Jagdamba Education Society’s

S.N.D. COLLEGE OF PHARMACY

At-Babhulgaon, Tal. Yeola, Dist. Nashik, Maharashtra-423401
Website- www.sndpharmacy.com
Contact No- 02559-225041/42

NACC Accredited with Grade “B”

BACHELOR’S IN PHARMACY
FINAL YEAR B. PHARMACY STUDENTS
-PROJECT REPORT-
Year – 2023-2024

1
 A
PROJECT REPORT ON FORMULATION AND
EVALUATION OF HERBAL LIPSTICK

Submitted to

Jagdamba Education Society’s

SND College of Pharmacy
Babhulgaon, Yeola, Dist. Nashik - 423 401
Academic Year - 2023-24

BACHELOR’S OF PHARMACY

Submitted by :-

Miss. More Shraddha Sunil

(Final year B. Pharmacy)

Guided By:

Prof.W.F. Jagadale.

(M.pharm)

2
 Jagdamba Education Society’s
SND College of Pharmacy,
Babhulgaon, Yeola

Declaration by the Candidate

I hereby declare that this Project Report entitled

“FORMULATION AND EVALUATION OF

HERBAL LIPSTICK”
is a bonafide and genuine Project Report carried out by me under the guidance
of Prof. W.F. Jagadale. HOD of Diploma, Jagdamba Education Society’s SND
College of Pharmacy, Babhulgaon, Yeola.

Date:
Place: Babhulgaon
Miss. More Shraddha Sunil
(Final Year B Pharm)

3
 Jagdamba Education Society’s
SND College of Pharmacy,
Babhulgaon, Yeola
Declaration by the Guide
This is to certify that the Project Report entitled “FORMULATION
AND EVALUATION OF HERBAL LIPSTICK” a
bonafide Project Report done by Miss. More Shraddha Sunil, (Final Year
B. Pharmacy)in partial fulfillment of the requirement for the Bachelor of
Pharmacy.

Prof. W.F. Jagadale.

Date:
HOD of Diploma,
Place :Babhul
gaon Jagdamba Education
Society’s SND College of
Pharmacy, Babhulgaon,
Yeola.

4
 Jagdamba Education Society’s
SND College of Pharmacy,
Babhulgaon, Yeola

Endorsement by the Principal

“FORMULATION
This is to certify that the Project Report
AND EVALUATION OF HERBAL LIPSTICK”
is a bonafide Project Report done by Miss. More Shraddha Sunil in partial
fulfillment of the requirement for the Bachelor of Pharmacy.

Date: Dr. Pradyumna Ige

Place: Babhulgaon M. Pharm, Ph.D.
Principal, SND College
of
Pharmac
y, Yeola –
423 401
 Acknowledgement
The satisfaction that accompanies the successful completion of any
task would be incomplete without mention of the people who made it
possible with constant guidance, support and encouragement that crows
all effort with success. This was all possible due to the blessing of my
parents. I would like to express my appreciation for all the efforts to
everyone who have directly or indirectly contributed their ideas and
energies in successful completion of my project.

I wish to express my sincere thanks with a deep sense of gratitude,

to my respected guide Prof. W . F . Jagadale Assistant Professor, SND
College of Pharmacy Babhulgaon, Yeola for his immense guidance, help,
dedicated support, intellectual supervision and professional expertise he
has bestowed upon me for the timely completion of this work. All in all,
it’s my fortune and so I am proud to have him as my guide. I consider
myself to be very fortunate to work under him, whose belief, discipline,
principles, simplicity, caring attitude, provision of fearless work
environment and confidence in me has given courage to follow my
dreams in the arena of research. All in all, it’s my fortune and so I am
proud to have him as my guide.

I would like to express my gratitude to Prof. W.F. Jagadale for their

support, encouragement, for the facilities provided to me to carry out my
project as a successful one and for providing me all the possible guidelines
to carry out physical, chemical and spectral evaluation of my drug and
excipients. I also thank to all teaching and non-teaching staff for their
direct or indirect support.
 Just like each drop of water has its own importance in
contributing to the making of an ocean, each and every person
mentioned have played their own important and unique role in
making this work a reality.

