IS0

INTERNATIONAL STANDARD 6741-2

First edition
1987-04-M

INTERNATIONAL ORGANIZATION FOR STANDARDIZATION

ORGANISATION INTERNATIONALE DE NORMALISATION
MEXAYHAPOAHAfl OPTAHM3A~VlR I-IO CTAH~APTM3A~MM

Textiles - Fibres and yarns - Determination of

commercial mass of consignments -

Part 2 : iTeh STANDARD PREVIEW

Methods for obtaining laboratory samples
([Link])
Textiles - Fibres et fills - Ddtermination de ISO
la masse commerciale d’un lot -
6741-2:1987
Partie 2: Mkhodes
[Link]
d’ob ten tion des khan tillons pour labora toire
c5c7078d8061/iso-6741-2-1987

~ R eference number
I IS0 6741-2: 1987 (E)
Foreword
IS0 (the International Organization for Standardization) is a worldwide federation of
national standards bodies (IS0 member bodies). The work of preparing International
Standards is normally carried out through IS0 technical committees. Each member
body interested in a subject for which a technical committee has been established has
the right to be represented on that committee. International organizations, govern-
mental and non-governmental, in liaison with ISO, also take part in the work.

Draft International Standards adopted by the technical committees are circulated to

the member bodies for approval before their acceptance as International Standards by
the IS0 Council. They are approved in accordance with IS0 procedures requiring at
least 75 % approval by the member bodies voting.
iTeh STANDARD PREVIEW
International Standard IS0 6741-2 was prepared by Technical Committee ISO/TC 38,
Textiles. ([Link])
ISO 6741-2:1987
Users should note that all International Standards undergo revision from time to time
and that any reference made herein[Link]
to any other International Standard implies its
latest edition, unless otherwise stated. c5c7078d8061/iso-6741-2-1987

0 International Organization for Standardization, 1987

Printed in Switzerland
 --
INTERNATIONALSTANDARD IS0 6741-2 : 1987 (E)

- Fibres and yarns - Determination of

cial mass of consignments -

Part 2 :
Methods for obtaining laboratory samples

0 Introduction The procedures comprise :

This document forms part 3 of a four-part International Stan-

iTeh STANDARD PREVIEW
dard prepared by ISO/TC 38, Textiles. b
Nature of consignment Procedure described
Hand sampling (two methods)
Bulk staple in bales
Part 1 : Mass determination
([Link])
and calculations.
Core sampling

Part 2: Methods for obtaining laboratory samples. Tow and strands in bales
Hand sampling
and cases
ISO 6741-2:1987
Unsupported wound or coiled
Part 3: Specimen cleaning procedures.
[Link]
packages of raw silk, tow
Hand sampling
c5c7078d8061/iso-6741-2-1987
sliver, top or yarn in
Part 4: Values used for the commercial allowances and the containers
commercial moisture regains. (Technical Report.) Cutting method
Yarn wound on supports
Winding (four methods)
The terminology used in this International Standard is in ac-
cordance with IS0 6348.

Most contracts of sale between buyer and seller specify either When a replicate sample is required for other tests or as a pre-
that the invoice mass of a consignment shall be determined by caution against misadventure, the mass taken during sampling
an independent third party, or that the seller’s figure’may be shall be doubled and the sample shall then immediately be
subject to an independent third-party check. This part of halved to provide the two samples.
IS0 6741 describes the methods which are to be used by the in-
dependent third party in these cases. The figure for the com-
mercial mass which results from the application of the pro- 2 References
cedures in this part of IS0 6741 either becomes the invoice
mass of the consignment or is compared with the declared IS0 6348, TextlJles - Determination of mass - Vocabulary.
invoice mass plus or minus the tolerance agreed between the
buyer and seller. IS0 6741, Textiles - Fibres and yarns - Determination of
commercial mass of consignments
It is not intended that the methods in this part of IS0 6741
necessarily be used by the seller to establish his invoice mass. - Part I : Mass determination and calculations.

The methods described in this part of IS0 6741 are, for the - Part 4 : Values used for the commercial allowances and
most part, destructive. the commercial moisture regains. (Technical Report.)

