DEPARTMENT OF CHEMICAL ENGINEERING

ANNA UNIVERSITY, CHENNAI

Vision:

To be globally recognized programme and to function as a catalyst in providing outstanding

education. To develop Engineers who will excel in academia, industry, research, and to
strive for sustainable technologies and societal needs.

Mission:
1. To disseminate high-quality Chemical Engineering Education.
2. To develop quality engineers and technocrats with inter-disciplinary skills.
3. To collaborate with industries for innovative concepts/ideas.
4. To perform high-impact research for the benefit of society.

1
 ANNA UNIVERSITY: : CHENNAI: 600 025
UNIVERSITY DEPARTMENTS
M. TECH. CHEMICAL ENGINEERING
REGULATIONS – 2023
CHOICE BASED CREDIT SYSTEM

1. PROGRAMME EDUCATIONAL OBJECTIVES (PEOs)

To develop, analyze, and solve critical chemical engineering problems, and to pursue
I.
advanced study or research.
Design and evaluation of technical concepts to produce new products and answers to
II.
real-world challenges.
III. To work in groups on multidisciplinary projects and in a diversified professional context.
IV. Sustained knowledge on skill development and industrial needs.
Deliver sustainable solutions to chemical engineering challenges to meet the needs of
V.
industry and society on a global scale.

2. PROGRAMME OUTCOMES (POs)

PO PROGRAMME OUTCOMES
PO1 Ability to independently carry out research/investigation and development work to
solve practical problems
PO2 Ability to write and present a substantial technical report/document
Able to demonstrate a degree of mastery over the area as per the specialization
PO3 of the programme. The mastery shall be at a level higher than the requirements in
the appropriate bachelor programme.
PO4 Professional development in the design, modelling, simulation, and optimization of
chemical products and processes.
PO5 Plan and perform experiments, analyse data, interpret for finding optimal solutions.
PO6 Attainment of a scholastic approach to higher education, work, and entrepreneurship.

3. MAPPING OF PROGRAMME EDUCATIONAL OBJECTIVE WITH PROGRAMME

OUTCOMES
PROGRAMME PROGRAMME OUTCOMES
EDUCATIONAL
PO1 PO2 PO3 PO4 PO5 PO6
OBJECTIVES
I. 3 2 1 2 3 2
II. 3 1 3 2 1 1
III. 1 2 1 2 2 1
IV. 1 1 2 2 2 3
V. 1 1 1 2 3 3

2
1. PROGRAMME ARTICULATION MATRIX
PO PO PO PO PO PO
YEAR SEMESTER COURSE NAME
1 2 3 4 5 6
Advanced Numerical
3 - 3 3 2 2
Methods
Research Methodology
3 3 1 - - -
and IPR
Advanced Transport
3 1 3 3 2 1
Phenomena
Advanced Reaction
I 3 3 2 2 1 2
Engineering
Advanced Process
2.38 1.63 2.75 3 2.5 1.5
Control
Chemical Process
3 3 1.4 3 2.8 3
Design
Program Elective I
I Program Elective II
Separation Processes 2 1.5 1.63 1.88 1.5 2.13
Software applications in
1.8 2.4 2.8 3 2.8 -
Chemical Industries
Advanced
Thermodynamics for 2.8 3 3 3 3 1.6
Chemical Engineers
II
Chemical Process 3 1 2 3 3 1.2
Optimization
Program Elective III
Program Elective IV
Mini Project with
3 3 3 3 2 1
Seminar

Modeling of Chemical
3 2 3 3 2 1
Processes
Program Elective V
III
Program Elective VI
Program Elective VII
Project Work I 3 3 3 3 3 3
II

IV Project Work II 3 3 3 3 3 3

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively.

3
 ANNA UNIVERSITY, CHENNAI
UNIVERSITY DEPARTMENTS
M. TECH. CHEMICAL ENGINEERING
REGULATIONS – 2023
CHOICE BASED CREDIT SYSTEM
I TO IV SEMESTERS CURRICULA & SYLLABI

SEMESTER I
S. COURSE PERIODS TOTAL
NO. CODE COURSE TITLE CATEGORY PER WEEK CONTACT CREDITS
L T P PERIODS
THEORY
1. MA3155 Advanced Numerical Methods FC 4 0 0 4 4
2. RM3151 Research Methodology and RMC
2 1 0 3 3
IPR
3. CL3101 Advanced Transport PCC
3 0 0 3 3
Phenomena
4. CL3102 Advanced Reaction PCC
3 0 0 3 3
Engineering
5. CL3103 Advanced Process Control PCC 2 0 2 4 3
6. CL3104 Chemical Process PCC
3 0 0 3 3
Design
7. Professional Elective I PEC 3 0 0 3 3
8. Professional Elective II PEC 3 0 0 3 3
TOTAL 23 1 2 26 25

SEMESTER II

S. COURSE PERIODS TOTAL

NO. CODE COURSE TITLE CATEGORY PER WEEK CONTACT CREDITS
L T P PERIODS
THEORY
1. CL3201 Separation Processes PCC 2 0 2 4 3
2. CL3202 Software Applications in PCC 2 0 2 4 3
Chemical Industries
3. CL3203 Advanced Thermodynamics PCC 3 0 0 3 3
for Chemical Engineers
4. CL3204 Chemical Process PCC 3 0 0 3 3
Optimization
5. Professional Elective III PEC 3 0 0 3 3
6. Professional Elective IV PEC 3 0 0 3 3
PRACTICALS
7. CL3211 Mini Project with Seminar EEC 0 0 2 2 1
TOTAL 16 0 6 22 19

4
 SEMESTER III
S. COURSE PERIODS TOTAL
NO. CODE COURSE TITLE CATEGORY PER WEEK CONTACT CREDITS
L T P PERIODS
THEORY
1. CL 3301 Modelling of Chemical PCC 3 1 0 4 4
Processes
2. Professional Elective V PEC 3 0 0 3 3
3. Professional Elective VI PEC 3 0 0 3 3
4. Professional Elective VII PEC 3 0 0 3 3
PRACTICALS
5. CL3311 Project Work I EEC 0 0 12 12 6
TOTAL 12 1 12 25 19

SEMESTER IV
S. COURSE PERIODS TOTAL
NO. CODE COURSE TITLE CATEGORY PER WEEK CONTACT CREDITS
L T P PERIODS
PRACTICALS
1. CL3411 Project Work II EEC 0 0 24 24 12
TOTAL 0 0 24 24 12

TOTAL CREDITS: 75

FOUNDATION COURSES (FC)

S. COURSE PERIODS PER WEEK

COURSE TITLE CREDITS
NO CODE Lecture Tutorial Practical
1. MA3155 Advanced Numerical Methods 4 0 0 4
TOTAL CREDITS 4

LIST OF PROFESSIONAL CORE COURSES (PCC)

PERIODS PER WEEK

S. COURSE
COURSE TITLE CREDITS
NO CODE Lecture Tutorial Practical
CL3101 Advanced Transport
1. 3 0 0 3
Phenomena
CL3102 Advanced Reaction
2. 3 0 0 3
Engineering
3. CL3103 Advanced Process Control 2 0 2 3
4. CL3104 Chemical Process Design 3 0 0 3
5. CL3201 Separation Processes 2 0 2 3
CL3202 Software applications in
6. 2 0 2 3
Chemical Industries
CL3203 Advanced Thermodynamics for
7. 3 0 0 3
Chemical Engineers

5
 CL3204 Chemical Process
8. 3 0 0 3
Optimization
CL 3301 Modelling of Chemical
9. Processes 3 1 0 4

TOTAL CREDITS 28

PROFESSIONAL ELECTIVE COURSES

S. COURSE PERIODS PER TOTAL
NO. CODE COURSE TITLE CATEGORY WEEK CONTACT CREDITS
L T P PERIODS
1. Biochemical PEC
CL3001 3 0 0 3 3
Engineering
2. CL3002 Waste to Energy PEC 3 0 0 3 3
3. Membrane Separation PEC
CL3003 3 0 0 3 3
Processes
4. CL3053 Fluidization Engineering PEC 3 0 0 3 3
5. Multicomponent PEC
PP3251 3 0 0 3 3
Distillation
6. CL3004 Nanocomposites PEC 3 0 0 3 3
7. Thermal processing of PEC
CL3005 3 0 0 3 3
food Products
8. CL3006 Bioprocess Technology PEC 3 0 0 3 3
9. Computational Fluid PEC
CL3051 3 0 0 3 3
Dynamics
10. CL3052 Design of Experiments PEC 2 0 2 4 3
11. CL3055 Sustainable
PEC 3 0 0 3 3
Management
12. PP3051 Multiphase flow PEC 3 0 0 3 3
13. Polymer Processing
CL3056 PEC 3 0 0 3 3
Technology
14. CL3007 Business Analytics PEC 3 0 0 3 3
15. Chemical Processes
CL3008 PEC 3 0 0 3 3
and Pollution Control
16. Risk Analysis and
CL3009 PEC 3 0 0 3 3
Management
17. Project Engineering of
CL3010 PEC 3 0 0 3 3
Process Plants
18. CL3011 Operations Research PEC 3 0 0 3 3
Safety and Environment
19. CL3012 PEC 3 0 0 3 3
in Chemical Industries
Biomass Conversion
20. CL3013 PEC 3 0 0 3 3
Techniques
Electrochemical
21. EV3051 Environmental PEC 3 0 0 3 3
Technology
Industrial PEC
22. CL3054 3 0 0 3 3
Instrumentation
Piping and
23. PP3052 PEC 3 0 0 3 3
Instrumentation

6
 RESEARCH METHODOLGY AND IPR COURSES (RMC)

S. COURSE PERIODS PER WEEK

COURSE TITLE CREDITS
NO CODE Lecture Tutorial Practical
1. RM3151 Research Methodology and 2 1 0 3
IPR

LIST OF EMPLOYABILITY ENHANCEMENT COURSES (EEC)

S. COURSE PERIODS PER WEEK

COURSE TITLE Lecture Tutorial Practical CREDITS
NO CODE
1. CL3211 Mini Project with Seminar 0 0 2 1
2. CL3311 Project Work I 0 0 12 6
3. CL3411 Project Work II 0 0 24 12
TOTAL CREDITS 19

SUMMARY

Name of the Programme: M.Tech. Chemical Engineering

SUBJECT AREA CREDITS PER SEMESTER CREDITS TOTAL

I II III IV
1. FC 4 - - - 4
2. PCC 12 12 4 - 28
3. PEC 6 6 9 - 21
4. RMC 3 - - - 3
5. EEC - 1 6 12 19
6. TOTAL CREDIT 25 19 19 12 75

7
MA3155 ADVANCED NUMERICAL METHODS L T P C
4 0 0 4
OBJECTIVES:
 To make the students understand the methods/algorithms to numerically solve a system of
simultaneous algebraic equations.
 To make the students understand the methods to numerically solve the system of
simultaneous ordinary differential equations.
 To make the students understand the methods to numerically solve the partial differential
equations.
 To make the students understand the methods to numerically solve the elliptic equations.
 To make the students understand the finite element methods for solving the PDEs.

UNIT I ALGEBRAIC EQUATIONS 12

Systems of linear equations: Gauss Elimination method, pivoting techniques, Thomas
algorithm for tridiagonal system – Jacobi, Gauss Seidel, SOR iteration methods - Systems of
nonlinear equations: Fixed point iterations, Newton Method, Eigenvalue problems: power
method, Faddeev – Leverrier Method.

UNIT II ORDINARY DIFFERENTIAL EQUATIONS 12

Runge Kutta Methods for system of IVPs, numerical stability, Adams-Bashforth multistep method,
solution of stiff ODEs, shooting method, BVP: Finite difference method, collocation method,
orthogonal collocation method, Galerkin finite element method

UNIT III FINITE DIFFERENCE METHOD FOR TIME DEPENDENT PARTIAL 12

DIFFERENTIAL EQUATION
Parabolic equations: explicit and implicit finite difference methods, weighted average
approximation - Dirichlet and Neumann conditions – Two dimensional parabolic equations – ADI
method; First order hyperbolic equations – method of characteristics, Lax-Wendroff explicit and
implicit methods; numerical stability analysis, method of lines – Wave equation: Explicit scheme-
Stability of above schemes

UNIT IV FINITE DIFFERENCE METHODS FOR ELLIPTIC EQUATIONS 12

Laplace and Poisson’s equations in a rectangular region: Five point finite difference schemes,
Leibmann’s iterative methods, Dirichlet and Neumann conditions – Laplace equation in polar
coordinates: finite difference schemes – approximation of derivatives near a curved boundary
while using a square mesh.

UNIT V FINITE ELEMENT METHOD 12

Partial differential equations – Finite element method - collocation method, orthogonal collocation
method, Galerkin finite element method.
TOTAL: 60 PERIODS
OUTCOMES:
At the end of the course, students will be able to
CO1 Solve numerically system of simultaneous algebraic equations.
CO2 Solve the simultaneous ordinary differential equations (IVP) numerically.
CO3 Solve numerically set of Partial differential equations.
CO4 Solve the set of Elliptic equations numerically.
CO5 Solve the set of PDEs by finite element method.

REFERENCES:
1. Burden. R. L. and Faires. J. D., “Numerical Analysis; Theory and Applications”, India Edition,
Cengage Learning, 2010.
2. Jain M.K., Iyengar S.R.K. and Jain R.K., Computational Methods for Partial Differential
Equations, New Age International, 2nd Edition, New Delhi, 2016.

