Pgc5000 Series
Pgc5000 Series
PGC5000 Series
Process Gas Chromatographs
As a part of ABB, a world leader in process automation technology, we offer customers application expertise, service
and support worldwide.
We are committed to teamwork, high quality manufacturing, advanced technology and unrivalled service and support.
The quality, accuracy and performance of the Company’s products result from over 100 years of experience,
combined with a continuous program of innovative design and development to incorporate the latest technology.
SI/PGC5000-EN, rev B 2
Contents
1 Glossary ..............................................................5 5.7.1 System backup and recovery.................... 30
5.7.2 System backup error messages ................ 31
2 Safety and symbols .............................................6 5.8 Restarting the analyzer .......................................... 32
5.9 Upgrading software ............................................... 33
3 Introduction ........................................................7 5.10 Optional discharge ionization detector ................ 33
3.1 General..................................................................... 7 5.10.1 Plasma will not light .................................. 33
3.2 Drawings .................................................................. 7 5.10.2 No signal .................................................... 33
3.3 Master controller..................................................... 7 5.10.3 Low signal .................................................. 34
3.4 Class b oven ............................................................. 7 5.10.4 Noisy .......................................................... 34
3.4.1 Liquid version.............................................. 8 5.10.5 High baseline ............................................. 35
3.4.2 Vapor version.............................................. 8 5.10.6 Drifting baseline ........................................ 35
3.5 Class c oven .............................................................. 8 5.10.7 Spikes ......................................................... 35
3.6 Air purge systems .................................................... 8 5.10.8 Shifting retention times ............................ 35
3.7 System variations .................................................... 8
6 Component repair .............................................36
4 Maintenance .......................................................9 6.1 General ................................................................... 36
4.1 Equipment and supplies required........................... 9 6.1.1 Preparation and procedures .................... 36
4.2 Preventive maintenance ......................................... 9 6.1.2 Electrostatic discharge information ......... 36
4.2.1 Gas cylinder replacement .......................... 9 6.1.3 Powering down the analyzer system ....... 36
4.2.2 Cleaning .................................................... 10 6.1.4 Equipment and supplies required ............ 36
4.3 System backup ....................................................... 10 6.2 Master controller cabinet ...................................... 37
4.4 USB connectors...................................................... 10 6.2.1 SBC and card cage assembly..................... 37
6.2.2 Oven controller pcb .................................. 38
5 Diagnostics and troubleshooting ....................... 11 6.2.3 Power supply............................................. 38
5.1 General................................................................... 11 6.2.4 Optional wago modules............................ 38
5.1.1 Power-on self test ................................................. 11 6.3 Master controller cabinet door ............................. 38
5.1.2 Indicator boxes and hex codes.............................. 11 6.3.1 Front panel pcb ......................................... 39
5.2 Power ..................................................................... 13 6.3.2 Liquid crystal display assembly ................ 39
5.2.1 Power failure recovery ............................. 13 6.4 Oven component locations ................................... 40
5.2.2 Oven LED indicators ................................. 13 6.4.1 Class b oven components, v1 ................... 40
5.2.3 System board battery ............................... 14 6.4.2 Class b oven components, v2 ................... 40
5.3 Board level light emitting diodes .......................... 14 6.4.3 Class c oven components ......................... 41
5.3.1 Single board computer ............................. 14 6.5 Replacing the epc control pcb ............................... 41
5.3.2 Oven controller pcb .................................. 16 6.6 Replacing the epc control assy .............................. 41
5.3.3 DTC digital pcb, version 1 ......................... 17 6.6.1 Preparation ............................................... 41
5.3.4 DTC digital pcb, version 2 ......................... 19 6.6.2 Removing the epc control assy ................ 42
5.3.5 Detector CANbus node identification...... 20 6.6.3 Installing the epc control assy .................. 43
5.4 Indicator troubleshooting procedures ................. 21 6.6.4 Removing a sensor pcb ............................. 44
5.4.1 Identifying issues ...................................... 21 6.6.5 Installing a new sensor pcb ...................... 45
5.4.2 Correcting issues ...................................... 21 6.6.6 Removing a proportional valve ................ 45
5.5 Status indicators .................................................... 21 6.6.7 Installing a new proportional valve .......... 46
5.6 Operation troubleshooting ................................... 27 6.6.8 Removing the control pcb ........................ 46
5.6.1 Baseline noise ........................................... 27 6.6.9 Installing a new control pcb ..................... 46
5.6.2 Baseline or signal offset ........................... 27 6.6.10 Removing the heater ................................ 47
5.6.3 No peaks ................................................... 28 6.6.11 Installing a new heater ............................. 47
5.6.4 Double sampling ....................................... 28 6.7 FID amplifier assembly........................................... 47
5.6.5 Mystery peaks .......................................... 28 6.8 FPD electrometer ................................................... 48
5.6.6 Individual peak missing on report ........... 29 6.9 TCD amplifier assemblly ........................................ 48
5.6.7 Chromatogram oversized or off scale ..... 29 6.10 Replacing the dtc analog pcb, v1........................... 48
5.6.8 Variable sample size ................................. 29 6.11 Replacing optional zone board .............................. 49
5.6.9 Variable retention times .......................... 29 6.12 Replacing dtc digital pcb, v1 .................................. 49
5.6.10 Reduced peak size .................................... 29 6.13 Replacing oven indicator pcb ................................ 49
5.6.11 Loss of power............................................ 26 6.14 Replacing dtc master analog pcb, v2..................... 49
5.6.12 Flame Out LED on ..................................... 30 6.15 Replacing dtc digital pcb, v2 .................................. 50
5.7 Software................................................................. 30 6.16 Replacing dtc auxiliary pcb .................................... 50
SI/PGC5000-EN, rev B 3
6.17 Replacing power distribution board ..................... 50 7.7.3 Replacing the wedges ............................... 68
7.7.4 Replacing the o-rings ................................ 68
7 Subassembly repair ........................................... 52 7.7.5 Replacing the valve plate .......................... 70
7.1 Column repair ........................................................ 52 7.8 Replacing diaphragm valves .................................. 70
7.1.1 Column removal ....................................... 52 7.8.1 Preparation ............................................... 70
7.1.2 Packed column installation ...................... 52 7.8.2 Removing a valve ...................................... 71
7.1.3 Capillary column installation.................... 52 7.8.3 Replacing the diaphragm (4 screw).......... 71
7.1.4 Cutting capillary columns ......................... 53 7.8.4 Replacing the diaphragm (1 screw).......... 72
7.2 Repairing the flame ionization detector ............... 53 7.8.5 Installing the new diaphragm valve ......... 72
7.2.1 FID cell access ........................................... 54 7.9 Optional discharge ionization detector ................ 73
7.2.2 Replacing the breather ............................. 54 7.9.1 Scheduled maintenance ........................... 73
7.2.3 Replacing the thermocouple assembly ... 54 7.9.2 Removing the detector ............................. 73
7.2.4 Replacing the polarizer............................. 54 7.9.3 Installing the detector .............................. 73
7.2.5 Replacing the igniter assembly ................ 55 7.9.4 Replacing the Exhaust tube ...................... 74
7.2.6 Cleaning the fid jet ................................... 55 7.9.5 Replacing the Power Supply ..................... 74
7.2.7 Replacing the fid cable assembly ............. 56
7.3 Repairing the single port tcd ................................. 56 8 Replacement parts.....................................................75
7.3.1 Removing the filaments ........................... 57 8.1 Ordering information ............................................. 75
7.3.2 Installing the filaments ............................. 57 8.1.1 Equipment identification .......................... 75
7.3.3 Filament checkout .................................... 57 8.1.2 Master controller config identification .... 75
7.3.4 Leak test .................................................... 58 8.1.3 Oven configuration identification ............ 76
7.3.5 Connecting the filaments ......................... 58 8.1.4 Software configuration identification ...... 76
7.3.6 Potting the filaments ................................ 58 8.1.5 How to order ............................................. 76
7.3.7 Re-installing mounting bracket cover ...... 58 8.2 Master controller ................................................... 77
7.4 Repairing the multiport tcd ................................... 59 8.2.1 Back of door .............................................. 77
7.4.1 Accessing the detector ............................. 59 8.2.2 Master controller chassis ......................... 77
7.4.2 Removing the filaments ........................... 59 8.3 Class b1 oven components .................................... 78
7.4.3 Installing new filaments ........................... 59 8.3.1 Left side components ............................... 78
7.5 Repairing the flame photometric detector .......... 61 8.3.2 Left front door components ..................... 78
7.5.1 Replacing the photomultiplier assembly . 61 8.4 Class b2 oven components .................................... 79
7.5.2 Replacing the burner block ...................... 61 8.3.1 Left side components ............................... 79
7.5.3 Replacing the burner block o-rings .......... 62 8.3.2 Left front door components ..................... 79
7.5.4 Replacing the jet ....................................... 62 8.5 Class b main interior components......................... 80
7.6 Liquid sample valve repair .................................... 63 8.5.1 Liquid sample valve ................................... 81
7.6.1 LSV disassembly on the analyzer ............. 64 8.5.2 Flame ionization detector......................... 82
7.6.2 LSV reassembly on the analyzer .............. 64 8.5.3 Single-port tcd ........................................... 82
7.6.3 Removing LSV from the analyzer ............. 66 8.5.4 Multiport tcd ............................................. 83
7.6.4 Installing LSV on the analyzer .................. 66 8.5.5 Flame photometric detector .................... 83
7.7 CP valve repair ....................................................... 67 8.5.6 Burner block components ........................ 84
7.7.1 Preparation and safety ............................. 67 8.5.7 M2CP valve ................................................ 84
7.7.2 Replacing the slider .................................. 67 8.5.8 Optional DID replacement parts .............. 85
8.6 EPC control assembly............................................. 85
8.7 Class c oven ............................................................ 86
SI/PGC5000-EN, rev B 4
1 Glossary
ACL Access Control List
AOC Absence of Condition
BIOS Basic Input/Output System
CAN Controller Area Network
CPU Central Processing Unit
DID Discharge Ionization Detector
DSP Digital Signal Processor
DTC Digital Temperature Controller
EPC Electronic Pressure Controller
ESD Electrostatic Discharge
FID Flame Ionization Detector
FPD Flame Photometric Detector
I/O Input/Output
LCD Liquid Crystal Display
LED Light Emitting Diode
LSV Liquid Sample Valve
LUI Local User Interface (operational software interface located on the Master Controller)
MC Master Controller
PC Personal Computer
PCB Printed Circuit Board
PDO Process Data Object
PGC Process Gas Chromatograph
PIC Programmable Integrated Circuit
POST Power-On Self Test
PTFE Polytetrafluoroethylene
RAM Random Access Memory
RTC Real Time Clock
RTD Resistance Temperature Detector
SBC Single Board Computer
TCD Thermal Conductivity Detector
TCF Time Coded Function
USB Universal Serial Bus
SI/PGC5000-EN, rev B 5
Indicates that the referred item can be Indicates that referenced items are
hot and should not be touched without susceptible to Electrostatic Discharge
care. (ESD) damage and should not be
touched without ESD safe handling
tools.