Thank you, one and all…

Ms .More Shraddha Sunil

(Final year B. pharmacy)

 INDEX

Sr.No. Content Page No

1 Abstract 9

2 Introduction 10

3 Literature Survey 14

4 Materials and Methodology 16

5 Evaluation Parameters 23

6 Discussion 25

7 Result and Conclusion 26

8 Reference 27
ABSTRACT:

The makeup used to color the lips is called lipstick. It improves the lips' look. Lipstick
is used to the lips to enhance attractiveness, make them appear more appealing, and shield
them from various UV radiation that can cause damage. A cosmetic item including pigments,
oils, scents, preservatives, colors, textures, and lip protection is called a herbal lipstick. It is
now practically a standard component of women's handbags. Lips that are shiny, smooth, dry,
or moist all simply depend on how makeup is applied. Because natural cosmetics are safe,
herbal lipsticks are becoming more and more popular. Hundreds of color variations are
available on the market to meet women's demands for liquid and stick-on lip tints. Lipsticks
made of herbs have few adverse effects. It is safe to use and contains natural nutrients or
chemicals that maintain healthy lips. Lipstick with synthetic colorants is really bad for our
skin because they are composed of dangerous chemicals. Synthetic colorants can cause major
health issues such as skin discoloration, lip cancer, skin inflammation, etc. when used
continuously over an extended period of time. Lipstick has been shown to have a variety of
harmful effects, including allergic reactions, nauseousness, dermatitis, lip dryness, and even
death. Consequently, due to their safety, demand for cosmetics using herbal elements has
grown worldwide. This review paper discusses the benefits of herbal lipstick, as well as its
formulation flaws, ideal qualities, anatomy of the lips, and evaluation.

Keywords: Herbal Cosmetics, Lipstick, Synthetic material, Harmless, Evaluation parameter.

INTRODUCTION:

Cosmetics have become an integral part of every woman’s life. Herbal cosmetics are
products which are formulated using various permissible cosmetic ingredients in which one
or more herbal ingredients are used to provide distinct cosmetic benefits. They are also called
as herbal cosmetics. Herbal cosmetics are the latest trend in the field of beauty and fashion.
The herbal cosmetics industry is experiencing a rising graph for its market and products
which are being sold the world over. Today, there are a plethora of brands in the cosmetics
market. Yet, the market is still growing and there is scope for new products who can deliver
quality natural based products that will satisfy the consumer’s requirements. Herbal products
are gaining popularity as nowadays most women prefer natural products over chemicals for
their personal care to enhance their beauty as these products supply the body with nutrients
and enhance health and provide satisfaction as these are free from synthetic chemicals and
have relatively less side-effects compared to the synthetic cosmetics. Lipstick is cosmetic
preparation used to color the lip and protect lips from external environment. Coloring lips in
an ancient practice date back to prehistoric period. Now-a-days the use of herbal product has
increased and choice of shades of colors, textures, luster, have been changed and become
wider. This can be observed from the facts that lipstick is marketed in hundred of sheds of
colors to satisfy latest demand of the women. The dyes that contribute to the color of the
lipstick are very harmful to humans on consumption. Coal tars are the basic ingredients from
which synthetic dyes are formed can cause allergy, nausea, dermatitis, and drying of the lips.
In a more severe form they can be carcinogenic and even fatal. Cosmetic means any article
intended to be sprayed poured rubbed or sprinkled on, or introduced into or any parts for
cleansing, beautifying, promoting attractiveness or altering the appearances. Cosmetics are
the substance use to alter of appearance or fragrance of human body. Lipstick are most
widely used cosmetic added in the make up to enhance the beauty of lips. A good lipstick
should have persuading characteristics and be acceptable to consumer, such as having a
suitable texture and antioxidant properties. Bases, oils, emollient and colorant are among the
variety of components that contribute to properties of fine lipstick. Texture, melting point and
hardness of lipstick are the dominant characteristics that are modified by varying the ratio of
component that are used in the formulation. Colorant or pigment are the component that play
an important role in the lipstick formulation as it determines the aesthetic value of lipstick.
Colorant can be from synthetic and natural sources. Synthetic colors are manufactured
chemically. The synthetic dyes that contribute the color to the lipstick are dangerous to
human on consumption and may cause adverse effect such as allergy, dermatitis, skin
discoloration, drying of lips, etc. In some cases, they can be carcinogenic and even fatal. This
limitation thus leads the use of natural colorants in production of lipstick. Natural colors are
extracted from natural sources such as plants, insects, and algae.