8
3. Morton K.W., and Mayers D.F., “Numerical Solution of Partial Differential Equations,
Cambridge University Press, Second Edition, Cambridge, 2005.
4. Santosh K Gupta, “Numerical Methods for Engineers”, New Age International (P) Limited,
Publishers, New Delhi, 2014.
5. Sastry S.S., "Introductory Methods of Numerical Analysis", Prentice - Hall of India Pvt.
Limited, 5th Edition, New Delhi, 2012.
6. Saumyen Guha and Rajesh Srivastava, “Numerical methods for Engineering and Science”,
Oxford Higher Education, New Delhi, 2010.
CO-PO Mapping:
PO1 PO2 PO3 PO4 PO5 PO6
CO1 3 3 3 3 2 2
CO2 3 3 3 3 2 2
CO3 3 3 3 3 2 2
CO4 3 3 3 3 2 2
CO5 3 3 3 3 2 2
Avg 3 3 3 3 2 2

RM3151 RESEARCH METHODOLOGY AND IPR LTPC

2103
OBJECTIVES:
To impart knowledge on
 Formulation of research problems, design of experiment, collection of data,
interpretation and presentation of result
 Intellectual property rights, patenting and licensing

UNIT I RESEARCH PROBLEM FORMULATION 9

Objectives of research, types of research, research process, approaches to research;
conducting literature review- information sources, information retrieval, tools for identifying
literature, Indexing and abstracting services, Citation indexes, summarizing the review, critical
review, identifying research gap, conceptualizing and hypothesizing the research gap

UNIT II RESEARCH DESIGN AND DATA COLLECTION 9

Statistical design of experiments- types and principles; data types & classification; data
collection - methods and tools

UNIT III DATA ANALYSIS, INTERPRETATION AND REPORTING 9

Sampling, sampling error, measures of central tendency and variation,; test of hypothesis-
concepts; data presentation- types of tables and illustrations; guidelines for writing the
abstract, introduction, methodology, results and discussion, conclusion sections of a
manuscript; guidelines for writing thesis, research proposal; References – Styles and
methods, Citation and listing system of documents; plagiarism, ethical considerations in
research

UNIT IV INTELLECTUAL PROPERTY RIGHTS 9

Concept of IPR, types of IPR – Patent, Designs, Trademarks and Trade secrets, Geographical
indications, Copy rights, applicability of these IPR; , IPR & biodiversity; IPR development
process, role of WIPO and WTO in IPR establishments, common rules of IPR practices, types
and features of IPR agreement, functions of UNESCO in IPR maintenance.

UNIT V PATENTS 9
Patents – objectives and benefits of patent, concept, features of patent, inventive steps,

9
specifications, types of patent application; patenting process - patent filling, examination of
patent, grant of patent, revocation; equitable assignments; Licenses, licensing of patents;
patent agents, registration of patent agents.
TOTAL: 45 PERIODS
COURSE OUTCOMES
Upon completion of the course, the student can
CO1: Describe different types of research; identify, review and define the research problem
CO2: Select suitable design of experiment s; describe types of data and the tools for
collection of data
CO3: Explain the process of data analysis; interpret and present the result in suitable form
CO4: Explain about Intellectual property rights, types and procedures
CO5: Execute patent filing and licensing

REFERENCES:
1. Cooper Donald R, Schindler Pamela S and Sharma JK, “Business Research Methods”,
Tata McGraw Hill Education, 11e (2012).
2. Soumitro Banerjee, “Research methodology for natural sciences”, IISc Press, Kolkata,
2022,
3. Catherine J. Holland, “Intellectual property: Patents, Trademarks, Copyrights, Trade
Secrets”, Entrepreneur Press, 2007.
4. David Hunt, Long Nguyen, Matthew Rodgers, “Patent searching: tools & techniques”,
Wiley, 2007.
5. The Institute of Company Secretaries of India, Statutory body under an Act of parliament,
“Professional Programme Intellectual Property Rights, Law and practice”, September
2013.

CL3101 ADVANCED TRANSPORT PHENOMENA L T P C

3 0 0 3
OBJECTIVES:
 To impart knowledge on the concepts of transport phenomena and its relationships with
other core chemical engineering subjects.
 To make the students to develop governing equations for complex system in chemical
engineering
 To make the students to learn solution techniques in momentum, energy and mass
transport phenomena.
 To help the students to understand the flow behavior in different systems
 To make the students to develop critical thinking skills, interpret physicochemical
phenomena to and from mathematical expressions.

UNIT I BASIC CONCEPTS 9

Phenomenological Equations and Transport properties, Rheological behavior of fluids, Models
for Rheological Behavior; Balance Equations – Differential and Integral equations

UNIT II APPLICATIONS OF DIFFERENTIAL EQUATIONS OF CHANGE 9

Applications in laminar and turbulent transport in compressible and incompressible fluids,
Boundary layer theory – Momentum, Thermal and Concentration Boundary layer, Similarity
Transformation – Blasius Solution

UNIT III APPLICATIONS OF INTEGRAL EQUATIONS OF CHANGE 9

Reynolds Transport Theorem – application of RTT to solutions for Macroscopic balance for
isothermal and non-isothermal systems and their applications in Momentum, Heat and Mass
transport problems.

10
UNIT IV INTERPHASE AND MULTIPHASE MOMENTUM TRANSFER 9
Friction factor, Fluid Fluid systems, Flow patterns in vertical and horizontal pipes, Formulation
of bubbles and drops and their size distribution, Solid fluid systems, Forces acting on stagnant
and moving solids, Flow through porous medium, capillary tube model and its applications.

UNIT V INTERPHASE TRANSPORT IN NON-ISOTHERMAL SYSTEMS 9

Heat Transfer coefficient, Forced convection in tubes, around submerged objects, Heat
Transfer by free convection, film type and dropwise condensation and equations for heat
transfer, Heat transfer in boiling liquids, Mass Transfer co-efficient in single and multiple
phases at low and high mass transfer rates, Film theory, Penetration theory, Boundary layer
theory, Macroscopic balance to solve steady and Unsteady state problems.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recall Phenomenological Equations, Transport properties and rheological behavior of
fluids.
CO2: Apply differential equation of change for momentum, heat and mass transport problems.
CO3: Apply integral equations of change for momentum, heat and mass transport problems.
CO4: Analyze interphase and multiphase momentum transfer
CO5: Evaluate interphase transport in non-isothermal system and to solve steady and
Unsteady state problems.

REFERENCE BOOKS:
1. Bird, R. B., Lightfoot, E. N., & Stewart, E. W., “Transport phenomenon”, Wiley, 2007.
2. Welty, J.R., Wicks, C. E. and Wilson, R. E., “Fundamentals of Momentum, Heat Mass
Transfer”, 5th Edn., John Wiley and Sons, 2007
3. Deen, W. M., “Analysis of Transport Phenomena”, Topics in Chemical Engineering (Vol.
Oxford University Press, New York. 1998.
4. Leal, L. G., “Advanced transport phenomena: fluid mechanics and convective transport
processes”, (Vol. 7). Cambridge University Press, 2007.
5. Brodkey, R. S., and Hershey, H. C., “Transport phenomena: a unified approach”, Brodkey
publishing, 2003.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recall Phenomenological Equations, 3 1 3 3 2 1
Transport properties and rheological
behavior of fluids.
CO2 Apply differential equation of change for 3 1 3 3 2 1
momentum, heat and mass transport
problems.
CO3 Apply integral equations of change for 3 1 3 3 2 1
momentum, heat and mass transport
problems.
CO4 Analyze interphase and multiphase 3 1 3 3 2 1
momentum transfer
CO5 Evaluate interphase transport in non- 3 1 3 3 2 1
isothermal system and to solve steady and
Unsteady state problems.
Average CO 3 1 3 3 2 1

11
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3102 ADVANCED REACTION ENGINEERING L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to Analyze the different types of models and kinetics of non-catalytic
reaction.
 To enable the students to Determine the properties of catalyst and understand catalytic
deactivation mechanism.
 To enable the students to Understand to write the kinetic expression for catalytic reactions.
 To enable the students to Understand the mass and heat transport process in catalyst.
 To enable the students to Understand the modelling of the reactors.

UNIT I GAS SOLID NON-CATALYTIC REACTIONS AND REACTORS 9

Reaction kinetics, Different models used for gas solid non-catalytic reactions, shrinking core
model, volume reaction model, zone models, grain models, rate controlling steps; time for
Complete Conversion for Single and Mixed Sizes, design of gas solid reactors.

UNIT II GAS SOLID CATALYTIC REACTION 9

Steps in catalytic reaction, Single site, dual site mechanisms, Langmuir Hinshelwood, Eley
Rideal, Rate controlling steps. Experimental methods for determining rate. Intra particle
diffusion mechanism of catalytic reactions- under isothermal and non-isothermal condition.

UNIT III FLUID-FLUID REACTION 9

Kinetics and design of Fluid‐Fluid Reactions. Rate equation, Kinetic regimes for absorption
combined with chemical reaction. Various cases of mass transfer with chemical reaction,
Factors to select the contactor, gas-liquid reactor design, liquid-liquid reactors and Design.

UNIT IV ADVANCED REACTOR SYSTEMS 9

Conventional reactors, advanced reactors– Static mixer reactor, Monolith Reactors, Spinning
disc reactor, Multifunctional Reactors– Reactive distillation, Reactive extraction, Membrane
reactor; Solar reactors, Micro channel reactors.

UNIT V MODELLING OF CHEMICAL REACTOR SYSTEMS 9

Steady state and unsteady state modelling concepts, Modelling batch reactors and tubular
reactors systems, Reactor optimization.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Analyze the various models and kinetics of non-catalytic reaction.
CO2: Evaluate the mechanism of catalytic reaction mechanism.
CO3: Apply the knowledge to evaluate the fluid- fluid reactor tower design
CO4: Distinguish different types of the advanced reactor systems
CO5: Develop different models for the chemical reactors

REFERENCE BOOKS:
1. Dorasiswamy, L.K., Deniz Uner, Chemical Reaction Engineering Beyond the
fundamentals, First edition, CRC Press, 2014
2. Froment, G.F. and Bischoff, K.B., “Chemical Reactor Design and Analysis”, Third
Edition, John Wiley &Sons, New York,2011.
3. S. Suresh S. Sundaramoorthy Green Chemical Engineering: An Introduction To

12
 Catalysis Kinetics And Chemical Processes, First edition CRC Press;,2014
4. Levenspiel, O. Chemical Reaction Engineering, Third Edition, JohnWiley1999
5. H.S.Fogler, Elements of Chemical Reaction Engineering,
ThirdEdition,PrenticeHallofIndia,1999
Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Analyze the various models and 3 2 2 1 2 2
kinetics of non-catalytic reaction.
CO2 Evaluate the mechanism of 3 2 2 1 2 -
catalytic reaction mechanism.
CO3 Apply the knowledge to evaluate 3 2 2 1 2 --
the fluid- fluid reactor tower
design
CO4 Distinguish different types of the 3 2 - 1 2 --
advanced reactor systems
CO5 Develop different models for the 3 2 2 1 2 -
chemical reactors
Average CO 3 3 2 2 1 2

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3103 ADVANCED PROCESS CONTROL L T P C

2 0 2 3
OBJECTIVES:
 To enable the students to learn fundamentals of linear time-varying systems and non-linear
systems
 To make the students aware of different advanced control strategies for various industrial
applications
 To impart students the knowledge on model-based control methods for linear and nonlinear
systems
 To facilitate students the understanding on the dynamics of multivariable systems
 To educate the students on industrial implementation of digital control systems

UNIT I ADVANCED CONTROL STRATEGIES 6

Linear, nonlinear regression fitting for first order, second order models without and with time delay;
development of discrete time model and parameter identification; Advanced control - Feed
forward, cascade, dead time compensation, split range, inferential, selective and override control;
smith predictor; automatic tuning and gain scheduling

UNIT II MODEL BASED CONTROL DESIGN 6

Model based control – IMC structure, development and design; Direct synthesis method; IMC
based PID control, Overview of MPC - prediction for SISO and MIMO models, MPC calculation,
set point calculation, selecting the tuning parameters in MPC, Design examples for typical case
studies; Introduction to Non-linear MPC

UNIT III MULTIVARIABLE CONTROL 6

Control loop interaction – general pairing problem, relative gain array and application, sensitivity;
Multivariable control – zeros and performance limitations, directional sensitivity and operability,
decoupling

13
 UNIT IV DISCRETE SYSTEMS & NON-LINEAR SYSTEMS 6
Z – Transform and inverse Z – transform properties; Discrete – Time Response of dynamic system,
Pulse Transfer Function, Closed Loop System Stability; Models for Time-varying and Nonlinear
systems; Hammerstein and Wiener Systems; Fuzzy logic controls; Neural network control

UNIT V DIGITAL FEEDBACK CONTROLLERS 6

Design of digital feedback controllers - Essential components, Digital control implementation,
Programmable Logic Controller, Distributed Control System, SCADA, Hardware for computer -
based control, Interfacing computer system with process

LIST OF EXPERIMENTS
1. Level control process with data acquisition
2. Temperature control process with data acquisition
3. Flow control process with data acquisition
4. Pressure process trainer with data acquisition
5. Implementation of Model Predictive Control in process control station
6. Implementation of Fuzzy logic, control in process control station
7. PLC and web based real time process control system
8. Integration of process control equipment in COMOS software
9. Create P & ID diagram
10. Simulation of process plant using COMOS software
TOTAL: 60 PERIODS

COURSE OUTCOMES:

CO1: Identify and apply different advanced control configurations for specific
applications
CO2: Compare and understand the capability of model-based control systems
CO3: Analyze the multivariable systems with interaction and its sensitivity
CO4: Gain fundamental knowledge on Z transform to analyze discrete systems
CO5: Gain exposure on the implementation of digital control systems