Indicates that a risk of electrical shock
and/or electrocution exists.
SI/PGC5000-EN, rev B 6
3 Introduction
3.1 General
The PGC5000 Series Process Gas Chromatograph (analyzer) separates and measures the individual components of gas or liquid
samples. It automatically samples and analyzes process streams, using the analyzer’s Master Controller to control analytical
functions.
The PGC5000 analyzer is compatible with early versions (before version 4) of the STAR Data Management System.
Each analyzer has a temperature code (T-Rating) listed on the nameplate. This T-Rating indicates the temperature classification
of the area in which the analyzer has been designed to operate. T-Ratings and area classifications for analyzer locations are
determined and supplied by the customer.
The analyzer consists of a Master Controller and associated ovens (see Figure 3.1).
Class C Class B
Oven Oven
Master
Controller
An Important Documents CD-ROM comes with the analyzer. Included on this CD are data sheets, installation drawings, and
replacement parts lists needed to support installation and operation of the analyzer. This manual refers to these data sheets
and drawings as the “Data Package.”
3.2 Drawings
Since analyzer configuration depends on the particular application, this manual does not contain generic engineering drawings
and diagrams. You should utilize the drawings, diagrams and replacement parts lists provided on the Data Package supplied
with your analyzer to ensure you are using the correct ones for your system.
The Master Controller contains a Card Cage with a Single Board Computer (SBC) PCB, a Power Supply, one or more Oven
Controller PCBs, and optional Wago input/output modules. The front panel assembly has a liquid crystal display (LCD), keypad,
and front panel board. Later versions of the front panel assembly have a touchscreen.
SI/PGC5000-EN, rev B 7
• The liquid sample valve injects a fixed volume of sample into a vaporizing chamber.
• “Sweep gas” transports sample out of the vaporizing chamber.
• Carrier transports the vaporized sample into the column.
• The column then separates the components and passes them into the detector.
• The detector measures the sample across the range of high to low concentration.
The liquid sample valve is externally mounted on the right side of the Oven Compartment and extends through the isothermal
oven, allowing direct injection. It is actuated by a solenoid valve located in the Oven Electronics Compartment. The liquid
sample valve captures a specific volume of liquid sample below its bubble point, injects it into a temperature controlled
(vaporizing) chamber of the LSV, which then sends the vaporized sample into the oven.
SI/PGC5000-EN, rev B 8
4 Maintenance
4.1 Equipment and supplies required
Factory Data Sheets from the Data Package
Flow measuring device
To aid in preventive maintenance, keep reference chromatograms for comparison and assisting with early
detection of issues as described in the Troubleshooting section.
INTERVAL ROUTINE
Check:
• Instrument air supply
• Sample system flows and pressures
• Cylinder gas pressures; replace as necessary
Monthly/Quarterly Check carrier line dryers; change as necessary to prevent pressure drop.
SI/PGC5000-EN, rev B 9
When you use a single cylinder to supply a gas, check the cylinder regularly and replace it when the pressure falls below 100
psig, using another cylinder containing the specified gas.
4.2.2 Cleaning
Prior to cleaning the analyzer, turn off the power to the unit. Avoid using chemical agents which might
damage the component parts of the analyzer.
Clean the analyzer as often as environmental conditions require. Accumulation of dirt in certain oven subassemblies can cause
overheating and component failure, because dirt on components acts as insulating material preventing efficient heat
dissipation.
Remove loose dirt accumulated on the outside of the analyzer with a soft cloth or a small paint brush.
Remove any remaining dirt with a soft cloth dampened in a mild solution of water and detergent. Do not use abrasive cleaners
on the analyzer.
Remove dust in the inside of the oven, to eliminate electrical conductivity, and possible short circuits under high humidity
conditions.
The best way to clean the interior is to dislodge the accumulated dust with dry, low-velocity air and then
remove any remaining dirt with a soft paint brush and vacuum cleaner.
USB
Ports
SI/PGC5000-EN, rev B 10
The POST process tests the basic integrity of the analyzer’s boards during every startup cycle. The POST Failure indicator is
triggered if any of the process tests fail.
If the analyzer triggers the POST Failure indicator, reboot the Master Controller and watch the Local User Interface (LUI) display
screen for “Red” text. The “Red” text reveals the board subsystem having the initialization problem.
Indicator Boxes
Hex Codes
Setup Sub-Tab
Not all indicator boxes denote issues with the system, but they represent processes in action.
SI/PGC5000-EN, Rev B 11
SI/PGC5000-EN, Rev B 12
5.2 Power
If the Master Controller or Ovens do not power on, check for power related problems including external power, fusing, and
breaker boxes for possible issues.
LEDs
CLASS C OVEN
CLASS B OVEN
SI/PGC5000-EN, Rev B 13
If the LEDs are not illuminated, check power to the unit. If the top LED is GREEN and flashing, the system is initializing.
For all other instances use the table below.
Removal procedures: Place fingers or tool on both sides of the battery. Apply equal force to both sides and pull it away from
the SBC.
Installation Procedures: Locate battery connection base on the SBC. Ensure all four connection pins are straight and free of
contaminants. Align pins with base, push in firmly.
The displayed activity and error codes are used to troubleshoot or confirm the ongoing functions of the analyzer system.
Not all LEDs are assigned blinking response states. They are primarily used for debugging when no user interface is available.
Network
Activity
USB
Ports
Health
Monitor
The USB Port Activity light identifies activity on the Universal Serial Busses. One is used to connect to the front panel.
SI/PGC5000-EN, Rev B 14
The Health Monitor lights display the status of the system (see Figure 5.4).
CR30
CR25
CR29
U48 U50 CR27 U51 U53
CR31
CR24
CR26
SI/PGC5000-EN, Rev B 15
The Network Activity lights display network activity and configuration. The lights are viewed from top to bottom (see Figure
5.5).
CR2 10 Megabit
CR4 Link
CR5 Transmit
CR6 Receive
CR7 Collision
Upper right: Green – heartbeat that blinks being lit more than off at about once per second
Lower right: Green – blinks whenever a RTC signal is present; blinks faster when a method is active
Lower left: Amber – blinks slowly after power-up while the oven devices are being downloaded code
Upper left: Red – turns on when an error occurs; if heartbeat is blinking, then red indicates a loss of the life indicator
from the master controller; it will turn off if the Master Controller recovers.
Errors during startup will blink the lower left LED with a code that can be counted between pauses:
1 No initialized DPM
2 Unable to create virtual clock
3 Unable to create DPM exception handler
4 Unable to initialize RTC
5 Unable to create tasks
6 CAN comm error (not reliable)
7 Miscellaneous startup error
8 CAN asynchronous receive error
9 RTC asynchronous receive error
10 Error trying to start remote CAN node
11 Error during shutdown
When power is applied to the board, via the system power, the lower pair alternately blink for a few seconds indicating the
bootloader is functioning and loading the oven controller code from the master controller. If the bootloader fails, the two LEDs
will blink in unison five times and stop with an error code:
Off Green Invalid code size
Amber Off No code file
Amber Green No initialized DPM
Six small LEDs on the populated side of the Oven Controller PCB reflect CAN activity. CAN A refers to the oven fiber CANBus;
CAN B refers to the optional electrical CANBus; CAN C refers to the optional fiber CANBus. Under normal operation
SI/PGC5000-EN, Rev B 16
these LEDs blink green; they may appear solid during heavy traffic. If a CAN communication error is detected, an LED will turn
red.