Objectives:

 Herbal colours are non-toxic, highly lipophilic, antioxidant and anti-microbial anti-
inflammatory and are used in leucoderma more particularly of lips.
 Colorant has different original shades of colours from purplish red, ruby red,
beetroot purple, dark violet, pastel red, pale red, purplish red, rose red, deep
magenta, dark purple, orange, deep violet.
 From these colours, by different combinations, further shades can be obtained.
 Colour may be changed to the different shades with organic and inorganic acid and
bases.

Ideal characteristics of good lipstick:

 It should be non- irritant.

 It should have required plasticity.
 It should nontoxic.
 That should be physically and chemically stable.
 It is not expected to dry up on board.
 It should be heavily particulate free.
 After application it can retain lip color for longer periods.
 This should offer sweating-free shiny and smooth appearance.
  It should look, smell and feel good.
 It should not fuse or harden within acceptable climatic temperature variation

Types of lipstick with basic charateristics:

1. Moisturizing Lipsticks:-

Individuals who have dry lips should use moisturizing lipsticks as it keeps lips soft
and smooth. These lipsticks moisturize lips due to ingredients like
vitamin E, glycerin and aloe. Other great things about using moisturizing lipsticks are wet
and very shiny lips.

2. Satin and Sheer Lipsticks:-

These lipsticks also moisturize and nourish lips and ensure it is shiny and glossy.
Sheer and satin lipsticks have high oil ingredients and they could appear
darker in the package than they are on lips. Another characteristic of lipsticks with oil
components is that it must be replied many times.

3. Mate and Lipstick:-

Mate lipsticks are perfects selection for women who are seeking colorful and nice
shade. These lipsticks have affectation of flat and not shiny lips. Your
lips will look smother and younger with matte lipstick. Plus it is advised to mix products with
vitamin E and aloe with mate lipsticks.

4. Cream Lipstick:-

Women who’d small lips should use cream lipsticks. Lipstick with cream formula is
not shiny, but it’s smooth influence on lips. You need to use lip gloss
afterward for desire look. Cream lipsticks contain more wax to be able to protect lips, but also
cause aftereffect of dry lips.

5. Pearl and Frosted Lipstick:-

 Frosted lipstick makes lips sparkle and glisten. Pearl and frosted lipstick reflects light
and makes very shiny effect on your own lips. Negative effects are that could cause lips feel
heavy, crack and dry. It is advised to moisturize your lips before utilize this lipsticks.

6. Gloss Lipstick:-

Gloss is extremely popular lipstick for girls with thin and small lips because make lips
shine and improve the dimension of depth. Gloss may be along
with traditional lipstick.

7. Long Wearing and Transfer Resistant Lipsticks:-

Women who don’t have time to utilize Lipstick frequently may use long wearing
lipstick. These lipsticks have formula that keep lips look perfect from
4-8 hrs. They’re resilient and soon you eat something greasy or oily. Many of them contain
moisturizer to balance the dryness of lips.