PRACTICAL
CO6: Implement PLC based control of a process
CO7: Implement Model Predictive control of a process
CO8: Implement PLC and webserver based real time process control
REFERENCE BOOKS:
1. Bequette, B. W., “Process Control: Modeling, Design, and Simulation”, Prentice Hall, 2003
2. Stephanopoulos G., “Chemical Process Control”, 1st ed., Pearson Education India, New
Delhi, 2015.
3. Kannan M. Moudgalya, “Digital Process Control”, John Wiley & Sons Ltd,2007
4. W L Luyben, “Process Modeling Simulation & Control for Chemical Engineers”, McGraw
Hill Education, 2nd edition, 2013
5. Seborg D.E., Edgar, T. F., Mellichamp D.A., “Process Dynamics and Control”, 3rd ed.,
Wiley India, New Delhi, 2013.
Course Articulation Matrix

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Identify and apply different
2 1 1 3 2 1
advanced control

14
 configurations for specific
applications
CO2 Compare and understand the
capability of model-based 1 1 3 3 1 1
control systems
CO3 Analyze the multivariable
systems with interaction and 2 2 3 3 3 1
its sensitivity
CO4 Gain fundamental knowledge
on Z transform to analyze 2 1 3 3 2 1
discrete systems
CO5 Gain exposure on the
implementation of digital 3 2 3 3 3 2
control systems
CO6 Implement PLC based control
3 2 3 3 3 2
of a process
CO7 Implement Model Predictive
3 2 3 3 3 2
control of a process
CO8 Implement PLC and
webserver based real time 3 2 3 3 3 2
process control
Average CO 2.38 1.63 2.75 3 2.5 1.5

CL3104 CHEMICAL PROCESS DESIGN L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to learn individual aspects of chemical plant design, optimization
and
 To enable the students to understand the hierarchy of analysis and decisions in chemical
process design
 To impart knowledge on the synthesis methods for chemical process and its alternatives
 To enable the students to integrate the unit processes and energy networks
 To impart knowledge on various process loops and optimization

UNIT I THE NATURE OF CHEMICAL PROCESS DESIGN AND INTEGRATION 9

Process design development; process comparison; formulation of design problem - the
hierarchy and approaches of chemical process design, economics, health, safety hazards and
integration.

UNIT II DESIGN OF REACTORS 9

Types of reaction systems; design of idealized reactors; reactor performance; reactor
conditions and reactor configuration.

UNIT III DESIGN OF SEPARATION SYSTEM 9

Separation systems introduction - choice of separator for homogeneous fluid mixtures, choice
of separator for heterogeneous fluid mixtures; distillation sequencing; adsorption - Pressure
swing, thermal swing.

UNIT IV ENERGY INTEGRATION AND HEAT EXCHANGER NETWORK SYNTHESIS 9

Heat exchanger networks design; energy target – pinch technology; heat recovery systems -
composite curves, problem table algorithm.

15
 UNIT V RECYCLE SYSTEMS FOR CONTINUOUS AND BATCH PROCESS 9
Functions of process Recycles in continuous and batch processes; process Yield; optimization
of recycle loop in continuous and batch process.
TOTAL: 45 PERIODS

COURSE OUTCOMES:
CO1: Recognize various aspects of process design project objectives, approaches of
process design.
CO2: Classify various choice of reactors and its performance assessment, reactor
configuration
CO3: Formulate design of different types of separations process for homogeneous and
heterogeneous mixtures.
CO4: Apply types of Heat exchanger networks for the target of energy and costs.
CO5: Analyze Recycle systems in order to optimize the process

REFERENCE BOOKS:
1. Smith, R., “Chemical Process: Design and Integration”, John Wiley and Sons, UK, 2005.
2. Peters, Max S., Timmerhaus K.D., and West R.E., “Plant Design and Economics for
Chemical Engineers”, 5th Ed., McGraw-Hill International Editions (Chemical Engineering
Series), New York, 2003.
3. Silla.H., “Chemical Process Engineering(Design and Economics)”, Taylor and Francis
Group LLC,USA, 2003.
4. Douglas, James M., “Conceptual Design of Chemical Processes”, McGraw-Hill
International Editions ( Chemical Engineering Series), New York, 1988.
5. Robert E. Treybal, “Mass Transfer Operations”, 3rd Ed., McGraw-Hill International
Editions, Singapore, 1981.
6. Xian Wen Ng, “Concise Guide to Heat Exchanger Network Design”, Springer Nature
Switzerland AG, 2021.
7. Xing Luo, Wilfried Roetzel, Dezhen Chen, “Design and Operation of Heat Exchangers
and their Networks”, 1st Ed. Academic Press. 2019.
Course Articulation Matrix:
Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recognize various aspects of process 3 3 1 3 2 3
design project objectives, approaches of
process design.
CO2 Classify various choice of reactors and its 3 3 1 3 3 3
performance assessment, reactor
configuration
CO3 Formulate design of different types of 3 3 1 3 3 3
separations process for homogeneous
and heterogeneous mixtures.
CO4 Apply types of Heat exchanger networks 3 3 1 3 3 3
for the target of energy and costs.
CO5 Analyze Recycle systems in order to 3 3 3 3 3 3
optimize the process
Average CO 3 3 1.4 3 2.8 3
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

16
CL3201 SEPARATION PROCESSES L T P C
2 0 2 3
OBJECTIVES:
 To impart knowledge on recently developed unit operations like membrane separation,
adsorption, Chromatography, supercritical fluid extraction and advanced distillation
techniques.
 To acquaint the students with various types of contacting systems viz. liquid-liquid, solid-
liquid, gas-solid with their technical insights.
 To impart knowledge on theoretical and practical insight of advanced separation
techniques.
 To make the students understand the utilization of soft wares for the design of membrane
and distillation units.
 To enable the students to select appropriate separation methodology for an intended
application.

UNIT I MEMBRANE SEPARATION PROCESSES 6

Membrane types, materials, synthesis and characterization; Different membrane modules;
Working principle, operating parameters, membranes used, transport processes/mechanisms
and industrial applications for individual membrane processes such as Reverse osmosis,
nanofiltration, ultrafiltration, microfiltration; MBR; Reverse Osmosis process design using
software

UNIT II ADSORPTION AND ION EXCHANGE 6

Fundamentals and types of adsorption, Types and properties of adsorbents, Adsorption
Equilibrium and isotherms, stage contact operations, Fixed bed adsorption; Ion Exchange -
Fundamentals of Ion Exchange Types of Ion Exchange Resins Theory of Ion Exchange,
Applications - Removal and recovery of heavy metals, Removal of nitrogen, Removal of
phosphorus, Organic chemical removal

UNIT III CHROMATOGRAPHIC SEPARATION 6

Principle and operation, Types of chromatography - Ion exchange chromatography, Gel
filtration and affinity chromatography, Thin layer and paper chromatography, Liquid
chromatography, Simulated Moving bed chromatography, Multicomponent Differential
Chromatography; Advantages and disadvantages of chromatographic separations.

UNIT IV SUPERCRITICAL EXTRACTION 6

Working Principal, unique properties and solubility behavior of supercritical fluids, Advantages
of supercritical extraction, Decaffeination, ROSE process for purification of crude oil,
hydrothermal oxidation, and Commercial applications of supercritical extraction

UNIT V ADVANCED DISTILLATION TECHNIQUES 6

Reactive and catalytic distillation Concept, advantage & disadvantages, Structured packing
and its comparison with conventional techniques, Concept & working of short path Distillation
Unit (SPDU)
TOTAL: 30 PERIODS
COURSE OUTCOMES:
CO1: Design and develop membrane system for the determination of flux.
CO2: Discuss fixed bed column (Adsorption / Ion Exchange) for the separation of
component from the system of fluids.
CO3: Apply chromatographic techniques.
CO4: Interpret simple phase diagrams and judge their implication in the design of a
supercritical fluid process.
CO5: Assess and optimize advanced distillation techniques.
Practical

17
CO6: Recall and apply foundational concepts in real membrane system
CO7: Demonstrate column studies for the separation of components
CO8: Optimize the results

REFERENCE BOOKS:
1. J.D. Seader and E.J. Henley, “Separation Process Principles”, John Wiley & Sons, 1998.
2. B. K. Dutta, “Principles of Mass Transfer and Separation Processes”, Prentice Hall India
Learning Private Limited, 2006.
3. Baker, R. W., “Membrane technology and applications”, John Wiley & Sons, 2012.
4. C.J. Geankoplis, “Transport Processes and Separation Process Principles”, Prentice
Hall India Learning Private Limited, 2004.
5. Wankat, P. C., “Separation process engineering”, Pearson Education, 2006.

LIST OF EXPERIMENTS 30
1. Determination of the water permeability of a given polymeric membrane.
2. Determination of permeation flux of a membrane in flat-sheet module (Dye-water
solution may be used as feed) (RO/NF/UF membranes can be used)
3. Numerical/design of reverse osmosis process using software.
4. Waste Water Treatment using MBR.
5. Adsorption Equilibrium and fixed bed adsorption studies for generation of breakthrough
curves
6. Determination of ion exchange capacity of a given cation or anion exchanger
7. To separate a mixture of dyes using chromatography
8. Experimental design in supercritical fluid extraction
9. Study of extraction efficiency for the extraction of essential oils
10. Numerical/design assignment based on reactive and catalytic distillation.
TOTAL: 60 PERIODS

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Design and develop membrane 3 3 3 3 3 3
system for the determination of flux.
CO2 Discuss fixed bed column 3 3 3 3 3 3
(Adsorption / Ion Exchange) for the
separation of component from the
system of fluids.
CO3 Apply chromatographic techniques. 3 3 3 3 3 3
CO4 Interpret simple phase diagrams and 3 3 3 3 3 3
judge their implication in the design
of a supercritical fluid process.
CO5 Assess and optimize advanced 3 3 3 3 3 3
distillation techniques.
Practical
CO6: Recall and apply foundational 3 2 3 3 3 3
concepts in real membrane system
CO7: Demonstrate column studies for the 2 2 1 2 2 3
separation of components
CO8: Optimize the results 1 2 1 2 2 3
Average CO 2 1.5 1.63 1.88 1.5 2.13

18
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3202 SOFTWARE APPLICATIONS IN CHEMICAL INDUSTRIES L T P C

2 0 2 3
OBJECTIVES:
 To enable the students to learn about python language with its application.
 To impart knowledge about Microsoft-excel for solving various chemical engineering
 To enable the students to learn about the role of MATLAB in various chemical industries
and its applications
 To impart knowledge on ASPEN and its application in various chemical industries
 To enable the students to learn about HYSYS and its application in chemical and
petroleum refining industries

UNIT I PYTHON FOR PROCESS ENGINEERS 6

Introduction – variable and identifiers; Arithmetic operators – conditionals – If else loop, while
loop, for loop – function cell ; simple data structure in python – strings, dictionaries & modules
; File handling. Exercises can be generalized.

UNIT II MICROSOFT EXCEL FOR CHEMICAL THERMODYNAMICS 6

Application in Density, molecular weight, mole and percentage compositions; Empirical and
Molecular formula calculations, Heat of mixing, Gas laws, Vapor pressure, and Chemical
Kinetics calculations; Application in data processing- Statistical analysis of data and
Regression. Analysis of variance, Interpolation, and Graphical representations of various
Chemical Engineering problems; Interfacing with different soft-wares for data transfer and job
applications Exercises can be generalized.

UNIT III MATLAB FOR NUMERICAL APPLICATIONS 6

Introduction to MATLAB, workspace environment, variable and data entry, matrix operations;
MATLAB functions, Programming in MATLAB to solve Chemical engineering problems;
Introduction to Simulink Exercises can be generalized.

UNIT IV ASPEN FOR PROCESS INDUSTRIES 6

Introduction to ASPEN, application of ASPEN in chemical engineering problems; simulation of
Individual process equipment and flow sheet using Aspen Plus, property analysis and
estimation using Aspen Properties Exercise can be generalized.

UNIT V HYSYS FOR SIMULATION IN PROCESS INDUSTRIES 6

Introduction to HYSYS, process modelling and simulation using HYSYS, design performance
monitoring using HYSYS, application of HYSYS in petroleum industries, case studies,
Chemical Engineering Problems using HYSYS. Exercise can be generalized.
TOTAL: 60 PERIODS
List of Exercises: 30
1. Write a python program for temperature conversion from oC To oF
2. Write a python program to determine the excess oxygen supplied for combustion
3. Determine the molar volume and compressibility factor using Goal Seak
4. Determine the three-phase bubble point using Solver
5. Determine the terminal velocity using Goal Seek
6. Write a MATLAB program to calculate the vapor pressure of water according to
Antoine equation: logP=(A-B/(T+C))
Where T is any given temperature in Kelvin and A, B, and C are Antoine coefficients:
A=18.3036,B=3816.44,C= -46.13.

19
 7. Write a MATLAB program to solve this problem using Runge-Kutta 4 order equation
8. Problem: Distillation: A mixture containing 50.0 wt% acetone and 50.0 wt% water is
to be separated into two streams – one enriched in acetone and the other in water.
The separation process consists of extraction of the acetone from the water into
methyl isobutyl ketone (MIBK), which dissolves acetone but is nearly immiscible with
water. The overall goal of this problem is to separate the feed stream into two streams
which have greater than 90% purity of water and acetone respectively.
9. Problem: Flash separation: A stream containing 15% ethane, 20% propane, 60% i-
butane and 5% n-butane at 50°F and atmospheric pressure, and a flow rate of 100
lbmole/hr. This stream is to be compressed to 50 psia, and then cooled to 32°F. The
resulting vapor and liquid are to be separated as the two product streams. What are
the flow rates and compositions of these two streams?