1 Scope and field of application 3 Principle

This part of IS0 6741 specifies methods for obtaining Laboratory samples are taken from the containers in the
laboratory samples for mass determination by one of the consignment samples obtained as specified in IS0 6741-1 and
methods given in IS0 6741-1. The method appropriate for par- placed in stoppered, air-tight vessels for subsequent process-
ticular fibres is indicated in IS0 6741-4 ing.

1
IS0 6741-2 : 1987 (E)

4 Apparatus Consider the bale as being made up of two zones, inner and
outer, both of about the same volume (see figure I). The
Air-tight vessels, of low hygroscopicity and known mass, dimensions of the inner zone shall be 80 % of those of the bale,
capable of holding the material being tested. For example, a i.e. the thickness of the outer layer represents 10 % of the cor-
stoppered glass jar or a clean, grease-free polyethylene bag of responding dimension of the bale.
minimum thickness 70 pm, inside a second similar polyethylene
bag, is sometimes used. In the latter case, both bags shall be a) From the outer zone take 12 samples, each weighing
sealed and free of holes. about 5 g, two being taken from each face at randomly dif-
ferent positions and depths within the layer.

5 Sampling procedure b) From the inner zone take a further six samples, each
weighing about 10 g. Consider the inner zone to be made
Sample, preferably immediately after weighing each container up of six equal layers (see figure 21, three layers above and
in the consignment sample as specified in 6.2 of IS0 6741-1, in three layers below the centre line of the bale, and take one
accordance with 5.1, 5.2 or 5.3, as appropriate. sample at random from each of these layers.

As each sample is taken from the bale, place it immediately into

5.1 Consignments of bulk staple in bales a pre-weighed, air-tight vessel. There should finally be about
120 g of fibre in the vessel.
5.1.1 Method A
5.1.2 Method B
Remove the bale wrappers. Take samples from the bale in such
a manner that Remove the bale wrappers.

- each sample is taken from the appropriate zone described Use a hand sampling method similar to that described in 5.1 .I.
below;
Employ three distinct points of sampling situated on a diagonal
iTeh STANDARD
- no more than 30 s elapse between the exposure of a line of thePREVIEW
parallelepiped constituted by the bale and positioned
sample and its confinement in an air-tight vessel (clause 4). at 20 %, 50 % and 80 % of its length. Take one sample, mass

Samples may be taken with

([Link])
a hook, but any handling shall be
at least 150 g, at each point and place it immediately into a pre-
weighed, stoppered, air-tight vessel (clause 4). The mass of the
carried out with gloves of an impervious material. staple in the vessel should finally be about 500 g.
ISO 6741-2:1987
[Link]
c5c7078d8061/iso-6741-2-1987

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f
I I I
I I
I I
I I I
I
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Figure 1 - Zones of a bale Figure 2 - Layers of inner zone

2
 IS0 6741-2 : 1987 (E)

5.1.3 Method C Use either one vessel per bale or, if a global sample is to be
used, one or more large vessels between which all the cores
Select and use one of the following methodsl). from all the containers are equally divided.

In the case of high-density bales (more than 450 kglms), spe-

[Link] Method Cl
cial equipment shall be employed. The commercial mass of
high-density bales can nevertheless be determined by partial or
Use a core sampler with a non-rotating coring tube with manual
complete removal of wrappers, followed by methods B, Cl
pressure. The diameter of the cutting tip (which shall be sharp
and C2.
to achieve good bale penetration) shall be 12 to 25 mm and the
tube length shall be 600 + 20 mm.

Clear the point of tube penetration and insert the corer in a Table 2 - Coring programme for bales, method C2
direction which is parallel to the sides of the bale in the direc-
tion of compression to a depth of not less than 47 % of the bale Number of bales in the
Number of cores per bale
length. consignment sample
1 20
Extract not less than 35 core samples at random from the con- 2 10
signment sample in accordance with table 1. Place the samples 3 7
from each bale immediately into a pre-weighed, stoppered, air- 4 5
tight vessel. Use either one vessel per bale or, if a global sample 4
5, 6
is to be used, one or more large vessels between which all the 3
7, 8, 9
cores from all the containers are equally divided. 10 to 19 2
20 and above 1