CR2 CAN A transmit
CR4 CAN A receive
CR6 CAN B transmit
CR8 CAN B receive
CR11 CAN C transmit
CR13 CAN C receive
On the unpopulated side of the Oven Controller PCB), CR9 is a small green LED which when lit, means the OC is in a hold state.
The OC PCB comes up in this state. Once the Master Controller initializes the DPM between the two, the Master Controller will
release the OC PCB, at which time CR9 will go off.
CR3
CR2
On the Power-up Cycle, the four LEDs indicate the processes attempted if the DSP fails (none are blinking):
CR1 CR2 CR3 CR4
off red off off CAN initialization error
off amber off off application initialization error
red red off off CAN node/network setup error
green red off off no other node on CAN bus
amber red green off programming failed during last power-up
amber amber green off watchdog timeout during last power-up
red off green off power-up state chip inaccessible
red amber green off invalid power-up state
red amber off off reload in progress
off off green off start hardware setup
off green off off bootloader CAN setup
off off amber off DSP initialization
red amber red off EEPROM access error
off off red off bootloader initialization
off amber amber off CANopen setup
SI/PGC5000-EN, Rev B 17
CR3 is set red and CR4 is set amber upon receiving an NMT reset command from the OC. If the DSP can successfully reset, all
the LEDs will be turned off and then altered again during normal execution.
Specific CR4 functions: After the DTC becomes operational, unhandled interrupts might occur. These are reflected by a staying
solid red or blinking CR4.
A blinking red CR4 will blink for a count, pause, and then blink repeat the count again (continuously). Count the blinks between
pauses and determine the cause using the following list:
Blinks Source
1 (unused)
2 (rfu)
3 non-maskable
4 illegal operation
5 data logger
6 RTOS
7 Emulation
8 CPU timer 1
9 CPU timer 2
When a solid re CR4 occurs, the status of CR1 through 3 identify the interrupt source:
CR1 CR2 CR3 CR4 Source
off off amber red INT1.x
off amber off red INT2.x
off amber amber red INT3.x
amber off off red INT4.x
amber off amber red INT5.x
amber amber off red INT6.x
amber amber amber red INT7.x
off off red red (rfu)
off red off red (rfu)
off red red red reprogram flash memory
red off off red erase flash memory
red off red red user trap
red red off red test
red red red red misc. disabled source
green green red red SCI-A RX
green red green red SCI-A TX
green red red red SCI-B RX
red green green red SCI-B TX
red green red red eCAN 0
red red green red eCAN 1
SI/PGC5000-EN, Rev B 18
If the Digital Signal Processor (DSP) system fails during power-up, the LED bank indicates what was being attempted. No green
LEDs (CR1 to CR6) are blinking and CR7 and CR8 are off. CR1 (MSB) through CR6 form a binary code as follows:
000001 CAN initialization error
000010 application initialization error
000011 CAN node/network setup error
000100 no other node on CANBus, still trying
000101 CAN and application timer engaged
000110 reload in progress
000111 CAN disabled, reload jumping to start over
001000 bootloader initialization
001001 bootloader CAN setup
001010 bootloader start hardware setup
001011 bootloader end hardware setup
001100 bootloader received reset application
100001 bootloader flash erase in progress
110011 bootloader flash program in progress
111111 bootloader flash program complete
001110 start board setup
001111 start DSP initialization
010000 end DSP initialization
010001 Analog/Digital initialization
010010 temperature zone setup
010011 temperature conversion setup
010100 number valves detection
010101 end board setup
010111 start DTC initialization
011000 valve initialization
011001 safety switch initialization
011010 PIC initialization
011011 signal testing initialization
011100 purge testing initialization
011101 miscellaneous initialization
011110 end DTC initialization
100000 start setup CANopen
100001 CAN PDO setup
100010 end setup CANopen
100100 solenoid start initialization
100101 solenoid access
100110 solenoid test
100111 solenoid reverse test
101000 solenoid test complete
101001 solenoid end initialization
101111 received reset application
SI/PGC5000-EN, Rev B 19
If CR7 remains solid red and CR8 is OFF, an unexpected fatal condition occurred. CR1 (MSB) through CR6 form a binary code as
follows indicating the error:
000001 flash erase error
000010 flash write error
000011 powerfail interrupt
001000 no viable CANbus detected after 10 tries
001001 no auxiliary board detected
If CR7 and CR8 stay solid red (after the Digital Temperature Controller is operational) an unhandled interrupt has occurred. CR1
(MSB) through CR6 form a binary code indicating the error as follows:
000001 INT1.x
000010 INT2.x
000011 INT3.x
000100 INT4.x
000101 INT5.x
000110 INT6.x
000111 SCI-A RX
001000 SCI-A TX
001001 SCI-B RX
001010 SCI-B TX
001011 eCAN 0
001100 eCAN 1
001101 user trap
001110 PIE_RESERVED
001111 rsvd_ISR
010000 CPU timer 1
010001 CPU timer 2
010010 data logger
010011 RTOS
010100 emulation
010101 non-maskable
010110 illegal operation
Other LEDs also indicate various procedures, as noted on the previous figure, occurring via the board and are noted below:
CR10: Green. Blinking CANBus active.
CR12: Green, Blinking CANBus active.
CR13: Red, blinking Power to zone 2 heater.
CR14: Red, blinking Power being applied to zone 3 heater.
CR15: Red, blinking Power being applied to zone 4 heater.
CR16: Red, blinking Power being applied to zone 5 heater.
CR17: Red, blinking Power being applied to zone 1 heater.
CR18: Red PIC has enabled the main heater switch.
CR20: Green DSP power voltages good
Red DSP Power issue
SI/PGC5000-EN, Rev B 20
Some Status Scopes have multiple sub-scopes to choose from or may require using the ‘Page Down’ icon
to view all indicators.
If not assigned to a scope, a “Triggered” Indicator on the Status Tab, (displaying red, yellow or blue) is not
reflected at the Status Indicator. It maintains a green (good) status.
If the triggering condition still exists, the indicator will re-trigger after pressing the reset button.
SI/PGC5000-EN, Rev B 21
Column Description
Indicator: “Name” listed on Status Tab screen
Issue: Possible problem triggering indicator
Reset: Displays the means of reset. The ‘Absence of Condition’ (AOC) is the most common. If an indicator is
marked HOLD, the AOC becomes manual reset.
Source: “Group,” listed on Status Tab screen, is the most likely origin of the triggering condition.
SI/PGC5000-EN, Rev B 22
Out of Control Temperature deviates > Check analysis temperature control AOC Oven.DTC#.Tz.#
±10° from setpoint TCF settings. Check zone indicators
and Diagnostic Displays.
Ramp Out of Temperature deviates > Check analysis temperature control AOC Oven.DTC#.Tz.#
Control ±10° from setpoint during TCF settings. Check zone indicators
Temperature Ramp and Diagnostic Displays.
DTC Digital Input 1 Low oven purge air pressure. Check purge pressure settings at AOC Oven#DTC#.1
Open on alarm. oven’s front panel gauge. Adjust as
necessary. Check instrument air
supply pressure. Check oven gauge
pressure switch.
DTC Digital Input 2 Differential Pressure Check purge pressure settings at AOC Oven#DTC#.2
Sensor oven’s front panel gauge. Adjust as
necessary. Check instrument air
supply pressure. Check oven gauge
pressure switch. Ensure all oven
doors are closed and secure.
DTC Digital Input 3 Temperature Programmed Check purge pressure setting at AOC Oven#DTC#.3
Oven Purge Air Pressure oven’s front panel gauge. Adjust as
necessary. Check instrument air
supply pressure. Ceck oven purge
pressure switch.
DTC Digital Input Optional hardware inputs. Verify input is functioning AOC Oven#DTC#.4-14
4-14 Open on alarm or action properly.
request input.
SI/PGC5000-EN, Rev B 23
SI/PGC5000-EN, Rev B 24
SI/PGC5000-EN, Rev B 25
SI/PGC5000-EN, Rev B 26
“#” is used in place of numbers to eliminate repeats in multiple card and oven systems. "Information
Only" signifies the set indicator is activated in response to the setup criteria. It does not necessarily
identify a fault.
Cause: Baseline or detector noise can result from contaminated carrier, makeup gas, tubing or regulators. This type of
contamination is much less pronounced with a TCD than for an FID. Other causes include defective filaments (TCD), detector
wiring, or electrical noise in the detector electronics or power supplies.