COURSE OUTCOMES:
CO1: Recognize the various software’s used in chemical engineering industries and learn
about C and C++ language with its application
CO2: Solve various chemical engineering problems using Microsoft excel
CO3: Demonstrate the role of MATLAB in various chemical industries and its applications
CO4: Apply basic knowledge about ASPEN and its application in various chemical
industries
CO5: Evaluate HYSYS and its application in chemical and petroleum refining industries
PRACTICAL
CO6: Analyze chemical engineering problems using python programing and Microsoft
excel
CO7 Using MATLAB and Aspen solve problems based on material balance without
reaction, with reaction and energy balance
CO8 Solve process industry-oriented problems using HYSYS

REFERENCE BOOKS:
1. Hanna, O.T. Scandell, O.C. Computational Methods in Chemical Engineering, Prentice
Hall, 1995.
2. R.K. Taxali, T.K. dBase IV made simple, Tata McGraw-Hill 1991. 80
3. Finlayson, B. A., Introduction to Chemical Engineering Computing, John Wiley & Sons,
New Jersey, 2006.
4. Jerry, O., Breneman, G.L. Spreadsheet Chemistry, Prentice Hall, Englewood Cliffs,
1991.
5. Myers, A.L. Seider W.D. Introduction to Chemical engineering and Computer
Calculations.
6. Reema Thareja, Python programming using problem solving approach, oxford university
press, 2017.
7. Allen B. Downey, Think Python: How to think like a computer scientist, second edition,
shroff/O’Reilly Publishers, 2016.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recognize the various software’s
used in chemical engineering 1 1 2 3 2 -
industries and learn about C and
C++ language with its application

20
 CO2 Solve various chemical 2 2 3 3 3 -
engineering problems using
Microsoft excel
CO3 Demonstrate the role of MATLAB 2 3 3 3 3 -
in various chemical industries
and its applications
CO4 Apply basic knowledge about 2 3 3 3 3 -
ASPEN and its application in
various chemical industries
CO5 Evaluate HYSYS and its 2 3 3 3 3 -
application in chemical and
petroleum refining industries
Practicals
CO6 Analyze chemical engineering 2 3 3 3 3 -
problems using python programing
and Microsoft excel
CO7 Using MATLAB and Aspen solve 2 3 3 3 3 -
problems based on material balance
without reaction, with reaction and
energy balance
CO8 Solve process industry oriented 2 3 3 3 3 -
problems using HYSYS
Average CO 1.8 2.4 2.8 3 2.8 -

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3203 ADVANCED THERMODYNAMICS FOR CHEMICAL ENGINEERS L T P C

3 0 0 3
OBJECTIVES:
 To impart knowledge on the basics of laws of energy relations and partial derivatives
for PVT relations
 To enable the students to understand the thermodynamics of phase equilibria typically
present in design of chemical processes, in particular, in separation operations
 To enable the students to learn about advance Phase and chemical equilibria of multi-
component systems
 To enable the students to learn about molecular thermodynamics to understand the
multi-component interactions
 To enable the students to relate thermodynamic concepts to separation applications,
specifically related to petroleum and chemical process industries.

UNIT I OVERVIEW OF THERMODYNAMICS 9

Thermodynamic Energy Law; Reversibility and second Law; Review of Basic Postulates,
equation of state and its applications, corresponding states, equilibrium criteria, Entropy
calculations ,Legendre Transformation and Maxwell’s relations.

UNIT II FLUID PHASE EQUILIBRIA 9

Phase rule, Stability of thermodynamic systems, first order phase transitions and critical
phenomenon, single component phase diagrams, thermodynamic properties of single phase
and multicomponent system.

21
UNIT III SOLUTION THERMODYNAMICS 9
Partial molar properties, Gibbs-Duhem equation, fugacities in gas and liquid mixtures, activity
coefficients, Ideal and Non-ideal solutions, azeotropes, Excess Functions; Calculation of
vapor liquid equilibria using equations of state; Classical and excess free energy based mixing
rules,Wilson, NRTL, and UNIQUAC equations, UNIFAC method.

UNIT IV VAPOR LIQUID EQUILIBRIA 9

Vapour Liquid Equilibrium involving low pressure, high pressures and multi component
systems, VLE in ideal and non- ideal solutions, Solid‐Liquid Equilibria (SLE); Vapor‐Liquid
Liquid Equilibria(VLLE);Phase Equilibria of Solid‐Solid Mixtures. Applications - Phase
equilibria in polymer solutions, Electrolytes

UNIT V REACTION EQUILIBRIA 9

Criteria of chemical reaction equilibrium in thermodynamic systems, Homogeneous gas and
liquid phase reactions, heterogeneous reactions – phase and chemical equilibrium ,
Introduction to molecular thermodynamics, Intermolecular forces, Potential function
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recall the basic concepts of energy and laws of thermodynamics to applications
that require quantitative knowledge of thermodynamic properties at macroscopic level.
CO2: Review the thermodynamics of phase equilibria for the design of chemical
processes
CO3: Analyze the fundamental property relation and derivative relations and compute the
VLE using excess energy models
CO4: Apply the solution methods for vapor -liquid equilibrium and understand the LLE
and VLLE phase behavior, including the ability to identify the onset of liquid instability
CO5: Assess the influences of pressure, nonstoichiometric feed and inerts on reaction
equilibrium and the Gibbs minimization method for calculating reaction equilibrium.

REFERENCE BOOKS:
1. J. Richard Elliott, Carl T. Lira, a Introductory Chemical Engineering Thermodynamics,
2nd Edition", 2nd edition, Prentice Hall, 2012
2. J.M.Smith, H.C.Van Ness, Michael M. Abbott, Introduction to Engineering
Thermodynamics, McGraw Hill, New York, 2005.
3. M.D. Koretsky, Engineering and Chemical Thermodynamics, 2nd edition, Wiley; 2nd
edition, 2012
4. Prauznitz, J.M., R.N. Lichtenthaler, E.G. de Azevedo, "Molecular Thermodynamics of
Fluid Phase Equilibria", 3rd ed., Prentice Hall, 1999
5. S.M. Walas, Phase Equilibria in Chemical Engineering•, Butterworths, 1985.
6. Y.V.C.Rao, Chemical Engineering Thermodynamics, 2003

Course Articulation Matrix:

Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recall the basic concepts of 3 3 3 3 3 1
energy and laws of
thermodynamics to applications
that require quantitative
knowledge of thermodynamic
properties at macroscopic level.
CO2 Review the thermodynamics of 3 3 3 3 3 1
phase equilibria for the design of
chemical processes

22
 CO3 Analyze the fundamental 3 3 3 3 3 2
property relation and derivative
relations and compute the VLE
using excess energy models
CO4 Apply the solution methods for 2 3 3 3 3 2
vapor -liquid equilibrium and
understand the LLE and VLLE
phase behavior, including the
ability to identify the onset of
liquid instability
CO5 Assess the influences of 3 3 3 3 3 2
pressure, nonstoichiometric feed
and inerts on reaction equilibrium
and the Gibbs minimization
method for calculating reaction
equilibrium.
Average CO 2.8 3 3 3 3 1.6

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3204 CHEMICAL PROCESS OPTIMIZATION L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to learn basics of Optimization.
 To enable the students to learn Formulation of an optimization problem
 To impart knowledge on finding solutions for nonlinear unconstrained optimization.
 To enable the students to understand the role of constraints on the solution of an
optimization problem
 To make the students to explore the optimal and dynamic optimization techniques.

UNIT I INTRODUCTION 9
Introduction to optimization; applications of optimization in chemical engineering; classification
of optimization problems; Problem formulation, degree of freedom analysis, objectives
functions, constraints and feasible region, general procedure for solving optimization
problems, Types of optimization problem, obstacles to optimization.

UNIT II LINEAR PROGRAMMING 9

Introduction to Linear Programming (LP). Graphical representation. Basic assumptions.
Simplex method, Barrier method, sensitivity analysis, Examples.

UNIT III NONLINEAR UNCONSTRAINED OPTIMIZATION 9

Convex and concave functions unconstrained NLP, Newton’s method Quasi-Newton’s
method, Examples.

UNIT IV CONSTRAINED OPTIMIZATION 9

Direct substitution, Quadratic programming, Penalty Barrier Augmented Lagrangian Methods.

UNIT V MULTI OBJECTIVES OPTIMIZATION 9

Weighted Sum of Squares method, Epsilon constrain method, Goal attainment, Examples.
Introduction to optimal control and dynamic optimization.
TOTAL: 45 PERIODS

23
COURSE OUTCOMES:
CO1: Describe the basics problem formulation and optimization.
CO2: Discuss mathematical characteristics of linear programming.
CO3: Explain computational solution techniques for nonlinear unconstrained
optimization.
CO4: Demonstrate various techniques used in constrained optimization
CO5: Apply the optimal and dynamic optimization.

REFERENCE BOOKS:
1. Edgar, T. F., Himmelblau, D. M. and Ladson, L. S., “Optimization of Chemical
Processes”,2nd Ed., McGraw Hill, New York, 2003.
2. Rao, S. S., Engineering Optimization: Theory and Practice, New Age Publishers, 2000
3. Diwaker, U. W. “Introduction to Applied Optimization”, Kluwer, 2003.
4. Joshi, M. C. and Moudgalya, K. M., “Optimization, Theory and Practice”, Narosa, New
Delhi, 2004.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Describe the basics problem 3 1 2 3 3 2
formulation and optimization.
CO2 Discuss mathematical 3 1 2 3 3 -
characteristics of linear
programming.
CO3 Explain computational solution 3 1 2 3 3 2
techniques for nonlinear
unconstrained optimization.
CO4 Demonstrate various techniques 3 1 2 3 3 1
used in constrained optimization
CO5 Apply the optimal and dynamic 3 1 2 3 3 1
optimization.
Average CO 3 1 2 3 3 1.2

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3211 MINI PROJECT WITH SEMINAR L T P C

0 0 2 1
OBJECTIVES:
 To provide exposure to the recent developments, and to improve the student's
presentation skills.
 To conduct literature review and to demonstrate the studies
 To gain knowledge on writing and presentation skills

24
COURSE CONTENT
 The students will be exposed to training in preparation and presentation skills.
 They will be involved in searching latest research in the area of chemical engineering
 Skill development on Report and Thesis writing

COURSE OUTCOMES
CO1: Gain knowledge on practical based work and use it to computational methods
CO2: Analyze data on CFD and other software’s
CO3: Analyze the lab data and interpret with real time problems to bring solutions

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Gain knowledge on practical
based work and use it to 3 3 2 3 3 1
computational methods
CO2 Analyze data on CFD and other
2 2 3 3 2 2
software’s
CO3 Analyze the lab data and
interpret with real time problems 3 2 3 3 1 2
to bring solutions
Average CO 3 3 3 3 2 1

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

SEMESTER III

CL3301 MODELING OF CHEMICAL PROCESSES L T P C

3 1 0 4
OBJECTIVES:
 To enable students to develop steady state and transient models for processes and
unit operations
 To impart knowledge on lumped and distributed parameter models and to seek solution
of models using analytic and numerical techniques
 To enable students to construct data driven models and estimate the parameters
 To make the students learn computational techniques to solve the process models
 To enable students to use simulation tools such as MATLAB/SCILAB

UNIT I OVERVIEW 12
Need for developing models for a process - Incentives of process modeling and simulation -
classification of mathematical models, conservation equations and auxiliary relations - Closed
form of solution – Well posedness of Models, Degree of freedom analysis - Design and Control
degrees of Freedom - Degrees of Freedom Analysis for flowsheets involving single and
multiple process units – Flowsheeting, Intoduction to Black box, White Box and Grey Box
Modelling, Artificial Neural Networks – ANN Applications.

UNIT II ALGEBRAIC MODELS 12

Models yielding linear and non-linear algebraic equations - Solution to linear and non-linear
algebraic equations - Convergence - Types of Convergence - Wegstein's Algorithm -

25
Levenberg-Marquadt Method, Application of algebraic models to dimensional analysis and
determination of independent species in a set of reactions.

UNIT III MODELS YIELDING ODE 12

Models yielding ODE - Classification of ODE - Solution of ODE - analytical methods using
matrices and numerical methods, Runge- Kutta methods of various orders, Mathematical
models with Initial and or Boundary conditions of surge tank, Transient isothermal and non-
isothermal Mixed flow reactor, separation systems such as distillation, flashing, Coiled and
Jacketed heaters.

UNIT IV MODELS YIELDING PDE 12

Models yielding PDE's - Characteristics and differences between Lumped and Distributed
Parameter systems - classification and solution of partial differential equations – Characteristic
curves for parabolic, Elliptic and Hyperbolic equations - Mathematical models of Heat
Exchanger, Packed bed reactor, plug flow reactor, Convection-Diffusion-Reaction (CDR)
model, packed bed adsorption, Solution of ODE boundary value problems – Finite difference,
Finite Element and Finite volume methods.

UNIT V OTHER MODELS AND SOFTWARES 12

Empirical modeling, parameter estimation, principle of linear and non-linear least squares -
Population balance and stochastic modeling- Application of population balance models in
crystallization, particle comminution, RTD in reactors - Principal Component Analysis - Kernel
PCA - Singular Value Decomposition. Solve the problems using MATLAB/SCILAB and ASPEN
Plus in association with any programming language, Machine learning or Deep Learning
Model Development.
TOTAL: 60 PERIODS
COURSE OUTCOMES:
CO1 Understand the fundamentals of modeling and their applications to
transport/energy equations, chemical and phase equilibria kinetics.
CO2 Construct mathematical models for different unit operations equipments such as
stirred tank heaters, Heat exchangers, Evaporators, Reactors, distillation columns.
CO3 Analyze the principles of steady state/unsteady state lumped systems and steady
state/ unsteady state distributed systems.
CO4 Apply relevant solution methods for the mathematical models with relevant initial
and/or boundary conditions both the manually and using software.
CO5 Evaluate the applicability of stochastic, population balance model and data driven
models.