A cosmetic lip care should have the following criteria from a customer
perspective:
attractive color Homogeneous color when applied

 Attractive colour
 Homogeneous colour when applied
 Pleasant smell and taste
 Easy to apply
 No staining or bleeding into fine line surrounding the lips
 Long lasting effect

Marketed brands of Lipsticks:

1. MAC
2. Huda Beauty
3. Glossier
 4. L’oreal
5. Maybelline
6. LPSY
7. Avone
8. Wet and Wild
9. Lakme
10. Sugar

Merits of Natural Lipsticks over existing Synthetic ones:

 Herbal dyes are non-toxic, highly lipophilic, antioxidant and anti-microbial anti-
inflammatory
 and are used for leukoderma especially on the lips.
 Colorant has different original colors from purplish red, ruby red, beetroot purple,
dark violet,
 pastel red, red pale, red purplish, rose red, deep magenta, dark purple, orange,
violet deep.
 In these colors, with different combinations, other shades can be found.
 Colour can be changed to different colors with organic and inorganic acid and bases.
Literature Survey:
Meher Dipali , et.al.(2011)

Herbal cosmetics have growing demand in the world market and are an individual gift
of nature. There are a wide range satisfy your beauty regime, adding herbal in cosmetics is

very safe for skin. Human being have been herbs for different purpose like food, medicine,

beautifying with advancement of science and technology use of natural things including

plant has been reduced except for food, vegetarian takes plants and plants only. However

there is resurgence of use of herbs both of drug and cosmetics.

Pooja Mishra et.al(2012)

Colouring lips in an ancient practice date back to prehistoric period. In present day’s
the use of product has increased and choice of Shades of colour, texture , lustrous , have been

changed and become wider. This can be observed from facts that lipstick is marked in 100

shades of colour to satisfy the demands for the women. Which will be extensively use by

women of communities with grate surety and satisfaction.

Rautela Sunil et.al(2013)

Cosmetics include skin-care creams, lotions, powder, perfume, lipstick, fingernail,

eye and facial makeup. Permanent waves, coloured contact lenses,

hair colour , hair spray and gels, deodorant , baby product are in great demand in both

developing and developed countries. The present investigating was done to formulate herbal

lipstick, since lipstick are one of the key cosmetics to be used by the women. Due to various

adverse effect of available synthetic preparation on the present work was conceived by us

to formulate lipstick having minimal or side effect

Swati Deshmukh et.al (2013)

Now a day’s, in the whole world there is turn to return towards the use of herbal
products and to adopt more natural way of life. People prefer natural food, herbal cosmetics,
medicine and natural curing practice for healthy life, there is much craze for the vegetable

products cultivated organic forming without using synthetic fertilizer and pesticides. The

use of herbal cosmetics has been increased to many folds in personal care system and there is
a grate demands for the herbal cosmetics. Natural products have been used for folk

medicine purposes throughout the world for thousands of years.

Farida Hayati, et.al.(2016)

Cosmetics with natural ingredients are believed to be safe than chemical based
cosmetics; in additional, natural cosmetics have the ability to protect the skin from ultra-
violet rays. One of the widely used cosmetics nowadays is lip colour in the form of better
known as lipstick, which can also serves as both natural and chemical . The development of
natural cosmetics ingredients must be accompanied by effort to improve the quality of raw

materials use in extract.

Materials and Methodology :

1.Bees Wax:

Biological Source: Beeswax is a naturally occurring wax produced in the bee's hives by
honeybees A. mellifera.

Family: Apidae.

Chemical constituents: The main chemical constituents are carbon (73.3%), hydrogen
(13.2%) and oxygen (7.5%).

It is an agent thickening. Melting point: between 62 and 64 degrees C. The material that gives
a honeycomb its structure is beeswax. In order to create honeycomb to store their honey,
these wax transform nector into wax. Bee wax aids in keeping skin hydrated. Bee wax is a
common ingredient in cosmetics. The properties and amount of waxes determine the gloss
and hardness in most cases.
2.Coconut Oil:

Biological Source: It is oil expressed from the dried solid part of endosperm of coconut,
Cocos nucifera L.

Family: Palmae.

Chemical constituents: It is composed of the fatty acids, caprylic acid C-8:0 (8%), capric
acid C-10:0 (7%), lauric acid C-12:0 (49%), myristic acid C-14:0 (8%), palmitic acid C-16:0
(8%), stearic acid C-18:0 (2%), oleic acid C-18:1 (6%) and 2% of C-18:2 linoleic acid.

It shields skin from UV radiation. It eases irritability. It has a moisturizing purpose. Because
the molecules in coconut oil are so small—nearly as small as the molecules in essential oils—
it can easily permeate the skin and facilitate the easy absorption of essential oils when mixed
with it. It efficiently removes dead skin, heals blisters and sunburns, and encourages the
development of new, healthier skin for a radiant complexion.

3.Olive Oil:

Biological source: It is a liquid fat obtained from olives (the fruit of Olea europaea), a
traditional tree crop of the Mediterranean basin, produced by pressing whole olives and
extracting the oil.
Family: Oleaceae.

Chemical constituents: It is composed mainly of triacylglycerols and contains small

quantities of free fatty acids, glycerol, phosphatides, pigments, and sterols.

It keeps the moisture on your lips. its alleviation of chapped and cracked lips. It provides
organic SPF defense. It was utilized to revitalize your skin and eliminate dead skin from your
lips. It feeds the lips.Olive oil is a great moisturizer and a common component in many skin
conditioning products, but it might make you think more of pizza and roasted garlic than lip
balm.

4.Castor Oil:

Biological Source: - It is non-volatile fatty oil obtained from the seeds of the castor bean,
Ricinus communis.

Family: Spurges

Chemical constituents: It is mainly composed of fatty acids and neutral lipids.

It has laxative properties. It has a moisturizing purpose. It might encourage cracked lips to
mend. It helps one stay hydrated. It offers gentle hydration without any negative side effects.
ideal for using as an all-natural remedy to chapped lips and cuticles.
5.Cocoa Powder:

Biological source: It is powder obtained from the beans of tree of Theobroma cacao.

Family: Malvaceae

Chemical constituents: 58% carbohydrates, 14% fat, 20% protein, and 3% water.

In addition to having an amazing scent, Wildly Organic Raw Cacao Powder provides your
lips with a healthy dosage of flavanols and polyphenols to help smooth and moisturize your
skin. Antioxidants included in cacao may help rejuvenate your skin and shield it from aging
symptoms.
6.Rose essence:

Biological source: Rose oil is made from the flowers of R. damascena, R. centifolia or other
species. It is made by distilling fresh flowers.

Family: Rosaceae.

Chemical constituents: The principal constituents of the oil are citronellol (34–55%),
geraniol, (around 14%) and nerol (around 7%).

It is used as flavouring agent in herbal lipstick.

7.Vitamin E:

Biological source: Vitamin E is found in plant-based oils, nuts, seeds, fruits, and vegetables.

Family: The Vitamin E family consists of four tocopherols and four tocotrienols.

Chemical constituents: Tocopherol, as a group, is composed of soluble phenolic

compounds that consist of a chromanol ring and a 16-carbon phytyl chain.

They present strong antioxidant activities. It has humectant properties that hydrate, and
emollient properties, which support the skin barrier.
Ingredients used for herbal lipstick:

Sr.No Ingredients Formulation Batches

B1 B2 B3 B4
1. Bees Wax 2gms 4gms 3gms 4gms

2. Coconut Oil 3ml 4ml 4.5ml 2ml

3. Olive Oil 3ml 4ml 3ml 2ml
4. Castor Oil 3ml 4ml 3ml 2ml
5. Cocoa 5gms 5gms 6gms 4gms
Powder

6. Rose Essence qs qs qs qs

7. Vitamin E qs qs qs qs
Formulation Method:

1. The herbal lipstick was formulated as per general method of lipstick formulation.
2. In this formulation, bees wax, coconut oil, olive oil, were melted in porcelain dish on
water bath with decreasing order of their melting point.
3. Edible coloring matter like cocoa powder mixed with Castor oil and heated. Both
phases were mixed at same temperature.
4. Rose essence were added at 35°C. Then mixture was poured into lipstick mould in
excess amount and mould was kept in room temperature.
5. After solidification lipstick is removed from the moulds.
Formulation Related Problems :

1.Sweating
It is the most common problem of lipstick formulation due to high oil content or inferior oil
binding. It may rise in any climate or temperature range.
2.Bleeding
This refers to the separation of colored liquids from the waxy base.
3.Streaking
A thin line or band of a different colour or a substance appears on the finished product.