Check the background level by going to the Setup Tab>FID button and with the flame lit manually, AUTO ZERO the baseline.
(The AUTO ZERO OFFSET for an FID should be > 10 mv.)
Causes:
1. Incorrect temperatures. Inspect temperature settings and correct if necessary.
SI/PGC5000-EN, Rev B 27
2. Contaminated or missing carrier gas, hydrogen fuel or burner air. Verify the supplied cylinders are analytical grade.
Replace cylinders one at a time; activate the pressure zones and relight the flame. Observe the baseline to isolate possible
contaminated cylinder. Replace cylinder as necessary.
3. Contaminated tubing (normally a startup issue). Locate supply cylinders as close as possible to the analyzer. Connect
them using a clean piece of tubing. Activate the pressure zones and relight the flame. Observe the baseline to isolate
possible contaminated tubing. Replace tubing as necessary.
4. Leaks. Pressure test supply lines from the source to the analyzer and pressure test the analyzer. Correct leaks as
necessary. Activate the pressure zones and relight the flame. Observe the baseline on the Manual Mode tab to verify
noise issue has been resolved.
5. Contaminated FID assembly. The FID may become contaminated due to flooding columns with liquid hydrocarbons or
running analyses with the flame out for long periods of time.
6. FID electrical failure. Disconnect the coaxial cable at the FID Amplifier assembly. Observe the baseline on the Manual
Mode tab. If baseline noise is not present, replace the coaxial cable. If it is still present reconnect the coaxial cable.
Replace the FID Amplifier assembly.
7. TCD detector balance. If the detector is not balanced between the reference and measurement filaments, balance is
needed.
8. TCD filament failure. Replace the filaments.
9. FPD baseline characterized by random noise and/or spikes. FPD noise is generally the result of electrical noise or
contamination.
5.6.3 No peaks
This generally indicates that either no sample was injected, or the injected sample is not being detected or processed.
Cause: Worn liquid sample valve. Service the liquid sample valve.
Cause: If only present on calibration sample and not on process, verify that the correct calibration and proto fuel samples are
being analyzed. Possibly a new calibration blend has been installed that contains a blending error. Perhaps the wrong
calibration sample has been selected or incorrect analysis is attached to it.
If mystery peaks are present on all process or calibration samples, the analyzer is experiencing a sampling problem. The sample
valve seals may be leaking. The sample valve may be double sampling (see "Double Sampling"). The sample stem may be
scratched or deformed. Peaks may also be originating from a previous analysis cycle.
SI/PGC5000-EN, Rev B 28
The gating in the method needs to be modified to ensure gating of the missing peak in the report. This can be done by
modifying the gate ON/OFF time in the method table.
Causes;
1. Wrong carrier gas. Verify the correct carrier gas is being used.
2. Splitter out of adjustment (liquid sample). Adjust splitter (if installed) per factory data sheet as necessary.
3. Sample size too large (vapor sample). Manually verify block and bleed valves are functioning, if applicable; correct as
necessary. Verify the analyzer’s sample vent is not restricted. Verify sample flow into analyzer is correct.
Causes:
1. Fluctuating sample size (liquid sample): Verify sample flow to analyzer. Verify sample is single phase. Verify splitter vent
is unrestricted.
2. Fluctuating sample size (vapor sample): Verify block and bleed valve vent is unrestricted, if applicable. Verify sample vent
pressure is not fluctuating. Verify sample flow to analyzer is not fluctuating. Verify sample flow to analyzer is correctly set
to 100 ml maximum. Possible leak in sample inject valve.
Causes:
1. Varying Carrier flow rate. Verify instrument air is per specification. Check oven indicators for more details. Monitor oven
purge pressure. Possible defective air purge regulator.
2. Varying oven temperature. Verify instrument air is per specification. Check oven indicators for more details. Monitor
oven purge pressure. Possible defective air purge regulator
3. Leak in column train. Leak check analyzer.
4. Contact the ABB factory for assistance in testing the functionality of the EPC Proportional Valves as well as Pressure
Sensors in the EPC block.
Causes:
1. Wrong carrier gas. Verify the correct carrier gas is being used.
2. Excessive sample splitting (liquid sample). Verify splitter vent flow is per factory data sheet.
3. Sample size too small. Residue in the LSV stem’s sample groove (liquid sample); service LSV. Verify sample flow to
analyzer coating on walls of the sample loop (vapor sample); clean or replace sample loop.
4. Detector gain (TCD only). Check detector gain jumper and adjust if necessary. Replacement TCD may not be correctly
jumpered. Compare jumpers to original TCD and correct as necessary.
5. Check that there are no leaks present on the valves and all make/break connections.
6. Inspect CP Valve sliders (if installed) for scratches and grooves.
Causes:
1. Air supply shut off.
2. Purged areas have leaks. Leak check with leak detector.
3. Purge air switches are defective. Replace purge switches.
SI/PGC5000-EN, Rev B 29
Causes:
1. Insufficient burner fuel and/or air. Check flows.
2. Plugged vent line. Check cell vent for restriction. Possible plugged breather assembly.
3. Defective igniter.
a. Measure resistance of the igniter at TB16 pins 3 and 4; it should be less than one ohm. Replace as necessary.
b. Measure voltage at TB16 pins 3 and 4 with igniter turned on; 2.0 VAC indicates an open igniter, 1.5 to 1.6 VAC
indicates a good igniter.
c. 0 VAC indicates an electrometer problem or the electrometer is not receiving the ignite signal from the A/D board.
4. Incorrect flame out indication. Measure thermocouple voltage at TB16 pins 1 and 2 on the electrometer PCB. With the
flame lit the reading should be greater than 2.5 mv.
a. If the voltage is greater than 2.5 mv the electrometer is defective.
b. If the voltage is less than 2.5 mv check flows and correct as necessary.
c. Inspect thermocouple for damage and replace as necessary.
d. Inspect jet tip for corrosion and restriction, and replace as necessary.
5.7 Software
A software repair can be as simple as restarting the system or may require performing a System Recovery from files created and
saved on a USB flash drive. In the unlikely event a system recovery is needed, it is easy to do so using a recovery image created
from the Local User Interface using the Setup Tab. The USB flash drive created contains a System Recovery image including all
the software files originally installed on your analyzer at the factory and changes made prior to the last backup.
It is important that you perform the system restore in the order described in this document.
Before starting any maintenance it is recommended that you create a restore point in the system local memory using the USER
Action icon as a precautionary measure.
SI/PGC5000-EN, Rev B 30
If only option names show, you do not have enough rights to use the backup and restore options.
Stop all schedules before creating a recovery USB or backing up the stream files to a USB flash drive.
ACCESS CONTROL LIST – Selecting the Access Control List (ACL) icon displays a dialog box containing a list of users, passwords,
and access levels that is distributed, encrypted and persisted at each device. The ACL can be modified from a PGC5000
(LUI or Remote Client), VNSA, or a STAR Client. If the analyzer is secured, any user with supervisory rights can modify the
ACL. If the PGC5000 is unsecured, everyone has the ability to modify the ACL.
Stop all schedules before restoring from a recovery USB flash drive.
FACTORY – Selecting the Restore Settings icon restores the analyzer to the factory configuration. AllL user configuration
changes to the system will be lost.
USER – Selecting the Save icon creates a User Restore point. The system copies all configuration files from the working
directory to the Restore directory on the analyzer. You should create a restore point prior to making any changes or
updates to the analyzer.
Selecting the Restore Settings icon restores the system to the user created restore point. It copies the configuration files
from the Restore directory to the Working directory of the Master Controller and restarts the system.
Creating the recovery drive takes several minutes. Wait for the “Operation Completed” message before
ejecting and removing the USB thumb drive. Remove and store the Recovery drive in a safe place.
You must use a USB drive having 32 gb or less. If you use a USB drive larger than 32 gb, the system will
appear to write the data to the drive and give a “Creation Complete” message, but no data will be on the
drive.
RECOVERY – Selecting the USB Flash Drive Operation icon creates a recovery drive on the USB flash drive inserted in the Master
Controller Single Board Computer. This operation takes up to thirty minutes to complete depending on system
configuration. The user restore director is NOT saved to the Recovery drive.
To restore the system from an unrecoverable lockup or after replacing the Single Board Computer, install the USB flash
drive and apply power to the system. The Master controller formats the flash memory and copies all of the files from the
USB flash drive to the system’s flash memory. Wait for the Upgrade Complete message to appear. Select the USB Eject
icon and wait for the Eject Complete message to appear. Remove the USB drive and cycle power on the Master Controller
to reboot.
STREAM FILE – Selecting the USB Flash Drive Operation icon copies all stored chromatogram files on the system to the flash
drive inserted in the Master Controller SBC board. Copying the data files will take several minutes. Wait for the Operation
Complete message to appear. Select the USB Eject icon and wait for the Eject Complete message to appear and then
remove the USB flash drive.
Selecting the Delete Icon deletes all saved chromatograms and report files on the system. It does not delete analyses
saved in the Analysis Config folder or Analysis Library folder.
DIAGNOSTICS – Selecting the USB Flash Drive Operation icon will copy all diagnostic files to a USB drive inserted in the Master
Controller SBC board. Diagnostic files are used to diagnose errors and events in software. These files are for factory use
and troubleshooting purposes. The copying of the files should take only a few minutes. Wait for the Operation Complete
SI/PGC5000-EN, Rev B 31
message to appear. Select the USB Eject icon and wait for the Eject Complete message to appear and then remove the
USB flash drive.
EJECT – Selecting the USB Flash Drive or the SD Card icon allows you to safely eject the USB Flash Drive or SD Card from the
Single Board Computer PCB in the Master Controller. Wait for the Eject Complete message before removing the USB Flash
Drive or SD Card. Report storage will automatically revert to RAM disk when the SD Card is not present.
The following popup messages may display during restore and recovery operations.
Stream Data Files No USB Drive Found No USB flash drive found. Insert USB flash drive in
Master Controller Board.
USB Recovery Drive Creation Complete Recovery data has been saved to the USB flash
drive.
USB Recovery Drive No USB Drive Found No USB flash drive found. Insert USB flash drive in
Master Controller Board.
User Configuration Restore No Restore Point No Restore point files found. Restore has not
Found been created.
When the Master Controller’s power is cycled, it forces the analyzer to clear and reload the configuration files into Random
Access Memory (RAM), allowing the system to reinitialize all attached ovens and connected equipment.
SI/PGC5000-EN, Rev B 32
This procedure describes general troubleshooting procedures, issues and resolutions for the optional Discharge Ionization
Detector.
Verify that:
• System has power.
• All switches and gas settings are at the correct positions.
• Column has proper flow rates and pressures.
• Plasma shield is in place on the reactor.
• Plasma center rod is grounded to the oven chassis.
• Bias tube is connected to a bias voltage source.
Identify whether the problem is with the oven or the detector. In general, if the problem is with retention times but not
sensitivity, look for problems with the oven, especially the valves or column connections.
Next determine the last thing done to the system. In general, this is the best place to begin the troubleshooting process.
If these steps identify that the problem is with the detector, use the following subsections to identify and correct the problem.
Air in plasma: The presence of too much air in the plasma will often cause the plasma not to light. Allow the system to purge
with the reaction gas for at least 15 minutes. If the plasma still will not initiate, check for air leaks in all of the fittings.
Back pressure too high: If a restriction in the exhaust line is too high, the detector plasma will not light. Replace the
exhaust/signal tube with a new one and see if the plasma will light.
Wrong plasma gas: If there is another gas besides helium or argon, the plasma will not light.
5.10.2 No signal
No power to plasma power supply: If the fuse is good, contact ABB customer support for further assistance.
Verify power to plasma: Observe the plasma tube with the lights off. There should be a pink or almost white glow in the
plasma tube. If the tube is very blue and the signal is low, there is nitrogen in the plasma. This may be because the wrong
SI/PGC5000-EN, Rev B 33
reaction gas is connected, there is an air leak, or there is no reaction gas flow. Turn off the power to the plasma and check
the gas supply. Check for leaks and check flow rate.
Signal cable problem: Verify that the collector shield BNC fitting contacts the exhaust tube.
Verify bias voltage: Using a VOM, measure the voltage at the bias rod. The voltage should be 110 volts between the rod and
the oven chassis.
Low or no bias voltage: Verify the connection of bias voltage to the bias voltage rod. If necessary, verify that bias voltage is
present on the bias voltage rod by connecting a volt-ohm-milliammeter to the bias rod (red lead) and ground (black lead).
The voltage should be at least 110 volts.
Leakage in the chromatographic system: Verify the retention times for the components of interest. If these are correct, check
for leakage on all the fittings on the detector end of the system. If the retention times have shifted, look for leaks on the
valve rod.
Wrong reaction gas: Using nitrogen as the reaction gas will cause low signal. Verify that the proper reaction gas is being used.
Improper restrictor in place: Too large of a restrictor results in poor plasma performance, leading to low sensitivity. Verify that
the proper restrictor is in place, or replace the restrictor with one of know proper dimensions.
High response and shifted retention times: This is a problem that may be caused by a restriction in the exhaust tube. In this
case, the retention times for the analyses will have shifted later in the chromatogram.
1. Visually inspect the exhaust tube to identify any materials that may be plugging the tube.
2. Insert a syringe cleaning wire into the exhaust tube.
If these actions do not resolve the problem, replace the exhaust tube with a new one.
5.10.4 Noisy
Bad electrical connections: Check the signal cable connection and the bias voltage cable connection. Check the signal cable
shield for fit. This fitting should be snug for best performance. Verify the connection between ground and ground.
Leak: Especially true when operating in the helium ionization detection (HID) mode. If the detector is being very noisy, check
all fittings within the oven system for leaks. Verify the installation of or replace the PTFE noise shield in the top nut.
Plasma electrode too close to Swagelok fitting: The plasma O-ring on the plasma tube is meant to prevent this issue. If this
appears to be the case:
SI/PGC5000-EN, Rev B 34
Air leak: If there is an air leak in the system before the detector, the presence of oxygen and nitrogen will cause a high baseline
and a noisy signal. Generally, an air leak at the detector will cause a low signal (due to the presence of nitrogen in the
plasma) rather than a high signal. If a high signal is encountered and a leak is suspected, verify the fittings before the
detector (i.e., the injector and the injector gas supply lines).
Column bleed: If the system is running isothermally, the changing baseline may be due to column bleed. This is especially
problematic when using packed columns. Verify that the system is leak free. Ensure that there is on oxygen in the
system. Re-condition, rinse, or replace the column.
Plasma cell leak: If the base of the plasma cell is not well sealed, it is possible to see a rise in the baseline. Initially this may
appear as column bleed, but the signal will settle down once the oven returns to an isothermal mode. Reset the plasma
cell in the Swagelok fitting and tighten to make it leak free.
Contamination or late-eluting components: Alter the cycle time of injections to determine if the drifting baseline changes
location. If it does, it is possible that there is a late eluting component or contamination that is coming off the column
several runs later. If this is the case:
5.10.7 Spikes
Loose connections: Verify the signal cable is securely attached to the electrometer and to the BNC fitting on the collector
shield. Verify that the signal spring contacts the exhaust tube.
Missing ground leads: Verify that the ground lead from the plasma center electrode is connected. If not, turn off the power to
the plasma and re-connect the center electrode ground lead. Verify that the main power supply ground lead is connected
to an appropriate oven chassis ground point.
Defective bias voltage: If the bias voltage is not stable, it is possible to get signal spikes. Verify the bias voltage and stability
using a VOM connected between the bias voltage rod and the oven chassis ground.
SI/PGC5000-EN, Rev B 35
6 Component repair
6.1 General
Ensure no hazardous or flammable gases are present in the immediate area of the analyzer, as they may
create the potential for fire, explosion, and damage to property and injury to personnel.
Equipment:
• Leak testing solution
• Flow Meter
• Grounding strap or equivalent
SI/PGC5000-EN, rev B 36
The Master Controller also has the network interface connections, which are located at the back of the Card Cage, on the top
right.
The following subsections give specification and removal procedures for components installed in the Master Controller.
System Board Battery: This is a small rectangular boxed object (“Snap Hat”) located in the middle of the SBC. While it isthe
unlikely the battery will fail, it can be replaced.
• Failure symptoms: System Clock resets when system is powered off.
• Removal procedures: Place fingers or tool on both sides of the battery. Apply equal force to both sides and pull away
from the SBC.
• Installation Procedures: Locate battery connection base on the SBC. Ensure all four connection pins are straight and
free of contaminants. Align pins with base, push in firmly.
SI/PGC5000-EN, rev B 37
If equipped with a Wago module, ensure electrical CAN connection is removed from the top of the
controller board before sliding board out.
Touch Panel
Controller
SI/PGC5000-EN, rev B 38
Transformers for the backlight converter are protected on this. Be careful when opening and closing the
Master Controller door to ensure safety.
Removal and replacement procedure for the PCB assembly (see Figure 6.3).
1. Remove power from unit and follow plant documentation procedures.
2. Label all cables attached to PCB assembly (noting position and orientation).
The upper power cables are secured with cable ties and must be cut. Be extremely careful when
removing the ribbon cable as the pins can be easily bent.
The upper power cables are secured with cable ties and must be cut. Be extremely careful when
removing the ribbon cable as the pins can be easily bent.
3. Remove the cables from the right side of the PCB assembly.
4. Remove and set aside the four hex nuts holding the panel to the front screen board clips at top and bottom.
5. Slide the board over the studs.
6. Reverse steps to replace the LCD Panel.
SI/PGC5000-EN, rev B 39
EPC Control
PCB
Power
Supply
Detector
Amplifier
Assy
DTC Digital
EPC Analog PCB
PCB Assy
EPC Control
PCB
Power
Supply
DTC
Detector
Auxiliary
Amplifier
PCB
Assembly
DTC Digital
PCB Assy
DTC Analog
PCB Assy
SI/PGC5000-EN, rev B 40
DTC
Control
PCB
Detector
Amplifier
PCBs
DTC DTC
Digital Analog
PCB PCB
Power
Supply
Always note routing and marking of cables (pin 1 location, etc.). Note jumpers and move to replacement
board as necessary.
To ensure integrity of the components within the EPC, use the tools in EP Service Took Kit 801K005-1
when disassembling or assembling the EPC Control Assembly.
6.6.1 Preparation
Before performing EPC repair, you must turn off power to the analyzer as described in the following
steps.
SI/PGC5000-EN, rev B 41
Be sure that the EPC Control Assembly has cooled to ambient temperature (approximately one hour)
before proceeding.
Use an ESD wrist strap and proper grounding procedures before handling any components in the EPC
Control Assembly.
This procedure is not required if you are only replacing EPC components.
SI/PGC5000-EN, rev B 42
10. On the wall inside the left side of the oven, remove the lock nut on the pipe nipple which retains the EPC Panel cables (see
Figure 6.7, which shows Class C oven).
Lock
Nut
SI/PGC5000-EN, rev B 43
Proportional
Valve
Sensor PCB
Heater
Control PCB
Heater Cable
AC Power Cable from
Backplane PCB J44
Valve Cable, Zone 1
Sensor PCB Cable, Valve Cable, Zone 2
Zone 1
Valve Cable, Zone 3
Sensor PCB Cable, Valve Cable, Zone 4
Zone 2
Valve Cable, Zone 5
Sensor PCB Cable,
Zone 3
If more than one zone is being replaced, they must be replaced starting with the highest numbered zone
(right side) and proceeding to the lowest numbered zone (left side).
SI/PGC5000-EN, rev B 44
RETAINER
WASHER
SCREW
SCREW
WASHER
SENSOR PCB
GASKET
1. Place a Belleville washer on each mounting screw, with the rounded side toward the screw.
2. Place the screws through the holes in the mounting plate.
3. Place the gasket on the end of the two screws, with enough screw thread showing through the gasket to start the screws
into the hole.
4. Insert the screws into the hole in the block, just far enough to hold them in place.
5. Place the Sensor PCB into position between the plate and the gasket, with the cable at the bottom right edge.
6. Slightly tighten the two screws evenly, removing any play in the assembly (but applying no torque) and ensuring it is
mounted straight up and down.
7. Tighten one screw, using torque limiting screwdriver ABB Tool 801Z003-1, set at 1 in.-oz.
8. Tighten the second screw to 2 in.-oz.
9. Retighten the first screw to 3 in.-oz.
10. Retighten the second screw to 4 in.-oz.
11. Retighten the first screw to 5 in.-oz.
12. Retighten the second screw to 6 in.-oz.
13. Retighten the first screw to 7 in.-oz.
14. Retighten the second screw to 7 in.-oz.
15. Plug the Sensor PCB cable into the corresponding connector on the Control PCB.
16. If another Sensor PCB Assembly needs to be replaced, repeat the appropriate steps to remove the old Sensor PCB
Assembly and install a new one. Be careful to observe the precautions stated in the Note at the beginning of this
procedure.
17. Reconnect the large ribbon cable to the Control PCB.
18. Ensure that the flame-proof or explosion-proof surfaces of the cover or the body of the Control Assembly are not
damaged.
19. Reinstall the EPC Control Assembly cover and insert the ten screws and tighten them to 16 in.-lb, using ABB Tool
TL1000/TL1002.
20. Reinstall the EPC cover panel and insert the four screws.
SI/PGC5000-EN, rev B 45
You may need to remove the Sensor PCB cable from the Control PCB to allow access to the connector of
some zones.
7. Using 3 mm hex socket wrench ABB Tool TL1009, remove the screws and washers that secure the valve in place.
8. Firmly grasp the valve and remove it from the enclosure.
SI/PGC5000-EN, rev B 46
Be sure that the EPC Control Assembly has cooled to ambient temperature (approximately one hour)
before proceeding.
Use an ESD Wrist strap and proper grounding procedures before handling any components in the EPC
Control Assembly.
SI/PGC5000-EN, rev B 47
SI/PGC5000-EN, rev B 48
SI/PGC5000-EN, rev B 49
SI/PGC5000-EN, rev B 50
SI/PGC5000-EN, rev B 51
7 Subassembly repair
7.1 Column repair
Mark capillary columns with white-out at the back of the tubing nut before removing to insure correct
insertion depth of replacement column.
8. To remove the column, loosen the fittings on both ends of the column and gently extract the column from the respective
fitting connections.
9. Loosen any screw securing the column to the column mounting brackets and remove the column.
1. Insert the end of the column through the back of the tubing nut.
2. Insert the column through the new ferrule.
3. Slide the ferrule down the length of the column (approximately three inches).
4. Cut the column as described in "Cutting Capillary Columns."
5. Connect the column and finger-tighten; then tighten and additional ¼- turn with an open-end wrench.
6. Test the column for a secure connection by gently pulling the column at the 1/8-inch tubing nut. Correct any withdraw.
Continue tightening the nut until the column is secure at the fitting.
7. Repeat steps 1 through 6 for the other end of the column.
8. For columns connected to an FID:
a. Insert the column end into the FID analysis inlet connection until it stops against the jet.
b. Withdraw the column approximately 1/16-inch and tighten the nut finger-tight. Tighten the nut an additional 1/4-turn
with an open-end wrench.
c. Check it for a secure fit.
If a metal capillary column is used, particular care should be taken to ensure that the column does not
contact the jet. The metal column will conduct electricity and could cause an electrical short at the jet.
SI/PGC5000-EN, Rev B 52
Do not use high speed cutting wheels or grinders to cut capillary columns. This type of cutting generates
heat that can damage the column and the resultant column cuttings could plug the column.
1. Use a diamond or ceramic scoring tool to score the surface of the outside tubing wall approximately one inch from the end
of the column. Take care not to cut through the tubing wall.
2. Wipe the scored area clean to prevent material from entering the column.
3. Secure the column with your fingers 1/2-inch on each side of the score and gently bend the tubing at the score, in the
direction opposite the score.
4. When the score point opens, bend the tubing back towards the score. The tubing should make a clean break.
5. Inspect the end of the column for roundness and ensure it is burr free. If the end is not round and burr free, repeat the
procedure until it is.
6. The column is now ready for installation.
Breather Microdot
Adapter Connector
Thermocouple
Polarizer
Ignitor
Jet
This repair should only be attempted by people who are properly trained and possess the expertise for
this repair.
Before disposing of any residual insulating materials, ensure that disposal methods comply with all
applicable regulatory restrictions.
It is the customer’s responsibility to ensure that the area is safe and hazard free, and will remain so the
entire time the analyzer is open. This responsibility includes ensuring adequate ventilation in analyzer
shelter and obtaining proper work permits, etc.
The thermocouple, polarizer and igniter assembly elements are fragile and can be easily damaged if not
handled with extreme care. Do not touch the end of the elements.
SI/PGC5000-EN, Rev B 53
SI/PGC5000-EN, Rev B 54
7. Roll each end of the green wire of the new polarizer between your forefinger and thumb, causing the wire ends to be
tightly spiral wrapped.
8. Using the 40 watt soldering iron and approved high temperature solder, “tin” the wire ends.
9. Spread or expand the end of approved heat shrink to allow easy installation over the solder connection.
10. Install heat shrink over each wire and slide it as far as possible from the connection. This will prevent premature shrinking
when the connection is soldered.
11. Overlap and solder the “tinned” ends of the green wire from the wiring harness and the green polarizer assembly wire
using approved high temperature solder and 40 watt soldering iron.
12. Apply a short wrap of glass tape over the connection.
13. Slide the heat shrink over the taped connection and shrink it with a heat gun.
SI/PGC5000-EN, Rev B 55
This procedure requires a special tool, Insertion Tool ABB P/N TL799M013-1, to assist in passing the cable
through the insulation between the Electronic Housing and the Oven.
1. Cut the cable just below where it passes through the Oven into the Electronics Housing and remove the cable from the
Oven.
2. Disconnect the other end of the cable from the FID Amplifier Assembly and remove the cable from the Electronics
Housing.
3. Remove the grommets from the grommet holes (located in the side of the Electronics Housing and the side of the Oven)
that will accommodate the routing of the new cable.
4. The new FID Cable Assembly has a Microdot connector on one and a BNC connector on the other end (see Figure 7.2).
Screw the Microdot connector end of the new cable assembly into the Insertion Tool.
Microdot BNC
Connector Connector
5. Pass the Insertion Tool through the grommet holes from the Electronics Housing to the Oven.
6. Remove the Insertion Tool from the cable connector.
7. Make a slit in each grommet from the outer diameter to the inner hole. (This is necessary because the cable connector will
not pass through the grommet.)
8. Position the cable in the grommets in the Electronics Housing and the Oven.
9. Push the grommets into the grommet holes.
10. Connect the cable connectors to their respective locations (BNC connector to the FID Amplifier Assembly and Microdot
connector to the top of the detector).
Reference Measure
Filament Filament
SI/PGC5000-EN, Rev B 56
It is the customer’s responsibility to ensure that the area is safe and hazard free, and will remain so the
entire time the analyzer is open. This responsibility includes ensuring adequate ventilation in analyzer
shelter and obtaining proper work permits, etc.
Replacement filament installation kits are supplied with two cable glands, a wire spreader, 736 RTV, high
temperature solder, and heat shrink.
1. Cut the four filament wires approximately the same length as the wires on the filaments that were removed.
2. Insert one pair of filament wires through the threaded end of the gland nut, then carefully insert the filament into the
detector cell cavity marked “M” (measurement). Position the filament with filament wire in the direction of the flow.
3. Slide the nut down the length of the wires to insert and align it with the measurement cavity.
4. Tighten the cable gland finger tight, and then finish tightening with a 3/8-inch open-end wrench.
5. Insert the second pair of filament wires through the threaded end of the gland nut, then carefully insert the filament into
the detector cell cavity marked “R” (reference). Position the filament with filament wire in the direction of the flow.
6. Slide the nut down the length of the wires to insert and align it with the reference cavity.
7. Tighten the cable gland finger tight, and then finish tightening with a 3/8-inch open-end wrench.
8. Using wire strippers, remove approximately 1/4 inch of insulation from the end of each detector filament wire.
SI/PGC5000-EN, Rev B 57
6. Repeat this measurement for each of the other three filament wires. If all resistance measurements are correct, go to
"Connecting the Filaments." If any resistance is too low, go to step 8.
7. If the resistance measurement is approximately 20 ohms, filament being tested is contacting the internal wall of the
detector cell cavity. When this occurs, carefully loosen the gland of the suspect filament. Continue to loosen by hand and
withdraw first the gland, then the filament from the detector cell body (taking care not to touch or damage the filament).
8. Inspect the filament for damage or bending. If it is damaged, the filament pair will have to be replaced.
9. If the filament is slightly bent, use small needle nose pliers to gently and carefully bend it straight.
10. If the filament orientation now appears to be correct, reinstall the detector filament and repeat the complete checkout. If
it fails again, replace the detector filament pair and repeat the checkout.
11. If the filament is damaged during this attempted correction process, the filament pair will have to be replaced.
SI/PGC5000-EN, Rev B 58
This repair should only be attempted by people who are properly trained and possess the expertise for
this repair.
Filament Replacement Kit 865K001-1 includes a set of four filaments, four gland nuts, and a wire splice
kit.
1. Carefully install the new filaments and gland nuts; being careful to not damage the filament.
2. Install the filaments so they are facing in the direction of flow into the detector housing.
Not following the torque pattern described in the next step can result in permanent damage to the
detector block.
3. Using a 11/32 deep well socket torque each gland nut individually in a clockwise pattern in 10 IN/LB increments, until 90
in./lbs is reached on all nuts.
4. Install a one inch piece of PTFE sleeving onto each filament lead and trim leads to ¼ inch above sleeving
5. Measure the resistance of all filaments. They should be 40-42 ohms at room temperature. All filaments should be within
one ohm of each other.
6. Verify the filaments are not in contact with the detector housing. Measure the resistance from one filament lead to the
block. It should read infinity. Repeat for all filaments.
7. Leak check the filaments
8. Cap the TCD cell vents
9. Ensure the wires removed from the filaments are not in contact with the detector block or each other or remove the AC
power connectors at the bridge amplifiers.
10. Turn on carrier gas and utilities.
11. Restore power to the oven.
12. Set carrier pressures as per the data sheet.
13. Wait five to ten minutes for the pressures to equilibrate in the analyzer.
14. Check for leaks around the filaments.
SI/PGC5000-EN, Rev B 59
ABB recommends using an alcohol such as Methanol to check for leaks as it dries quickly and leaves no
residue.
22. Route wires as shown in Figure 7.5 and solder to filament leads using a 40 watt soldering iron.
23. Cover each solder connection with ½ inch of clear shrink sleeving and shrink with a heat gun. Pinch the open end of the
sleeving together while still hot, to close the end of the sleeving.
24. Install o-ring as necessary into o-ring groove of cell body.
25. Re-install cover and screws removed in step 7.4.1.
26. Torque screws to 16 in./lbs.
27. Reposition detector and tighten the three brackets in the electronics housing to secure.
SI/PGC5000-EN, Rev B 60
It is the customer’s responsibility to ensure that the area is safe and hazard free, and will remain so the
entire time the analyzer is open. This responsibility includes ensuring adequate ventilation in analyzer
shelter and obtaining proper work permits, etc.
Do not remove the light pipe from the photomultiplier assembly as this will exhaust the purge gas which
is necessary for proper operation.
1. Turn off oven air to the isothermal oven; de-activate all heated zones under the set-up tab and allow all temperature
zones to cool.
2. Remove oven power.
3. Open the door on the left side of the analyzer.
4. Disconnect the cables to the Photomultiplier Assembly and set them aside.
5. Remove the four screws securing the Photomultiplier Assembly to the analyzer, being careful to retain the screws to
reinstall the Photomultiplier Assembly.
6. Carefully pull the Photomultiplier Assembly straight out of the analyzer.
7. Reinstall the Photomultiplier Assembly in reverse order of removing it.
Burner Block
SI/PGC5000-EN, Rev B 61
O-Ring
45051-4-106
O-Ring
45051-4-102
O-Ring
45051-5-18
Jet
Adapter
SI/PGC5000-EN, Rev B 62
Sample
Line
LSV Body
LSV Body
Mounting
Mounting
Clamps
Clamps
Sample
Line
It is also important to use two wrenches when tightening the sample line connections. One wrench must be used to back up
the force applied to tighten the fitting. Direct wrench force (not using a back-up wrench) will damage the seals and possibly
bend the stem.
Sample will spill or leak out during this procedure. Consult MSDS sheets on file at your location for safety
requirements.
Sample valve repair may necessitate the venting of flammable substances into the atmosphere
surrounding the analyzer. Remove power from all sources of ignition in the immediate area. Do not
open any purged enclosures that remain powered.
Ensure proper safety equipment is worn, such as rubber gloves and face shield or safety glasses.
It is the customer’s responsibility to ensure that the area is safe and and hazard-free, and will remain so
the entire time the analyzer is open. This responsibility includes ensuring adequate ventilation in
analyzer shelter and obtaining proper work permits, etc.
To ensure the integrity of the components within the Liquid Sample Valve (LSV), use the tools in LSV Tool
Kit 791K009-1 when assembling or disassembling the LSV.
SI/PGC5000-EN, Rev B 63
Piston Rod
O-Ring
Cone Point Set
Screws (2) Body
Stem
Seals
Cylinder
Piston
Tensioning Nut
Body O-Rings
Stem
Tensioning Nut
O-Ring Sample
Belleville Chamber
Rear
Springs Valve Seat
In all steps the lubricant used is High Vacuum Grease, ABB part number 006904-1.
SI/PGC5000-EN, Rev B 64
3. Lightly lubricate the tensioning nut O-Ring and the Tensioning Nut threads, internal threads and bore of the body with
High Vacuum Grease.
4. Install the O-ring onto the Tensioning Nut.
5. Screw the tensioning nut into the body until the bottom of the nut grooves is approximately flush with the ears on the
back of the body.
6. Lightly lubricate the piston rod O-ring and the threads of the piston rod.
7. Install the piston rod O-ring onto the piston rod. Do not allow grease to enter the small hole through the center of the
piston.
8. Insert the stem into the rear of the piston rod.
9. Screw the piston rod into the piston and tighten to 27 to 30 in-lb. Do not overtighten or bend the rod or stem! Do not
allow grease to contact the stem.
10. Lightly lubricate the body O-rings.
11. Install the body O-rings onto the body and the piston.
12. Insert the piston and the piston rod into the sleeve, being careful not to cut the O-ring. Fully insert the piston until it
contacts the stops.
13. Stack the 15 Belleville springs onto the 1/4-inch thin wall plastic tubing, as shown in Figure 7.10.
14. Using the tubing only as a guide, slide the Belleville springs over the stem into the bore of the body.
15. Install the rear valve seat over the stem and let it rest against the Belleville springs. Do not allow the seat to scratch the
stem.
16. Clean all the exposed area of the stem with acetone to ensure the stem and groove are free of grease and contamination.
SI/PGC5000-EN, Rev B 65
17. Slide the first cleaned seal over the stem using the “A” end of Seal Insertion Tool TL-791A006B. The 30° angle (pointed
end) of the seal must face the Belleville springs. Figure 7.11 shows the orientation of the seal.
Seal
Seal
Stem
18. Slide the cleaned sample chamber over the stem onto the seal.
19. Slide the second cleaned seal over the stem using the “B” end of Seal Insertion Tool TL-791A006B. The 30° angled
(pointed end) of the seal faces out, away from the sample chamber. Figure 7.11 shows the orientation of the seal.