REFERENCE BOOKS:
1. Bequette, B.W., “Process Dynamics: Modelling, Analysis and Simulation,” Prentice Hall
(1998).
2. Himmelblau D.M. and Bischoff K.B., Process Analysis and Simulation, Wiley, 1988.
3. Varma A. and Morbidelli M., Mathematical Methods in Chemical Engineering, Oxford
University Press, 1997.
4. Gilbert Strang, “Linear Algebra and its Applications”, Wellesley, MA : Wellesley-
Cambridge Press, Fourth Edition, 2009.
5. Ogunnaike B. and W. Harmon Ray, Process Dynamics, Modeling, and Control, Oxford
University Press, 1995.
6. Chapra S.C. and Canale R.P. Numerical Methods for Engineers, McGraw Hill, 2001.
7. Ramirez, W.; “ Computational Methods in Process Simulation “, 2nd Edn., Butterworths
Publishers, New York, 2000.

Course Articulation Matrix:

26
 Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Understand the fundamentals of
modeling and their applications to
transport/energy equations, 3 2 3 3 2 1
chemical and phase equilibria
kinetics.
CO2 Construct mathematical models
for different unit operations
equipments such as stirred tank
3 2 3 3 2 1
heaters, Heat exchangers,
Evaporators, Reactors, distillation
columns.
CO3 Analyze the principles of steady
state/unsteady state lumped
systems and steady state/ 3 2 3 3 2 1
unsteady state distributed
systems.
CO4 Apply relevant solution methods
for the mathematical models with
relevant initial and/or boundary 3 2 3 3 2 1
conditions both the manually and
using software.
CO5 Evaluate the applicability of
stochastic, population balance 3 2 3 3 2 1
model and data driven models.
Average CO 3 2 3 3 2 1

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3311 PROJECT WORK I L T P C

0 0 12 6
OBJECTIVES:
 To identify a specific problem related to Chemical Engineering and carrying out a
detailed literature review.
 To identify the materials and methods required to carry out the project.
 To guide the students in preparing project reports, to present their findings in reviews
and viva-voce examination.

COURSE CONTENT:
The student individually works on a specific topic selected by him/her which is
relevant to his/her specialization of the programme approved by a faculty member who is
familiar in the particular area of interest. The topic may be experimental or analytical or case
studies. At the end of the semester, a detailed report on the work done should be submitted
which contains a clear definition of the identified problem, detailed literature review related to
the area of work and methodology for carrying out the work. The students will be evaluated
through reviews internally by panel members and a final viva-voce examination conducted at
the end of the semester by a panel of one internal and one external examiner.

COURSE OUTCOMES:

27
CO1:Identify project goals, constraints, deliverables, performance criteria, control needs,
and resource requirements.
CO2: Interact with team in a professional manner to ensure a collaborative project
environment.
CO3: Ability to express clearly the findings and relate to theoretical background.
TOTAL: 180 PERIODS
Course Articulation Matrix:
Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Identify project goals, constraints, 3 3 3 3 3 3
deliverables, performance
criteria, control needs, and
resource requirements.
CO2 Interact with team in a 3 3 3 3 3 3
professional manner to ensure a
collaborative project
environment.
CO3 Ability to express clearly the 3 3 3 3 3 3
findings and relate to theoretical
background.
Average CO 3 3 3 3 3 3

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3411 PROJECT WORK II L T P C

0 0 24 12
OBJECTIVES:
 To execute the proposed procedure to solve the identified problem.
 To develop skills to analyze and discuss the results obtained and make conclusions.
 To relate the experimental data with the real time process

COURSE CONTENT:
The student individually works on a specific topic selected by him/her which is relevant to
his/her specialization of the programme approved by a faculty member who is familiar in the
particular area of interest. The topic may be experimental or analytical or case studies. At the
end of the semester, a detailed report on the work done should be submitted which contains
a clear definition of the identified problem, detailed literature review related to the area of work
and methodology for carrying out the work. The students will be evaluated through reviews
internally by panel members and a final viva-voce examination conducted at the end of the
semester by a panel of one internal and one external examiner.
TOTAL: 360 PERIODS
COURSE OUTCOMES:
CO1: Utilize technology and software tools for support.
CO2: Relate the findings to existing systems that they prioritize novel outcomes and
publish in Indian/International Journals, proceedings and patents proposal
CO3: Create their ideas, interpret the data acquired and defend their research work to a
panel of experts

Course Articulation Matrix:

28
 Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Utilize technology and software tools
3 3 3 3 3 3
for support.
CO2 Relate the findings to existing
systems that they prioritize novel
outcomes and publish in 3 3 3 3 3 3
Indian/International Journals,
proceedings and patents proposal
CO3 Create their ideas, interpret the data
acquired and defend their research 3 3 3 3 3 3
work to a panel of experts
Average CO 3 3 3 3 3 3

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3001 BIOCHEMICAL ENGINEERING L T P C

3 0 0 3
OBJECTIVES:
 To impart knowledge on the role of enzymes and microbes in biotechnology sectors.
 To enable students to understand the design parameters in designing biochemical
reactors.
 To impart knowledge on finding solutions to the problems with biomaterials and
processes
 To impart knowledge in bioreactors
 To enable students to study economy of bio based industries.

UNIT I ENZYME CATALYSIS 9

Overview of biotechnology, Principles of Enzyme catalysis, Enzyme inhibition, Immobilized
enzyme kinetics, internal mass transfer effects in immobilized enzyme kinetics.

UNIT II MICROBIAL GROWTH 9

Stoichiometry and energetics of microbial growth, Metabolic pathways and energetics of the
cell, concept of energy coupling, ATP and NAD, Unstructured models of microbial growth,
Structured models of microbial growth.

UNIT III BIOREACTOR DESIGN AND ANALYSIS 9

Bioreactors: CSTR, Plug flow and packed bed bioreactors, Fed batch reactors, Mass balances
for two phase reactors, Power requirements, sterilization.

UNIT IV PRODUCT RECOVERY 9

Bioproduct recovery- Centrifugation, Filtration, Ultra filtration, Precipitation of Protein,
Chromatography, Fixed bed adsorption, Phase theory of chromatography, Electrophoresis,
Crystallization.

UNIT V BIOPRODUCTS AND ECONOMICS 9

Manufacturing of biological products, cost analysis of bioprocesses, case studies.
TOTAL: 45 PERIODS

29
COURSE OUTCOMES:
CO1: Develop the ability to design novel bioprocesses for their research.
CO2: Classify engineering aspects of biological systems
CO3: Develop solutions to the problems with biomaterials and processes
CO4: Apply knowledge in bioreactors
CO5: Analyze economy of bio based industries.

REFERENCE BOOKS:
1. Shuler M.L. and Kargi F. Bioprocess Engineering: Basic Concepts, 1st Edition, Prentice
Hall, New Jersey, 1992.
2. Lee J., Biochemical Engineering, Prentice Hall Englewood Cliffs, 1992.
3. Blanch H.W and Clark D.S, Biochemical Engineering, Marcel Dekker
1997.
5. James M.Lee , Biochemical engineering – Prentice-Hall-1992.
4. Shigeo Katoh, Jun-ichi Horiuchi and Fumitake Yoshida, “Biochemical Engineering”,
Wiley, 2015.
5. Pauline M. Doran, Bioprocess engineering principles, Academic Press.
6. H.W. Blanch and D.S. Clark, Marcel Dekker, Biochemical Engineering, 1997

Course Articulation Matrix:

Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Develop the ability to design novel 1 2 1 - - 1
bioprocesses for their research.
CO2 Classify engineering aspects of 1 1 2 - 2 3
biological systems
CO3 Develop solutions to the problems 1 2 2 - 2 3
with biomaterials and processes
CO4 Apply knowledge in bioreactors 1 3 3 1 2 1
CO5 Analyze economy of bio based 1 2 3 1 2 3
industries.
Average CO 1 2 3 2 1 2

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3002 WASTE TO ENERGY L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to interpret the various types of wastes from which energy can
be generated
 To impart knowledge on biomass pyrolysis process and its applications
 To impart knowledge on various types of biomass gasifiers and their operations
 To impart knowledge on biomass combustors and its applications on generating energy
 To enable the students to summarize the principles of bio-energy systems and their
features

30
UNIT I INTRODUCTION TO EXTRACTION OF ENERGY FROM WASTE 9
Classification of waste as fuel – Agro based, Forest residue, Industrial waste - MSW –
Conversion devices – Incinerators, gasifiers, digestors.

UNIT II PYROLYSIS 9
Pyrolysis – Types, slow fast – Manufacture of charcoal – Methods - Yields and application –
Manufacture of pyrolytic oils and gases, yields and applications.

UNIT III GASIFICATION 9

Gasifiers – Fixed bed system – Downdraft and updraft gasifiers – Fluidized bed gasifiers –
Design, construction and operation – Gasifier burner arrangement for thermal heating –
Gasifier engine arrangement and electrical power – Equilibrium and kinetic consideration in
gasifier operation.

UNIT IV COMBUSTION 9
Biomass stoves – Improved chullahs, types, some exotic designs, Fixed bed combustors,
Types, inclined grate combustors, Fluidized bed combustors, Design, construction and
operation - Operation of all the above biomass combustors.

UNIT V BIO ENERGY 9

Properties of biogas (Calorific value and composition), Biogas plant technology and status -
Bio energy system - Design and constructional features - Biomass resources and their
classification - Biomass conversion processes - Thermo chemical conversion - Direct
combustion - biomass gasification - pyrolysis and liquefaction - biochemical conversion -
anaerobic digestion - Types of biogas Plants – Applications - Alcohol production from biomass
- Bio diesel production -Urban waste to energy conversion - Biomass energy programme in
India.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Identify various types of wastes from which energy can be generated
CO2: Describe biomass pyrolysis process and its applications
CO3: Appraise various types of biomass gasifiers and their operations
CO4: Evaluate biomass combustors and its applications on generating energy
CO5: Assess the principles of bio-energy systems and their features

REFERENCE BOOKS:
1. Biogas Technology - A Practical Hand Book - Khandelwal, K. C. and Mahdi, S. S., Vol. I
& II, Tata McGraw Hill Publishing Co. Ltd., 1983.
2. Biomass Conversion and Technology, C. Y. WereKo-Brobby and E. B. Hagan, John
Wiley & Sons, 1996.
3. Food, Feed and Fuel from Biomass, Challal, D. S., IBH Publishing Co. Pvt. Ltd., 1991.
4. Non Conventional Energy, Desai, Ashok V., Wiley Eastern Ltd., 1990.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Identify various types of wastes - - 2 - - -
from which energy can be
generated
CO2 Describe biomass pyrolysis - - 2 - - -
process and its applications

31
 CO3 Appraise various types of biomass - - 2 1 - -
gasifiers and their operations
CO4 Evaluate biomass combustors and 2 - 2 2 - -
its applications on generating
energy
CO5 Assess the principles of bio-energy - - 2 - - -
systems and their features
Average CO 2 - 2 1.5 - -
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3003 MEMBRANE SEPARATION PROCESSES L T P C

3 0 0 3
OBJECTIVES:
 To impart the students an insight to the membrane-based separations and development
of membranes modules
 To impart knowledge on Reverse Osmosis, Nanofiltration and Ultrafiltration
 To make the students understand about the principles of microfiltration and design of
membrane systems
 To enable the students to learn about problems encountered and solutions to membrane
processes.
 To make the students aware of other membrane separation processes.

UNIT I INTRODUCTION TO MEMBRANE SEPARATION PROCESS 9

Fundamentals of Membrane process, Membrane Materials, Types and preparation,
Membrane characterization, Membrane modules, Mechanism of Transport through porous
and nonporous membranes, Flow Pattern in membrane modules, Derivation of basic models
for fluid permeation by membranes

UNIT II REVERSE OSMOSIS, NANOFILTRATION AND ULTRAFILTRATION 9

Reverse Osmosis - The phenomenon of reverse osmosis, Thermodynamic consideration,
Solution diffusion model, Design and operating parameters; Nanofiltration - Principles of
nanofiltration, Transport mechanism in nanofiltration, Design, operating parameters and
process limitations; Ultrafiltration - Principle, Design parameters, Flux equation, Models for
solvent flux, Problems and solutions based on RO, NF and UF

UNIT III MICROFILTRATION AND DESIGN OF MEMBRANE SYSTEMS 9

Microfiltration - Modes of flow in microfiltration membranes, Membrane configuration,
mechanism of transport, Models for microfiltration, Membrane Module/Element designs:
Membrane System components, Design of Membrane systems, pump types and Pump
selection, Plant operations, Energy requirements in membrane separation process,
Economics of Membrane systems, Case Studies

UNIT IV MEMBRANE FOULING AND CONTROL 9

Membrane Fouling, Types of fouling, Factors responsible and Mechanism involved in fouling,
Theoretical models for membrane fouling, Pretreatment methods and strategies, monitoring
of Pretreatment – Langlier Index, Silt Density Index, Impact of membrane material on fouling,
Prevention of fouling, Methods to reduce concentration polarization, Fouling agents and their
control measures, Cleaning techniques and optimization

UNIT V MEMBRANE BIOREACTORS AND OTHER MEMBRANE PROCESSESS 9

32
Solid movement, mixing, segregation and staging, gas dispersion and gas interchange in
bubbling beds, Particle to gas mass and heat transfer, Experimental interpolation of mass
transfer coefficients, experimental heat transfer from bubbling bed model, applications of two
phase and three phase fluidized beds
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recall the basic principle, different types of membrane and membrane modules.
CO2: Recognize the various membrane process such as reverse osmosis, nanofiltration
and ultrafiltration
CO3: Illustrate the concepts of microfiltration and to develop necessary skills to design
appropriate membrane-based separation technique as per the need.
CO4: Review Fouling, Scaling, Concentration Polarization, and solutions
CO5: Evaluate the configuration of MBR and scope of Membrane technology.