Table 1 - Coring programme for bales, method Cl

Number of bales in
the consignment
iTeh STANDARD PREVIEW
Number of cores
Number of cores
from each face
per bale Method C3 [Link]
sample
1 35
([Link])
of the bale*
18/17 Use a core sampler with a non-rotating coring tube with manual
2 18 919 pressure. The diameter of the cutting tip (which shall be sharp
3 12 6/6
ISO 6741-2:1987
to achieve good bale penetration) shall be 25 + 1 mm and the
4 [Link]
9 5/4 tube length shall be 600 + 20 mm.
5 7 c5c7078d8061/iso-6741-2-1987
4/3
6 6 313 Clear the point of tube penetration and insert the corer in a
7, 8 5 3/2 direction which is parallel to the sides of the bale in the direc-
9, 10, 11 4 212 tion of compression to a depth of about 90 % of the bale
12 to 17 3 2/l length.
18 to 34 2 l/l
35 and above 1 l/O Extract from each bale the number of cores indicated in table 3.
* Core alternately through the cap and base. Place the samples from each bale immediately into a pre-
weighed, stoppered, air-tight vessel (clause 3). Use either one
vessel per container or, if a global sample is to be used, one or
more large vessels between which all the cores from all the con-
[Link] Method C2 tainers are equally divided.
Use a core sampler with a non-rotating coring tube with
mechanical pressure. The diameter of the cutting tip (which
shall be sharp to achieve good bale penetration) shall be
18 -+ 1 mm21 and the tube length shall be sufficient to achieve Table 3 - Coring programme for bales, method C3
a depth of penetration of at least 90 % of the bale length.

Clear the point of tube penetration on the base of the bale and
insert the corer in a direction which is parallel to the sides of the
bale in the direction of compression to the full depth of the
tube.

Extract not less than 20 core samples at random from the con-
signment sample in accordance with table 2. Place the samples
from each bale immediately into a stoppered, air-tight vessel.

1) Methods Cl and C2 are based upon the IWO manual and machine coring procedures respectively.
2) The interested parties may agree to use a cutting tip with a diameter between 12 and 25 mm.

3
 IS0 6741-2 : 1987 (E)

5.2 Consignments of tow and strands in bales or For supported packages, determine the total mass of the sup-
cases ports and wrappings to permit the calculation of the net mass
of the container (see sub-clause 6.2 of IS0 6741-I).
As with staple fibre, wear impervious gloves when handling the
material. As for staple, wear impervious gloves when handling the
material.

5.2.1 Method D Unwrap each unit package and immediately take about 30 g of
fibre (60 g in the case of wool) from its outer surface. Then cut
Take a sample of about 30 g from the material at the top of the or divide each package in order to reach its middle and take
bale or case. Take three further samples, each of about 20 g, 60 g (120 g in the case of wool) from here. Continue cutting or
from the interior of the bale, at points P, Q, and R in a middle dividing to the end of each package and take a final 30 g sample
t. layer of the bale shown in figure 3. One point is at the centre of (60 g in the case of wool). Place each sample immediately into
the layer and the other two half-way between the centre and a pre-weighed air-tight vessel (clause 4) within 30 s of ex-
the surface of the bale. Access to this middle layer may be ob- posure. There should finally be about 120 g fibre (480 g in the
tained either by winding off or by lifting off the upper layers. case of wool, half from each package) in the vessel.

Take a fifth sample (of about 30 g) from the material at the bot-
tom of the bale or case. 5.4 Consignments of yarn on packages

From each of the containers to be sampled take one package at

random, and from a different position in each container.

5.41 Method F

Rapidly cut the yarn from each package with a sharp knife, the
iTeh STANDARD PREVIEW cut being made in a n approximately axial pla ne.

([Link])
[Link] Packages of mass 250 g or less

Immediately place the yarn cut from each of the packages into
ISO 6741-2:1987
a pre-weighed air-tight vessel (clause
4). Carry out the
[Link]
laboratory test on the entire package.
c5c7078d8061/iso-6741-2-1987
[Link] Packages of mass more than 250 g

Lay flat the yarns cut from each of the packages” Take six sub-
samples of approximately 40 g very rapidly at various depths
and immediately place all together in an air-tight, tared vessel
(clause 4). Take these six sub-samples from six different layers,
one on the outside, another on the inside and the four others
Figure 3 - Tow in bale equally distributed between the two. Carry out the laboratory
test on the global sample.