Moulding Related Problems :

1.Laddering
Lipstick does not look smooth or homogenous after congealing and setting but instead has a
multi-layered appearance.
2.Deformation
This is a molding problem where the shape of the lipstick looks deformed. It is noticeable and
appears on both sides of the lipstick.
3.Cratering
This appears in split moulding and it shows up flaming when stick develops dimples.
4.Mushy Failure
This is a problem in which the central core of the lipstick lacks structure and breaks.
Evaluation Parameters Of Herbal Lipstick:

1.Surface anomalies
This was studied by the surface defects, such as no formation crystals on surfaces, no
contamination by moulds, fungi etc.
2.Aging stability
The product was stored in 40ºC at 1 hr. Various parameters such as bleeding, crystallization
of on surface and ease of application were observed.
3.Solubility test
The formulation herbal lipstick was dissolved in various solvents to observe the solubility
like acetone, hexane, water, alcohol, chloroform.
4.pH parameter
The pH of formulated herbal lipstick was determined using pH Paper.
5.Skin irritation test
It is carried out by applying product on the skin for 10 min.
6.Perfume stability
The formulation herbal lipstick was tested after 30 days, to record the fragrance.
Sr.No. Parameter Herbal Marketed Standard
Lipstick Formulation Values
Formulation
1. Colour Coffee Brown Brown -

2. Texture Smooth Smooth Smooth

3. pH 6.3 6.6 6.4

4. Melting point 60-64°C 62-64°C 60-66°C

5. Breaking point 250gm 140gm -

6. Softening point 60°C 62°C 50-60°C

7. Surface anamolies No defects No defects No defects

8. Aging Stability Smooth Smooth Smooth

9. Perfume Stability +++ +++ +++

 Discussion:

In last few decades there has been tremendous boost in use of cosmetics by women.
However, the hazards cause by these chemicals has come into limelight very recently. The
present work formulation and evaluation of herbal lipsticks was aimed to formulate a lipstick
using herbal ingredients with a hope to minimize the side effects as produced by the available
synthetic ones.
Hence, from present investigation it was concluded that this formulated herbal
lipstick has better option to women with minimal side effects though a detailed clinical trials
may be done to access the formulation for better efficacy.
 Result:

There has been enormous increase in women's use of cosmetics over the last
few decades. The hazards caused by these chemicals, however, have recently come
to the forefront. The goal of the present research formulating and evaluating herbal
lipsticks was to formulate a lipstick using herbal ingredients with the hope of
minimizing the side effects caused by the synthetic ones available. Therefore, from
the present investigation it has been concluded that this formulated herbal lipstick
has a better choice for women with limited side effects although a thorough clinical
trial can be performed for better efficacy to access the formulation.
 CONCLUSION:

The study came to the conclusion that a variety of natural

components, including castor oil, coconut oil, olive oil, and bees wax, may be successfully
used to create herbal lipstick. Because synthetic coloring compounds have various adverse
effects, cocoa powder is a better natural colorant option than rose oil, which is utilized for
perfume or smell. Following extensive clinical research, consumers can safely and effectively
benefit from this herbal lipstick.
There are various types of benefits of
herbal lipstick as follows:
 Nontoxic
 Improved blood circulation
 Nourishes the lips
 Helps to eliminate the wrinkles, cracking, dryness, and folds on the lips.
 Provide cooling effect on lips
These all are the essential benefits of our herbal lipstick and its formulation
The prepared formulation was evaluated and it was found that the herbal lipstick
batch B 3 was best among 4 batches.
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