however, the choice of drying method
can significantly alter the characteristics and quality of the final product. The primary motivation
behind developing hybrid drying technologies is to minimize product degradation while
achieving the desired moisture content. It is essential to consider the impact on food quality
parameters when utilizing different drying mechanisms to produce high-quality dried products.
Hybrid drying in food processing involves the strategic integration of multiple drying techniques
to enhance efficiency, improve product quality, and minimize energy consumption compared to
traditional single-method drying processes. This innovative approach combines conventional
methods like convective (hot air) drying with advanced technologies such as infrared (IR) or
microwave (MW) drying, leveraging the unique benefits of each method to achieve superior
results.
Classification of Hybrid drying
Hybrid drying technology are often defined as processes that utilizes two or more drying
stages, multiple heat transfer modes and also two or more types of dryers to achieve the product
quality, desired dryness, manufacturing throughput and drying time. The following flowchart
depicts general classification of hybrid drying technology.
-Similar drier type at each - Microwave freeze drying -Drying & filtration
stage
-Two stage vibro fluid
beds
-Two stage fluid beds
Hybrid drying systems, which typically combine different drying techniques such as
conventional air drying, solar drying, microwave drying, and others, offer several advantages for
drying agricultural products like fruits and vegetables, grains, dairy, and meat products.
Observation:
Type of Hybrid Initial Drying Final weight Moisture
product drying weight temperature content
method
Practical No. 14
FOAM MAT DRYING: WORKING PRINCIPLE, ADVANTAGES &
DISADVANTAGES; ITS APPLICATIONS IN FOOD INDUSTRY
Aim: To preserve any fruit pulp by foam-mat drying.
Introduction:
Most of the fruits are highly perishable with a limited shelf life and is susceptible to
mechanical damage during post-harvest handling and transportation. Therefore, the conversion
of the fruit into powder could be useful not only to reduce the post-harvest losses but also to
retain nutritional quality in the processed products. Processed food products from fruits are
highly desirable and dehydrated fruits can be used in many food product formulations.
In this drying process, a liquid material is converted into foam that is stable by being
whipped after adding an edible foaming agent. The stable foam is then spread out in sheet or mat
and dried by using hot air (40-90°C) at atmospheric pressure. Methyl cellulose (0.25-2%), egg
white (3-20%), maltodextrin (0.5-05%), and gum Arabic (2-9%) are the commonly utilized
additives for the foam-mat drying process at the given range, either combined together for their
effectiveness or individual effect. The foam-mat drying process is suitable for heat sensitive,
viscous, and sticky products.
Principle:
Observation:
Initial weight of sample :
Drying Temperature :
Drying Time :
Final weight of sample :
Moisture content in dried product :
Practical No. 15
CONVEYOR DRYER: WORKING PRINCIPLE, ADVANTAGES & DISADVANTAGES;
ITS APPLICATIONS IN FOOD INDUSTRY
Introduction:
A conveyor belt dryer is a kind of drying equipment for batch continuous production
which is heated by electric heating, steam heating, and hot air. It is using steel mesh as a
conveyor belt to carry materials for continuous drying.
The machine mainly conveys the materials directly to the flat conveyor through the conveyor.
The material is evenly distributed on the dryer through the scraper at the upper end of the flat
conveyor. This can improve the air permeability of the material to better achieve the drying
effect.
Working principle:
The main principle of a continuous belt dryer is to lay the material evenly and flatly on
the mesh belt. The mesh belt dragged by the transmission device to move back and forth in the
conveyor belt dryer, the hot air passes through the material and the water vapor is discharged
from the moisture discharge hole, so as to achieve the purpose of drying. The length of the box is
combined with standard sections. In order to save space, the conveyor dryer can be made into
multi-layer type.
Advantages
Food samples have very intimate contact with air/gas stream.
Good for heat sensitive products and products requiring long residence times.
Energy efficient due to recycling of process air Multiple zones offer flexibility for
temperature and process control.
Minimal handling of food product.
Unit can have integral cooling section.
Disadvantages
High temperature units can be troublesome.
Belt tracking can be problematic.
Belt may clog, requires frequent cleaning.
Write about the process parameters that affect the conveyor drying in fruits and
vegetables.
Practical No. 16
MOISTURE CONTENT DETERMINATION METHODS-HOT AIR OVEN METHOD,
INFRARED METHOD
Aim: To know about the methods for determination of moisture content.
Introduction:
The moisture content of food grains and other agricultural products plays an important
role in maintaining the desirable quality of the product. Changes in moisture content of a
agricultural material occur during their harvesting, processing and marketing. The change in
moisture content during successive post-harvest stages is dependent upon the initial moisture
content of product and atmospheric conditions.
There are several methods for determination of Moisture content of
agricultural products. For determination of Moisture content of a particular product, the
choice of method depends on many factors, they are:
The form in which water is present in the product
The relative amount of water present
The rapidity of determination
Accuracy of method
Products nature whether easily oxidised or decomposed
The cost of equipment used.
Moisture content determination methods
Hot air oven method:
Procedure
1. The container was dried for 30 min at 103±1°C in the oven and then the container was
cooled in desiccator to room temperature.
2. The container weight was recorded as w1.
3. 10 g sample was placed in the container, the sample and container was weighed and
initial weight, w2 was recorded.
4. The sample and container was placed in the oven for 16 h at 103±1 °C.
5. The sample with the container was removed from the oven and it was cooled in the
desiccator to room temperature.
6. After that, the sample with the container was removed from the desiccator and weighed
immediately, and weigh, w3 was recorded.
Two methods are used to express the moisture content of materials: wet basis
and dry basis moisture content.
When performing these calculations, it is assumed that the sample loses only
water and that the weight of the dry matter remains constant.
Wet basis moisture content (designated MW in the text) is described by the percentage equivalent of
the ratio of the weight of water (WW) to the total weight of the material (Wt).
Note that wet basis moisture content can range from 0 to 100 percent.
Wet basis moisture is used to describe the water content of agricultural materials and food products.
When the term "moisture content" is used in the food industry it almost always refers to wet basis
moisture content. One important example occurs in the grain industry where moisture content of
whole grains is determined at each point in the marketing channel where the grain changes
ownership.
Dry basis moisture content (designated Md in the text) is described by the percentage equivalent of
the ratio of the weight of water (WW) to the weight of the dry matter (Wd).
Note that dry weight moisture content can range from 0 to very large percentages.
Dry basis moisture is most commonly used for describing moisture changes during drying. When a
sample loses or gains moisture, the change in the dry basis moisture is linearly related to the weight
loss or gain.
If MW, the wet basis moisture content in percent, is known, the dry basis moisture content can be
calculated using:
If Md, the dry basis moisture content in percent, is known, the wet basis moisture content can be
calculated using: