27-05-2022 12:02:57

CEPHAS LIFE SCIENCES PVT.LTD

Sample Information
Acquired by : Phani Kumar
DateAcquired | 5/27/2022 8:48,52 AM
SampleName : Theruptor Steril€ Banier Wound Dressing
Sample ID : Diluent Blank
Trat# :l
Vial# :l
Injection Volume :20
Data File : Diluent Blank-002.Icd
Method File SPL-22-035 l_EX_LCMS-N-proc.lcm
Original Method File :SPL-22-0151 EX LCMS-N lcm
Processed by : Phani Kumar
Date Processed : 5/2712022 ll23:05 AM

MS Chromatogram
Diluent Blank-002.1cd

{r 10P00, totlooo>srrooo(+t@7
l.oo I
]t6.3e7
l .i
0.ofr
2.88 ](x10,000)
l2t-7s9

l0l 2000-,-56 0000( -)ir.1

I,i9 l (xlr:)>6 1. 1 000(+) ('5

#H __l

o.oaF T
0 3 4 7 8 I )0
nIn

MS Quantilalive Table

t ID#
I
Name
N-Nitrosomorpholine
Ret. Time fitJz
117. t0>45.0s
Height s/N

I, 2 N-Nitrosopyrrolidine l0l.l0>55.10
l N-Nitrosodimethylamine 75.10>43.00
I N-Nitrosodiethylamine 102 2D56.00
5 N-Nilroso-N-Methvlethlanrine 89.10>61.I0
N-Nilroso-Di-N-Propylamine l3 r. t 0>89.10
7 N-Nitrosopiperidine I15.l0>69. | 0
u N-Nitroso-N-Di-bulylamine t59.10>57.20
Tota 0 (l

*u'r*Orr,*;A,,r- Checked By:

1t1
 27-05-2022 12.03:02

CEPHAS LIFB SCIBNCES PVT.LTD

Sample Informalion
Acquired by : Phani Kumar
DateAcquired : 5121 /2022 8:5950 AM
Sample Name : TheruDlor Sterile Barrier Wound Dressins
Sample ID Workihg Standnd Solution-Ol
Tratr+ :l
Vial# :2
InjectionVolume :20
Dala File Working Slandard Solutjon-ooJ tcd
Melhod File : SPL-22-03 51_EX_LCMS-N-proc.lcm
Original Method File : SPL-22-0351 EX LCMS-N.lcm
Processed by : Phani Kumar
Date Processed : 5127n022 llt2306 AJ\.I,

MS Chromatogram
Working Standard Solution-003.1cd

Int€nsity
8.39l(xt00) nS H7 r000>15 0500(+)(71

f., /'E
o.oot,-
3.90 kxlO,O00) l0l 1000>55 1000(+)ia2

75 100D43.0000(+)@3

0.00
2.00 102.200D56.0000(+)@41

--
0.00
2.00 89imo-jr-r004tr)@l

) _l
2.96 (x10,000) 13 l. 1000>89. l 000(+)@6

0.00 F--
3.39 (x10.000) iTtrabaxrLoaF@l
]33.8e6
I
0.00 I
3.20 (x10.000)
13l.96l

o.oaf-- _ 1

0l I 56J 9 t0
min

MS Quantitative Table

ID# Name Ret. Time filz Height SrN

l N-Nitrosomorpholine |.497 I17.10>45 05 14222. 6s9 54.86
2 N-Nitrosopynolidine I 521 101.10>55.10 49950t 32019 67.84
.,] N-Nitrosodimethylamine 1188 75.10>43.00 7',7119 5268 l4t.55
t N-Nitrosodiethylamine 1.517 102.20>56.00 26830 178,1 21.7 t
5 N-Nitroso-N-Methylethlamine 1.5 l8 89 10>61 l0 28t572 22t12 324.8,{
N-Nilroso-Di-N-Propylamine 1 726 l3l.l0>89.10 368228 691 96
1 N-Nitrosopiperidine 1.6t0 ll5.l0>69 l0 4t 5949 27995 l8l l5
8 N-Nilroso-N-Di-bulylamine I 999 r59.t0>57.20 38049r 26698 445 73
Tota 2064133 l4I315

*.,r*dBr,:S{2r)r- Checked By:

1t1