20. Lightly lubricate the threads on the body.
21. Retract the stem until it is flush with the front of the seal.
22. Screw the body into the flange against the vaporizer chamber until tight.
23. Push the stem into place.
24. The sample chamber should be loose in the assembly at this point. If not, back out the tensioning nut until the sample
chamber is loose. Use the end of a 0.156 Allen wrench in the slot of the tensioning nut to adjust to the point of
eliminating the longitudinal play of the sample chamber.
25. Tighten the tensioning nut in 24 1/4-turn increments (6 turns total) to load the seals.
26. Lightly lubricate the inside bore of the cylinder.
27. Align the fittings on the cylinder with the sample chamber tubes, or with air lines if servicing.
28. Slide the cylinder onto the piston and the body.
29. Install two cone point set screws into the cylinder and tighten into the groove on the body.
30. Reinstall tubing to the LSV, being careful to connect each line to the proper connection on the LSV.
31. Close the isothermal oven door.
SI/PGC5000-EN, Rev B 66
VALVE BODY
VALVE PLATE
CARRIER
ASSEMBLY
Ensure that there are no hazardous or flammable gases present in the immediate area of the analyzer.
The purged electrical sections of the analyzer will be declassified when purge is removed, and a danger
exists for fire, explosion, damage to property and injury or death to plant personnel during the nonpurged
time. Obtain proper permits such as hot work, etc.
Verify that the oven is cool (ambient temperature) before removing carrier gas.
SI/PGC5000-EN, Rev B 67
PART NUMBER
DESCRIPTION (dimensions are in inches)
40-PSIG KIT 60-PSIG KIT
764K001N-2 764K001N-1
It is essential to the analyzer's operation that all valve ports remain correctly connected.
SI/PGC5000-EN, Rev B 68
8. Remove the Carrier Assembly from the Valve Plate and Valve Body, being careful to keep the latches in their open
position.
9. Push the piston rod into the Valve Body to release the piston, being careful not to scratch any valve surfaces.
10. Remove the piston and piston rod from the Valve Body.
11. Remove the piston rod O-ring and the piston O-ring.
12. Wipe all surfaces of the piston and piston rod to remove contamination.
13. Verify that the screw holding the piston rod to the piston is tight.
14. Lubricate one O-ring part number 45051-4-11 with Molykote 33.
15. Position O-Ring Tool part number 3122-1 over the piston rod (see Figure 7.14).
LOCKWASHER
PISTON
PISTON O-RING
PISTON ROD
INSTALLATION TOOL
Fig. 7.14. Installing the O-Rings on the Piston Rod and Piston
16. Install the O-ring over the O-Ring Tool and into the O-ring groove on the piston rod.
17. Lubricate O-ring part number 45051-4-61 (40-psig valve) or 45051-4-29 (60-psig valve) with Molykote 33 and install it in
the O-ring groove of the piston.
18. Remove the old O-ring from the Valve Body (see Figure 7.15).
O-RING
VALVE BODY
19. Wipe the inside of the Valve Body to remove contamination and old lubricant.
20. Inspect the piston rod bore to ensure the bore is clean.
21. Lubricate O-Ring part number 45051-4-35 (40-psig valve) or 45051-4-31 (60-psig valve) with Molykote 33 and install it in
the O-ring groove in the Valve Body.
22. Lubricate the piston rod and the inside of the Valve Body (the piston housing area) with Molykote 33.
23. Insert the piston rod and piston rod assembly into the Valve Body. Before seating the piston, ensure the flat surface on
the piston rod is facing up.
24. Insert the Carrier Assembly on the Valve Plate.
25. Close the back Carrier Assembly latch. This ensures the Carrier Assembly is locked into the hole in the piston stem.
SI/PGC5000-EN, Rev B 69
VALVE PLATE
SCREWS
VALVE BODY
1. Clean the inside counter-bored holes of the Valve Body to remove contamination and old sealant (see Figure 7.16).
2. Align the holes in the Valve Plate with the holes/dowels in Valve Body and set into place. Care should be taken not to
damage the finish surface of the Valve Plate.
3. Dip the screws into RTV (Dow Corning #732 or GE #108) to within 1/8 inch from flat surface on bottom of the screw head.
4. Position screws through countered-bored holes in Valve Body and install into Valve Plate.
5. Tighten both screws securing the Valve Plate to the Valve Body. Screws should be torqued to 19 in. lbs.
7.8.1 Preparation
Ensure that there are no hazardous or flammable gases present in the immediate area of the analyzer.
The purged electrical section of the analyzer will be declassified when purge is removed, and a danger
exists for fire, explosion, damage to property and injury or death to plant personnel during the non-
purged time. Obtain proper permits such as hot work, etc.
Verify that the oven is cool (ambient temperature) before removing carrier gas.
SI/PGC5000-EN, Rev B 70
Service or replacement of the O-rings, plungers, or springs must be performed at the factory. Do not
disassemble the valve unless system malfunction is definitely isolated to the valve. Perform all other
system checks first.
All disassembly operations must be performed in a clean, well-lighted area. Flush all hazardous or toxic
materials from the valve before starting.
Top Mounting
Screws
SI/PGC5000-EN, Rev B 71
Cap
Screw
Port 1
SI/PGC5000-EN, Rev B 72
DID Location
Power Supply
SI/PGC5000-EN, Rev B 73
2. Secure the shield with the Phillips head screw retained earlier.
3. Remove, inspect, and replace if necessary, the PTFE ferrule in the reaction gas assembly before continuing.
The plasma cell is marked with a dot on the end of the cell that installs in the detector body.
4. Install the unmarked end of the plasma cell into the reaction gas assembly. Use caution not to damage the center
electrode ceramic.
5. Tighten the 1/4-inch tube nut finger tight only.
6. Verify the position of the center electrode ceramic. Viewed from the detector end of the plasma cell, the tip of the center
electrode should protrude approximately 1/32-inch past the edge of the high voltage tube clamp.
7. To adjust, loosen the 5/32-inch tube nut on the back of the reactor gas assembly that secures the center electrode.
8. Position the center electrode and tighten the 5/32-inch tube nut.
There are two small parts behind the O-ring, a ceramic and a stainless steel noise shield. Be careful not to
lose these parts.
If the parts fall out, replace them with the ceramic first and then the stainless steel noise shield.
9. Remove the closest nut, ferrule and O-ring from the detector body.
10. Slide the closest nut, ferrule and O-ring onto the marked end of the plasma cell.
11. Gently insert the plasma cell into the body of the detector until it stops.
12. Tight the closest nut finger tight only.
13. While supporting the plasma cell, reconnect the plasma high voltage lead.
14. Reconnect the ground lead, if necessary.
15. Turn on power to the oven.
16. Purge the detector for at least five minutes with reactor gas.
17. Turn on the plasma power supply switch.
18. Enable isothermal oven temperature zone.
19. Allow the oven to heat and stabilize at temperature.
20. Allow the system to purge for five minutes prior to starting the plasma.
SI/PGC5000-EN, Rev B 74
8 Replacement parts
8.1 Ordering information
Since the particular application defines the component parts specific to any given system, please refer to
the “Recommended Spare Parts Lists” in the analyzer’s Data Package to obtain the full and correct part
number for the desired part or assembly.
• For serial numbered subassemblies such as PCBs, include the serial number and the part number (including dash
number and revision letter) for the subassembly in the request. If a PCB requires conformal coating, prefix the PCB
part number with the letters "CC."
• Applicable references from the “Recommended Spare Parts List” of the Data Package, included with each analyzer.
• Description of part.
Model
Number Sales Order
Number
The hardware configuration consists of the model number and sales order number.
SI/PGC5000-EN, Rev B 75
Model
Number Sales Order
Number
The remainder of this section lists the replaceable parts and components by their location in the equipment. Part numbers and
drawing numbers listed here are for identification purposes only. When you order parts for replacement, use the list of parts
included in the Engineering Data Package provided with your equipment to ensure you have the correct version of each part.
SI/PGC5000-EN, Rev B 76
Touch Panel
Controller
SI/PGC5000-EN, Rev B 77
EPC Control
PCB
Power
Supply
Detector
Amplifier
Assy
DTC Digital
EPC Analog PCB
PCB Assy
Oven
Indicator
PCB
SI/PGC5000-EN, Rev B 78
Power Supply
SI/PGC5000-EN, Rev B 79
Oven
Heater
M2CP
Valve
Detector
Assy
SI/PGC5000-EN, Rev B 80
SI/PGC5000-EN, Rev B 81
Reference Measure
Filament Filament
SI/PGC5000-EN, Rev B 82
SI/PGC5000-EN, Rev B 83
O-Ring
45051-4-106 Sulfur
Addition
O-Ring Wafer
45051-4-102
O-Ring
45051-5-18
Jet
Adapter
SI/PGC5000-EN, Rev B 84
Proportional
Valve
Sensor PCB
Heater
Control PCB
SI/PGC5000-EN, Rev B 85
SI/PGC5000-EN, Rev B 86
NOTES
SI/PGC5000-EN, Rev B 87
B 08.2016
01.2013
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