REFERENCE BOOKS:
1. Mulder, M., “Basic Principle of Membrane Technology”, Kluwer Academic Publishers,
1996.
2. Noble, R.D. and Stern, S.A., “Membrane Separations Technology: Principles and
Applications”, Elsevier, 1995.
3. Judd S., B.Jafferman, “Membranes for Industrial Waste Water Recovery and Re-use”,
Elsevier Publications, 2003.
4. M. C. Porter, “Handbook of industrial membrane technology”, Noyes publication, Park
Ridge, New Jersey, 1990.
5. Symon Jud, “MBR Book – Principles and application of MBR in water and wastewater
treatment”, Elservier, 2006.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recall the basic principle, 1 1 3 3 3 3
different types of membrane and
membrane modules.
CO2 Recognize the various 1 1 3 3 3 3
membrane process such as
reverse osmosis, nanofiltration
and ultrafiltration
CO3 Illustrate the concepts of 1 1 3 3 3 3
microfiltration and to develop
necessary skills to design
appropriate membrane-based
separation technique as per the
need.
CO4 Review Fouling, Scaling, 1 1 3 3 3 3
Concentration Polarization, and
solutions
CO5 Evaluate the configuration of 1 1 3 3 3 3
MBR and scope of Membrane
technology.
Average CO 1 1 3 3 3 3

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

33
CL3053 FLUIDIZATION ENGINEERING L T P C
3 0 0 3
OBJECTIVES:
 To enable the students to learn the fundamentals of fluidization and its applications.
 To enable the students to understand the basic concept of hydrodynamics in fluidized
bed.
 To impart knowledge on bubble dynamics in dense beds.
 To enable the students to encompass the new areas and introduce reactor models
specifically for these Contacting regimes
 To enable the students to understand the fluidization behaviour, write model equations
for fluidized beds and design gas-solid fluidized bed reactors

UNIT I INTRODUCTION 9
Phenomenon of fluidization, behaviour of fluidized beds, Nature of hydrodynamic suspension,
Characterization of particles, particle forces, Regimization of the fluidized state, operating
models for fluidization systems, Industrial application of fluidized beds

UNIT II HYDRODYNAMICS OF FLUIDIZATION SYSTEMS 9

General bed behaviour, pressure drop, pressure regimes, Incipient Fluidization, Pressure
fluctuations, Phase Holdups, Measurements Techniques minimum fluidization velocity,
pressure drop, Geldart classification of particles, Fluidization with carryover of particles,
mapping of fluidization regimes

UNIT III DENSE BEDS 9

Distributor types, gas entry region of a bed, gas jets in fluidized beds, pressure drop across
distributors, design of a gas distributors, power consumption, Bubbles in dense beds: single
rising bubbles, Davidson model for gas flow at bubbles, Evaluation of models for gas flow at
bubbles, coalescence and splitting of bubbles, bubble formation. Slug flow

UNIT IV BUBBLING FLUIDIZED BEDS, ENTRAINMENT AND ELUTRIATION 9

Effect of temperature and pressure on bed properties, Estimation of bed properties, bubble
size and bubble growth, physical model and flow model- K-L Model with its Davidson bubbles
and wakes, freeboard behaviour, entrainment from tall and short vessels, high velocity
fluidization: turbulent fluidized beds and fast fluidization

UNIT V SOLID MOVEMENT, MASS AND HEAT TRANSFER 9

Solid movement, mixing, segregation and staging, gas dispersion and gas interchange in
bubbling beds, Particle to gas mass and heat transfer: Experimental interpolation of mass
transfer coefficients, experimental heat transfer from bubbling bed model, applications of two
phase and three phase fluidized beds
TOTAL: 45 PERIODS
COURSE OUTCOMES
CO1: Recall the basics of fluidization and know the various industrial applications of
fluidization
CO2: Demonstrate the concepts of hydrodynamics in fluidized bed
CO3: Describe the formation and growth of bubble dynamics in dense beds
CO4: Analyze the bed behavior for various geometries of fluidized beds
CO5: Evaluate the transport processes of fluidized beds

REFERENCE BOOKS

34
 1. Kunii, D. and Levenspiel, O., “Fluidization Engineering”, 2nd Edn., Butterworth
Heinemann, London, 1990.
2. Fan, L. S., “Gas- liquid Solid Fluidization Engineering”, Butterworths, 1989,
3. Kwauk, M., “Fluidization - Idealized and Bubbleless, with applications”, Science Press,
2009

Course Articulation Matrix:

Course Statements PO1 PO2 PO3 PO4 PO5 PO6
outcomes
CO1 Recall the basics of fluidization and -
know the various industrial - 3 - - -
applications of fluidization
CO2 Demonstrate the concepts of -
- 2 1 1 -
hydrodynamics in fluidized bed
CO3 Describe the formation and growth 1
- 2 1 2 -
of bubble dynamics in dense beds
CO4 Analyze the bed behavior for 1
- 2 2 1 -
various geometries of fluidized beds
CO5 Evaluate the transport processes of 1
- 1 1 2 -
fluidized beds
Average CO 1 - 2 1.25 1.5 -

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

PP3251 MULTICOMPONENT DISTILLATION L T P C

3 0 0 3
OBJECTIVES:
1. To enable the students to learn the thermodynamic principles involved in VLE and the
nonideal behavior and characterize using activity and fugacity coefficients.
2. To enable the students to learn about bubble point and dew point temperatures for
multicomponent mixtures.
3. To enable the students to learn the column sequencing for distillation trains and evaluate
rigorous methods of distillation design.
4. To impart knowledge about Kb method and Lewis Matheson calculation.
5. To enable the students to study about staged columns for separation of multicomponent
and petroleum mixtures.

UNIT I OVERVIEW OF MULTICOMPONENT DISTILLATION 9

Fundamental principles involved in the separation of multi-component mixtures; Determination
of bubble-point and Dew Point Temperatures for multi-component mixtures; equilibrium flash
distillation calculations for multi-component mixtures, Multiflash calculations

UNIT II THERMODYNAMICS FOR MULTICOMPONENT DISTILLATION 9

Fundamental Thermodynamic principles involved in the calculation of vapor-liquid equilibria
and enthalpies of multi-component mixtures; Use of multiple equations of state for the
calculation of K values – DePriester Charts, Estimation of the fugacity coefficients for the vapor
phase of polar gas mixtures – calculation of liquid, phase activity coefficient; Residue curve
bundles – Matrix Description of Residue curve structure.

35
UNIT III CONSIDERATION IN COLUMN DESIGN 9
General considerations in the design of columns, Column sequencing – Heuristics for column
sequencing, Key components – Distributed components – Non-Distributed components –
Adjacent keys. Definition of minimum reflux ratio – calculation of Rmin for multi-component
distillation – Underwood method – Colburn method – Smoker’s equation – Pinch technology.

UNIT IV METHODS FOR COLUMN DESIGN 9

Theta method of convergence – Kb method and the constant composition method, Application
of the Theta method to complex columns and to system of columns – Lewis Matheson method
– Thick and Geddes, Stage and reflux requirements – Short cut methods and Simplified
graphical procedures – Hengstebeck Diagrams – Minimum reflux by Hengstebeck Diagrams
– Key ratio Plots.

UNIT V TYPES OF MULTICOMPONENT DISTILLATION COLUMN 9

Hydro treating of oil fractions - Fundamentals of HDT, Reactor modelling and simulation,
Catalytic reactors for fuel processing, Basic reactions for fuel processing, Reactor design and
fabrication, water gas-shift reactors; modelling of catalytic deoxygenation of fatty acids: model
equations, adsorption parameter evaluation, particle diffusion and parameter estimation study.
TOTAL: 45 PERIODS
COURSE OUTCOMES
CO1: Explain the thermodynamic principles involved in VLE and the nonideal behavior and
characterize using activity and fugacity coefficients.
CO2: Evaluate bubble point and dew point temperatures for multicomponent mixtures.
CO3: Apply column sequencing for distillation trains, evaluate rigorous methods of
distillation design.
CO4: Practice Kb method and Lewis Matheson calculation.
CO5: Design staged columns for separation of multicomponent and petroleum mixtures.

REFERENCE BOOKS
1. Holland, C. D. Fundamentals of multicomponent distillation. McGraw-Hill. 1981.
2. Kister, H. Z., Haas, J. R., Hart, D. R., & Gill, D. R. Distillation design (Vol. 1). New York:
McGraw-Hill. 1992.
3. Petlyuk, F. B. Distillation theory and its application to optimal design of separation units.
Cambridge University Press. 2004.
4. Towler, G., &Sinnott, R. K. Chemical engineering design: principles, practice and
economics of plant and process design. Elsevier. 2012.
5. Holland, C. D. Multicomponent distillation. Prentice-Hall. 1963.
6. Seader, Junior D., Ernest J. Henley, and D. Keith Roper., “Separation process principles:
With applications using process simulators”, John Wiley & Sons, 2016.
7. Mc Cabe, Warren L., Julian C. Smith, and Peter Harriott., “Unit operation of chemical
engineering”, McGraw-Hill, 2018.

Course Articulation Matrix:

Program Outcomes
Course
Statement
Outcomes
PO 1 PO 2 PO 3 PO 4 PO 5 PO 6
Explain the
thermodynamic
CO1 principles involved in 1 1 2 1 - 2
VLE and the nonideal
behavior and

36
 characterize using
activity and fugacity
coefficients.
Evaluate bubble point
and dew point
CO2 temperatures for 3 2 2 2 1 2
multicomponent
mixtures.
Apply column
sequencing for
distillation trains,
CO3 3 3 3 2 2 2
evaluate rigorous
methods of distillation
design.
Practice Kb method and
CO4 Lewis Matheson 3 3 3 2 2 2
calculation.
Design staged columns
for separation of
CO5 3 3 2 2 2 2
multicomponent and
petroleum mixtures.
Average CO 2.60 2.40 2.40 1.80 1.75 2.00
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively.

CL3004 NANOCOMPOSITES L T P C
3 0 0 3
OBJECTIVES:
 To impart knowledge in nano composite materials in engineering applications
 To enable the students to learn and apply principles of various metal oxide nano composite
preparation
 To enable the students to understand polymeric nano composite synthesis
 To enable the students to learn biological synthesis of nano composites
 To enable the students to understand preparation of natural nano composites

UNIT I INTRODUCTION 9
Definition- importance of nanocomposites- nano composite materials-classification of
composites- metal/ceramics, metal / polymer, Carbon-carbon composites, nano composites
,influence of size, shape and role of interface in composites applications.

UNIT II PREPARATION AND PROPERTIES 9

Hydroxyapatite composites with zirconia, alumina and titania – preparation and
properties. SiC whisker reinforced hydroxyapatite and bioactive glass ceramics composites,
zirconia toughened and bioactive glass ceramics composites, bioglass-hydroxyapatite
composites, carbon composites

UNIT III PHYSICAL AND MECHANICAL PROPERTIES 9

Elastic and strength properties – fracture behavior – fibre matrix load transfer – failure of a

37
composite – criteria, damage of composites from physical and mechanisms to modeling, long
term behavior of composite materials, high temperature stability – wear and friction

UNIT IV STRUCTURES OF NANOCOMPOSITES 9

Nanotubes, nanoparticles and inorganic-organic hybrid systems: Single walled carbon
nanotubes in epoxy composites; Fullerene/carbon nanotube (CNT) composites; Filled
polymer nanocomposites containing functional nanoparticles; Polymer/calcium carbonate
nanocomposites; Magnetic polymer nanocomposites; Phenolic resin/SiO2 organic-inorganic
hybrid nanocomposites; Polymer/graphite nanocomposites; Wear resisting polymer
nanocomposites: Preparation and properties

UNIT V NATURAL NANOCOMPOSITES 9

Natural nanocomposites: Nanocomposites synthesized biologically; Nanocomposites
synthesized by mimicking natural processes; Packaging proteins. Nanocomposite materials
modeling: current issues. Multiscale modeling. Multi-physics modeling.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Demonstrate the various engineering application of nano composites.
CO2: Explain various metal oxide nano composite preparation
CO3: Determine the physical and chemical properties of nano composites
CO4: Arrange biological synthesis of nano composites
CO5: Design and develop natural nanocomposites and multiscale modeling.