Take the samples immediately after exposing the surface con-

cerned, with a maximum delay of 30 s. As each sample is taken 5.4.2 Method G
from a single bale or case, place it immediately into a pre-
weighed air-tight vessel (clause 3). There should finally be The following method may, by agreement, be adopted as the
about 120 g of fibre in the vessel. alternative to method F in order to reduce yarn wastage when
the consignment comprises large packages (over I,5 kg).

5.3 Consignments of tow, sliver or top delivered Weigh the sample packages to within 0,l %.
as wound or coiled packages in con ltainers
Reel all the yarn from each package through a length-
measuring device at a speed not exceeding 200 m/min with a
5.3.1 Method E reeling tension in the range 0,4 to 0,6 cN/tex. The length-
measuring device shall consist of a hard, smooth measuring
Tow, sliver and top may be delivered as wound or coiled roller of uniform diameter not less than 100 mm, on the shaft of
packages, with or without support or wrapping, with a number which a revolution counter is mounted, and against which a
of such packages in each container of the consignment. roller of softer material is pressed with a force of at least 10 cN
per cm of the line of contact between the two rollers.
From each of the containers to be sampled take one package
(two in the case of wool) entirely at random, and from a dif- Whilst reeling the yarn, take six samples, each of mass about
ferent part of each container. 40 g, at positions distributed aPProximately equally throughout
 IS0 6741-2 :1987 E)

each package. Measure the length of each sample, and the port to an accuracy of 0,05 g. Record the difference between
length of yarn between it and the next sample, to within 0,l %. the two masses.
Take the first and the last samples from the beginning and from
the end of the package.
[Link] Packages of mass more than 250 g
Immediately place each sample into a pre-weighed air-tight
vessel (clause 4). Wind onto a wrap reel six successive sub-samples, each of
mass about 40 g, from positions spaced equally through the
package. Weigh the package to an accuracy of 0,05 g im-
5.4.3 Method H
mediately before and immediately after winding each sub-
sample; the mass change is the mass of the sub-sample.
From every group of three packages, wind a maximum of 400 g Record the total mass of the six sub-samples.
per package. The laboratory samples shall be taken from the
external surface of two packages and from the inside of the The recorded mass is the mass of the sample , free from any
third package. The mass of the laboratory samples shall be discrepancy due to moisture on winding.
calculated from the difference in mass of the package before
and after winding, disregarding and change in moisture content
of the yarn. 5.5 Consign ments of yarn and raw silk delivered
in containers which carry a number of s keins
5.4.4 Method J

If the package weighs less than 250 g, unwind all the yarn from 5.5.1 Method L
the package as a single laboratory sample. Otherwise unwind,
in turn, six sub-samples each of mass about 40 g equally From each of the containers to be sampled, take at least 350 g
distributed through the package. in at least three skeins from different positions within the con-
tainer, and place the skeins together into a pre-weighed air-
Take a sample from each package by unwinding and im- tight vessel (clause 4).
iTeh STANDARD PREVIEW
mediately place the sample into a pre-weighed air-tight vessel
(clause 4).
([Link])
5.6 Unspecified consignments
5.4.5 Method K
ISO 6741-2:1987 5.6.1 Method Z
[Link] Packages of [Link]
mass 250 g or less
c5c7078d8061/iso-6741-2-1987
Some other sampling procedure agreed between the inter-
Weigh the package, includi ng the support, to an accuracy of rested parties for use when the other methods described in this
0,05 g. Unwind all the yarn using a wrap reel. Weigh the sup- part of IS0 6741 are not suitable.
IS0 6741-2 : 1987 (E)

iTeh STANDARD PREVIEW

([Link])
ISO 6741-2:1987
[Link]
c5c7078d8061/iso-6741-2-1987

~~~~
UDC 677.061 : 531.755
Descriptors : textiles, textile fibres, yarns, tests, determination, commercial mass.

Price based on 5 pages