REFERENCE BOOKS
1. Yiu-Wing Mai Zhong-Zhen Yu, , Polymer Nanocomposites, 1st Edition, Woodhead
Publishing, 2006
2. Krishan Kumar Chawla, Composite Materials: Science and Engineering, springer,
2012
3. Nanocomposite science and technology, Pulikel M. Ajayan, Wiley-VCH, 2005
4. Ajayan P.M. Nanocomposite Science and Technology, Wiley Verlag GmbH,
Weinheim, 2003, ISBN 3-527-30359-6
Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Demonstrate the various
engineering application of nano 2 2 1 2 1 -
composites.
CO2 Explain various metal oxide nano
2 1 1 2 1 -
composite preparation
CO3 Determine the physical and
chemical properties of nano 2 2 - 2 1 -
composites
CO4 Arrange biological synthesis of
- 3 1 - - 2
nano composites
CO5 Design and develop natural
nanocomposites and multiscale - - 1 - 1 -
modeling.
Average CO 2 2 1 2 1 2

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

38
CL3005 THERMAL PROCESSING OF FOOD PRODUCTS L T P C
3 0 0 3
OBJECTIVES:
 To enable the students recall the fundamentals of Mass and Energy balance and to apply
them in the design of various thermal processing methods
 To enable the students understand the principle, equipment types of low temperature
processing and preservation methods
 To impart knowledge of the drying techniques in food processing and preservation
 To enable the students comprehend the working principle and equipment types of
different aseptic processing methods of food products
 To impart sound working knowledge of various emerging food processing and
preservation technologies

UNIT I PRINCIPLES OF MASS AND ENERGY BALANCE 9

Material Balances-Basic Principles, Material Balance Problems Involved in Dilution,
Concentration, and Dehydration, Blending of Food Ingredient, Multistage Processes; Energy
Balances-General Principles, Enthalpy Changes in Foods During Freezing, Properties of
Saturated and Superheated Steam. Heat balance.

UNIT II PROCESSING AND PRESERVATION BY LOW TEMPERATURE METHODS 9

Use of low temperature – Principles, equipment and effect on quality: Chilling, cold storage.
Principles of food freezing: freezing point of foods, Psychrometric chart, Freeze concentration,
Freeze drying, IQF. New direction in freeze bed drying, cyclic pressure freeze drying. Freezing
of foods, types of freezing equipment,. Methods of freeze concentration, design problems.

UNIT III DRYING 9

Principles of drying, drying rate, factors affecting heat and mass transfer during drying,
properties of air-water mixtures; different drying methods: tray, drum, foam mat, spray, and
other newer drying methods; construction and design of drying equipment; adiabatic driers.
Dehydration of fruits, vegetables, milk, animal products and ready to eat food products. Design
parameters of different types of dryers.

UNIT IV ASEPTIC PROCESSING 9

Heat Sterilization. Canning and Retort treatment of foods; spoilage of canned foods, storage
of canned foods; Influence of canning on the quality of food; improvement in canning
technology. Pasteurization, TST and UHT treatment of milk, fruit juices and other liquid foods.
In Package and In flow thermal processing equipment - plate, spiral and shell and tube heat
exchangers.

UNIT V EMERGING PROCESSING TECHNOLOGIES 9

High Pressure Processing – principles, mechanism of action, advantages and disadvantages
over conventional processing; Equipment and applications in food industry, Pulsed electric
field and Ultrasound processing - principles, mechanism of action, advantages and
disadvantages over conventional processing; Equipment and applications in food industry.
Dielectric and Ohmic heating of foods - principles, mechanism of action, advantages and
disadvantages over conventional processing; equipment and applications in food industry.
Infra – red heating – principles, mechanism of action food application. Principles of radiation
processing, applications like disinfestation, pasteurization and sterilization, extending shelf life
of plant products, advantages and limitations.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recognize and recall engineering principles to food processing

39
CO2: Develop problem solving ability on types of loads and capability to design cold
storage systems for food products
CO3: Interpret the role of drying in the preservation of different foods
CO4: Apply the principles of aseptic processing of foods
CO5: Describe the recent developments in food processing and preservation techniques

REFERENCE BOOKS:
1. Toledo, R.M. “Fundamentals of Food Process Engineering”, 3rd Edition, Springer,
2007
2. Fellows, P. J. “Food Processing Technology: Principles and Practices”, Wood Head
Publishing, 1997
3. Barbosa-Canovas, Gustavo et al., “Novel Food Processing Technologies”, Marcel
Dekker/CRC, 2005
4. Lopez, G.A. and Barbosa, C.G.V. “Food Plant Design”, Taylor & Francis, 2005
5. S. Yanniotis, B. Sunden, Heat Transfer in Food Processing, Recent Developments
and Applications, WIT Press, Southampton, 2007
6. Ranganna, S. “Handbook of Canning and Aseptic Packaging” Vol. I, II & III, Tata
McGraw – Hill, 2000

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO1 PO2 PO3 PO4 PO5 PO6
CO1 Recognize and recall engineering
1 1 2 1 2 1
principles to food processing
CO2 Develop problem solving ability on
types of loads and capability to design 1 1 3 1 1 -
cold storage systems for food products
CO3 Interpret the role of drying in the
1 1 2 1 1 1
preservation of different foods
CO4 Apply the principles of aseptic
1 1 2 1 1 -
processing of foods
CO5 Describe the recent developments in
food processing and preservation 1 1 2 1 1 1
techniques
Average CO 1 1 2.2 1 1.2 1

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3006 BIOPROCESS TECHNOLOGY L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to learn the basics of bioprocessing
 To enable the students to understand the DNA structure
 To enable the students to calculate the mass and energy balances
 To enable the students to understand the upstream processes
 To enable the students to learn the downstream processes

UNIT I FRONTIERS OF BIOPROCESSING 9

Defining Bioprocessing, Current and Emerging Trends in Bioprocess Engineering, Materials
Advances, Nanoscale advances, Bioprocessing for Chemical and Biologic Product

40
Manufacturing, Bioprocessing Leaders Worldwide Economic Predictions and Careers in
Bioprocess Engineering, Skills Needed for Future Bioprocess Engineers.

UNIT II INTRODUCTION TO CELLULAR MICROBIOLOGY 9

DNA Structure, RNA Structure, Protein Structure and Function, Carbohydrates, Lipids, Fats,
and Steroids, Basic Metabolic Pathways, General Cell Structure Eukaryotes, Prokaryotes,
Archaea, and Viruses, Intracellular Organelles, Cellular Transport.

UNIT III REACTION STOICHIOMETRY, THERMODYNAMICS, AND KINETICS 9

Mass and Energy Balances, Fundamentals of Chemical Reactions, Basic Mass Transfer:
Diffusion and Convection, Basic Fluid Dynamics, Basic Thermodynamics, Basic Reaction
Kinetics.

UNIT IV UPSTREAM PROCESSING 9

Bioreactors, Batch Culture, Continuous Culture, Fed-Batch Culture, Perfusion Culture,
Suspension Culture, Microcarrier Support ,Roller Bottle Culture System, Spinner Flask
Culture, Other Scale up Options, Wave Bioreactor, Cell Cube Technology, Rotary Culture
System ,Media

UNIT V DOWN STREAM PROCESSING 9

Purification Processes - Centrifugation, adsorption, Electrophoresis, Crystallization Protein
Properties, Chromatography, Scale-up and Optimization,
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recognize all Bioprocesses and need of chemical basics in bioprocesses.
CO2: Describe the basic of cell and its internal constituents
CO3: Apply reaction mechanisms in terms of chemical kinetics.
CO4: Analyze all unit operations in upstream process in manufacturing Industries.
CO5: Evaluate the downstream processing and industrial bioreactors

REFERENCE BOOKS:
1. Bioprocess engineering principles, Pauline M. Doran, 2nd ed, Academic Press, 2012.
2. Biochemical engineering fundamentals by J.E.Bailey and D.F.Ollis, 2nd ed, 1986,
McGraw Hill.
3. Bioprocess Engineering by Michael L. Shuler and Fikret Kargi, 2nd edition, Pearson
education.
4. Biochemical engineering by James M.Lee – Prentice-Hall-1992
5. Fundamentals of Modern Bioprocessing by Sarfaraz K. Niazi, Justin L. Brown, CRC
Press, 2017.
6. Biochemical Engineering, H.W. Blanch and D.S. Clark, Marcel Dekker, 1997

Course Articulation Matrix:

Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recognize all Bioprocesses and
need of chemical basics in - 3 1 2 - -
bioprocesses.
CO2 Describe the basic of cell and its
1 1 1 2 - -
internal constituents
CO3 Apply reaction mechanisms in
- 3 1 2 3 -
terms of chemical kinetics.

41
 CO4 Analyze all unit operations in
upstream process in 3 1 1 3 2 -
manufacturing Industries.
CO5 Evaluate the downstream
processing and industrial 1 2 1 - - -
bioreactors
Average CO 3 1 2 1 2 1
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

42
CL3051 COMPUTATIONAL FLUID DYNAMICS L T P C
3 0 0 3
OBJECTIVES:
 To impart knowledge on basics of CFD and reminisce conservation principle
 To enable the students to understand discretization techniques
 To explain the numerical analysis of solving diffusion in 1D, 2D and 3D
 To explain the numerical analysis of solving of convection-diffusion problems
 To impart the knowledge of turbulence modelling and grid generation

UNIT I INTRODUCTION AND PRINCIPLES OF CONSERVATION 9

Basics of Computational Fluid Dynamics, Illustration of the CFD approach, CFD as an
engineering analysis tool, CFD application in Chemical Engineering, Fundamental principles
of conservation, governing equations of fluid flow, heat and mass transfer. Equations of
continuity, motion and energy in differential and integral forms, conservation and non-
conservation form.

UNIT II DISCRETISATION TECHNIQUES: FINITE DIFFERNCE APPROXIMATION 9

Classification of Partial Differential Equations, Mathematical behaviour of PDE, Basic aspects
of discretization, Discretization techniques using finite difference methods – Taylor’s Series,
explicit and implicit methods. Error and stability analysis

UNIT III DIFFUSION PROCESSES: FINITE VOLUME METHOD 9

Steady one-dimensional diffusion, two and three dimensional steady state diffusion problems,
Solution of discretised equations.

UNIT IV CONVECTION - DIFFUSION PROCESSES: FINITE VOLUME METHOD 9

One dimensional convection – diffusion problem, Central difference scheme, upwind scheme,
Hybrid and power law discretization techniques, QUICK scheme, Assessment of discretization
scheme properties, Solution of discretised equations.

UNIT V TURBULENCE MODELING AND GRID GENERATION 9

Characteristics of turbulent flows, time averaged Navier Stokes equations, turbulence Models
– one and two equation, Reynolds stress, LES and DNS. Physical aspects of Grid generation,
staggered grid, SIMPLE algorithm, PISO algorithm
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Describe the basics of CFD and governing equations for conservation of mass
momentum and energy
CO2: Analyze the mathematical characteristics of partial differential equations.
CO3: Solve computational solution techniques for time integration of ordinary differential
equations
CO4: Formulate various discretization techniques used in CFD
CO5: Assess various turbulence models and grid generation techniques

REFERENCE BOOKS
1. Anderson, J. D., “Computational Fluid Dynamics: The Basics with Applications”,
McGraw Hill, 1995.
2. Versteeg, H.K. and Malalasekera, W., “An Introduction to Computational Fluid
Dynamics: The Finite Volume Method”, Pearson Education Ltd., 2007.
3. Chung T.J Computational Fluid Dynamics Cambridge University Press 2003.
4. Fletcher, C. A. J., “Computational Techniques for Fluid Dynamics”, Springer Verlag,
1997.
5. Muralidhar, K., and Sundararajan, T., “Computational Fluid Flow and Heat
Transfer”,Narosa Publishing House, New Delhi, 2001.

43
 6. Ghoshdastidar, P.S., “Computer Simulation of flow and heat transfer” Tata McGraw –
Hill Publishing Company Ltd. 1998.
7. Subas, V. Patankar “Numerical heat transfer fluid flow”, Hemisphere Publishing
Corporation, 1980.
8. Taylor, C and Hughes, J.B. “Finite Element Programming of the Navier Stoke
Equation”,Pineridge Press Limited, U.K., 1981.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Describe the basics of CFD and - - - 2 - -
governing equations for
conservation of mass momentum
and energy
CO2 Analyze mathematical 1 - 2 1 2 2
characteristics of partial differential
equations.
CO3 Solve computational solution 1 - 2 3 3 2
techniques for time integration of
ordinary differential equations
CO4 Formulate various discretization 1 - 2 3 2 2
techniques used in CFD
CO5 Assess various turbulence models - - 2 1 1 1
and grid generation techniques

Average CO 1 - 2 2 2 1.75
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectivel

CL3052 DESIGN OF EXPERIMENTS L T P C

2 0 2 3
OBJECTIVES:
 To impart knowledge on sampling and sampling distribution and to apply hypothesis
testing with different confidence intervals
 To enable the students, develop skills in linear regression, both univariate and
multivariate, and utilize least squares methods to estimate and interpret regression
models.
 To enable the students to interpret experimental results using ANOVA, report data, and
construct confidence intervals.
 To enable the students to perform ANOVA and regression analysis
 To enable the students to explore variable selection, fractional factorial design, and
robustness in experimental design.

UNIT I FOUNDATIONS OF PROBABILITY AND STATISTICS FOR ENGINEERS 6

Introduction to probability and statistics - including concepts and principles; Statistical
inference fundamentals - such as estimation and hypothesis testing; Confidence intervals -
providing a range of plausible values for population parameters; Hypothesis tests to make
decisions based on experimental data.

44
UNIT II PRINCIPLES OF EXPERIMENTAL DESIGN 6
Statistical principles in experimental design - including the control of sources of variation;
Blocking and complete randomization techniques; Factorial design to study the effects of
multiple factors on the response variable; Analysis of individual factor effects and interaction
effects; Introduction to response surface methodologies for optimizing response variables
within a design space.

UNIT III REGRESSION MODELING AND ANALYSIS 6

Linear regression techniques - both univariate and multivariate - to model relationships
between variables; Least Squares estimation - including its basic principles and variants;
Nonlinear regression methods to model non-linear relationships; Techniques for model
assessment, interpretation, and evaluation of regression models.

UNIT IV ANALYSIS OF VARIANCE AND EXPERIMENTAL INFERENCE 6

Introduction to ANOVA - a statistical technique for comparing means among multiple groups
or treatments; Interpretation of results from experiments using ANOVA; Effective reporting of
experimental data; Construction of confidence intervals to estimate population means and
differences.

UNIT V ADVANCED TOPICS IN STATISTICS AND EXPERIMENTAL DESIGN 6

Exploration of additional topics in statistics and experimental design; Variable selection
techniques to identify significant factors in regression models; Fractional factorial design for
efficient exploration of factor combinations; Robustness in experimental design and analysis
- focusing on the stability and reliability of statistical methods in the presence of deviations
from assumptions.

List of tasks to be performed by students: Software Minitab 15

1) Exploratory Data Analysis: Import a dataset into Minitab and perform exploratory data
analysis; Calculate descriptive statistics - such as mean, median, and standard deviation;
Create graphical representations of the data, including histograms, box plots, and scatter
plots.
2) Probability Distribution Analysis: Generate random numbers from different probability
distributions in Minitab - such as normal, exponential, or binomial; Fit probability distributions
to data and assess goodness-of-fit using Minitab's distribution fitting tools.
3) Hypothesis Testing and Confidence Intervals: Formulate hypotheses and perform
hypothesis tests using Minitab for various scenarios; Conduct t-tests, chi-square tests, or
ANOVA tests to compare population means or proportions.
4) Experimental Design and Analysis: Design and execute experiments using Minitab's
design of experiments (DOE) tools; Analyze the results of designed experiments - including
factorial designs, using Minitab's DOE analysis features; Assess the significance of factor
effects and interaction effects.
5) Regression Modeling and Analysis: Perform linear regression analysis in Minitab to
model relationships between variables; Interpret the coefficients and significance of predictors
in regression models; Assess the goodness-of-fit and validity of regression models using
diagnostic plots and statistical tests in Minitab.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recognize and recall foundational probability and statistics concepts and apply
them to solve engineering problems.
CO2: Apply statistical inference techniques to draw conclusions from experimental data.
CO3: Analyze variance (ANOVA) technique and apply it to experimental design and
interpretation of results.
CO4: Illustrate skills in linear regression modeling and interpret regression models for
engineering applications.

45
CO5: Apply statistical principles to experimental design and assess model adequacy for
regression models.

Practical
CO1: Recall and apply foundational statistical concepts in practical data analysis using
software tools like Minitab.
CO2: Demonstrate proficiency in conducting hypothesis tests, constructing confidence
intervals, and analyzing experimental data using software.
CO3: Analyze regression models, interpret their coefficients, and evaluate model
adequacy through diagnostic plots and statistical tests using software.

REFERENCE BOOKS:
1. R.L. Mason, R.F. Gunst and J.L. Hess (2005). Statistical Design and Analysis of
Experiments – with applications to engineering and science, 2 nd edition, John Wiley
& Sons
2. Design of Experiments in Chemical Engineering: A Practical Guide by Z. R. Lazic, John
Wiley
3. R.A. Johnson, I. Miller and J. Freund (2007). Probability and Statistics for Engineers,
7 th edition, Prentice Hall Inc.
4. D.C. Montgomery and G.C. Runger (2007). Applied Statistics and Probability for
Engineers, 4th edition, John Wiley & Sons Inc.
5. Box, George EP, J. Stuart Hunter, and William G. Hunter. "Statistics for
experimenters." In Wiley series in probability and statistics. Hoboken, NJ: Wiley, 2005.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
Recognize and recall the
fundamental concepts of
CO1 probability and statistics and 3 1 3 1 1 1
apply them to engineering
problems.
Apply statistical inference
CO2 techniques to draw conclusions 1 3 1 1 3 1
from experimental data.
Analyze variance (ANOVA)
technique and apply it to
CO3 1 1 3 1 1 1
experimental design and
interpretation of results
Illustrate skills in linear
regression modeling and
CO4 2 1 3 1 1 1
interpret regression models for
engineering applications
Apply statistical principles to
experimental design and assess
CO5 1 1 1 1 3 1
model adequacy for regression
models.

Practical

46
 Recall and apply foundational
statistical concepts in practical
CO1 1 1 2 2 3 2
data analysis using software
tools like Minitab.
Demonstrate proficiency in
conducting hypothesis tests,
constructing confidence
CO2 3 2 2 2 3 2
intervals, and analyzing
experimental data using
software.
Analyze regression models,
interpret their coefficients, and
CO3 evaluate model adequacy 2 1 1 2 3 2
through diagnostic plots and
statistical tests using software.
Average CO 1.80 1.40 2.00 1.40 2.30 1.40

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3055 SUSTAINABLE MANAGEMENT L T P C

3 0 0 3
OBJECTIVES
 To enable the students to learn the fundamentals of sustainability in the context of
engineering.
 To enable the students to analyze the environmental impact of chemical processes and
identify opportunities for improvement.
 To impart knowledge on sustainable process design and optimization techniques.
 To enable the students to evaluate energy efficiency and resource conservation
strategies in industries/ plants.
 To enable the students to develop skills for implementing sustainable practices in
engineering projects and operations.

UNIT I INTRODUCTION TO SUSTAINABLE MANAGEMENT 9

Overview of sustainability principles and their relevance to chemical/petroleum/environmental
engineering; Environmental challenges in the chemical industry; Introduction to sustainable
development goals and their application in chemical engineering; Role of engineers in
promoting sustainability; Introduction to life cycle assessment (LCA) and environmental impact
analysis.

UNIT II SUSTAINABLE PROCESS DESIGN AND OPTIMIZATION 9

Principles and strategies for sustainable process design, Analysis and optimization of chemical
processes for sustainability; Integration of green chemistry principles in process design; Case
studies on sustainable process design in chemical engineering; Tools and software for
sustainable process design and optimization.

UNIT III ENERGY EFFICIENCY AND CONSERVATION 9

Energy consumption and environmental impact of chemical processes; Strategies for
improving energy efficiency in chemical plants; Energy conservation techniques in heat
transfer, separation processes, and reactions; Integration of renewable energy sources in
chemical processes; Case studies on energy-efficient operations in chemical engineering.

47
 UNIT IV WASTE MINIMIZATION AND RESOURCE RECOVERY 9
Waste generation in chemical processes and its impact on the environment; Techniques for
waste minimization and treatment; Resource recovery from waste streams, Recycling and
circular economy principles in chemical engineering; Case studies on waste reduction and
resource recovery in chemical processes.

UNIT V SUSTAINABLE SUPPLY CHAIN MANAGEMENT IN INDUSTRY 9

Sustainability considerations in the chemical supply chain; Responsible sourcing of raw
materials, Green packaging and logistics practices; Supplier assessment and management for
sustainability; Certification systems and standards for sustainable supply chains.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Identify and discuss the key principles and concepts of sustainability in the context of
engineering.
CO2: Analyze and evaluate the environmental impact of chemical processes and propose
sustainable solutions.
CO3: Design and optimize chemical processes considering sustainability factors and green
chemistry principles.
CO4: Assess and implement energy-efficient strategies and resource conservation
techniques in chemical plants.
CO5: Apply sustainable supply chain management principles to ensure responsible sourcing
and minimize environmental impact.

REFERENCE BOOKS
1. Beder, Sharon., “Environmental principles and policies: an interdisciplinary introduction”,
Routledge, 2013.
2. Elkington, John, and Ian H. Rowlands. "Cannibals with forks: The triple bottom line of
21st century business." Alternatives Journal 25, no. 4,42, 1999.
3. Fiksel, Joseph. Design for environment: a guide to sustainable product development.
McGraw-Hill Education, 2009.
4. Johansson, Allan. Clean technology. CRC Press, 1992.
5. Kane, Gareth. The green executive: corporate leadership in a low carbon economy.
Routledge, 2012.
6. Kirkwood, Ralph, and Anite Longley, eds. Clean technology and the environment.
Springer Science & Business Media, 1994.
7. Mulder, Karel, ed. Sustainable development for engineers: A handbook and resource
guide. Routledge, 2017.
8. Marinova, Dora, David Annandale, and John Phillimore, eds. The international handbook
on environmental technology management. Edward Elgar Publishing, 2008.
9. Von Weizsäcker, Ernst Ulrich, Amory B. Lovins, and L. Hunter Lovins. Factor four:
doubling wealth—halving resource use: a new report to the club of Rome. Springer
International Publishing, 2014.
10. Willums, Jan-Olaf. The sustainable business challenge: a briefing for tomorrow's
business leaders. Routledge, 1998.
11. Harmsen, Jan, and Joseph B. Powell. Sustainable development in the process industries.
Hoboken, NJ: John Wiley & Sons, 2010.

Course Articulation Matrix:

Program Outcomes
Course
Statement
Outcomes
PO 1 PO 2 PO 3 PO 4 PO 5 PO 6

48
 Identify and discuss the
key principles and
CO1 concepts of sustainability 3 3 3 1 1 1
in the context of
engineering
Analyze and evaluate the
environmental impact of
CO2 chemical processes and 1 2 2 3 3 2
propose sustainable
solutions
Design and optimize
chemical processes
CO3 considering sustainability 2 3 3 3 3 2
factors and green
chemistry principles
Assess and implement
energy-efficient strategies
CO4 and resource conservation 2 2 1 3 1 1
techniques in chemical
plants
Apply sustainable supply
chain management
principles to ensure
CO5 1 2 2 2 3 2
responsible sourcing and
minimize environmental
impact
Average CO 1.80 2.40 2.20 2.40 2.20 1.60
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively.

PP3051 MULTIPHASE FLOW L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to understand the significance of multiphase flows and different
flow pattern in multiphase flow
 To enable the students to determine the hydrodynamic parameters in the multiphase
flow system
 To enable the students to understand the concept of different flow models in different
phases.
 To enable the students to understand the one-dimensional two-dimensional flow
equation in turbulent condition
 To enable the students to understand the Hydrodynamic characteristics in different
contactors

UNIT I INTRODUCTION 9
Introduction to Multiphase Flow, Scope and significance of multiphase flows, Dimensionless
numbers in multiphase flows; Flow Pattern and Flow Regimes: Fluid-Solid System, Fluid-
Fluid Systems, Solid- Fluid-Fluid systems. Flow patterns in pipes, analysis of two phase flow
situations. Two-phase Co- current flow of Gas-Liquid, Gas-Solid and Liquid-Liquid,
Upward and Downward Flow in Vertical pipes. Suspensions of Solid and their transport in
Horizontal Pipes. Drag Reduction Phenomena, Laminar, Turbulent and Creeping Flow
Regimes.

49
UNIT II PREDICTION 9
Prediction of holdup and pressure drop or volume fraction, Bubble size in pipe flow, Lock
chart- Martinelli parameters, Bubble column and its design aspects, Minimum carryover
velocity. holdup ratios, pressure drop and transport velocities and their prediction.

UNIT III MODELS 9

Flow patterns - identification and classification - flow pattern maps and transition - momentum
and energy balance - homogeneous and separated flow models - correlations for use with
homogeneous and separated flow models - void fraction and slip ratio correlations - influence
of pressure gradient - empirical treatment of two- p h a s e flow - drift flux model -
correlations for bubble, slug and annular flows

UNIT IV AVERAGING PROCEDURES 9

Averaging procedures - time, volume, and ensemble averaging, quasi-one-dimensional flow,
two-fluid volume-averaged equations of motion, turbulence and two-way coupling

UNIT V APPLICATIONS 9
Flow regime Hydrodynamic characteristics of gas-solid liquid contactors (agitated vessels,
packed bed, fluidized bed, pneumatic conveying, bubble column, trickle beds), Applications
of these contactors. Measurement techniques in multiphase flow: Conventional and novel
measurement techniques for multiphase systems (Carpt ,Laser Doppler anemometry,
Particle Image Velocimetry)
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Explain the significance of multiphase flows and different flow pattern in multiphase
flow
CO2: Review the hydrodynamic parameters in the multiphase flow system
CO3: Develop different flow models in multiphase system.
CO4: Formulate the one-dimensional and two-dimensional flow equation in turbulent
condition
CO5: Demonstrate the Hydrodynamic characteristics in different contactors

REFERENCE BOOKS
1. Govier, G. W. and Aziz. K., “The Flow of Complex Mixture in Pipes”, Van Nostrand
Reinhold, New York, 1972.
2. Clift, R., Weber, M.E. and Grace, J.R., Bubbles, Drops, and Particles, Academic
Press, New York, 2005.
3. Crowe, C. T., Sommerfeld, M. and Tsuji, Y., Multiphase Flows with Droplets and
Particles, CRC Press, 2011
4. Fan, L. S. and Zhu, C., Principles of Gas-solid Flows, Cambridge University Press,
2005
5. Kleinstreuer, C., Two-phase Flow: Theory and Applications, Taylor & Francis, 2003

Course Articulation Matrix:

Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Explain the significance of
multiphase flows and different 2 3 1 1 2 1
flow pattern in multiphase flow

50
 CO2 Review the hydrodynamic
parameters in the multiphase flow 2 3 1 1 - 1
system
CO3 Develop different flow models in
2 - 1 1 2 -
multiphase system.
CO4 Formulate the one-dimensional
and two-dimensional flow 2 3 1 - 2 1
equation in turbulent condition
CO5 Demonstrate the Hydrodynamic
characteristics in different 2 3 1 1 - -
contactors
Average CO 2 3 1 1 2 1

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3056 POLYMER PROCESSING TECHNOLOGY L T P C

3 0 0 3
OBJECTIVES:
 To impart knowledge on the types of polymers, polymerization reactions,
polymerization techniques.
 To impart knowledge on processing of elastomers and application-oriented polymers.
 To enable the students to learn the analytical characteristics of polymers
 To enable the students to learn the testing procedures of polymer composites
 To impart knowledge on polymer composites

UNIT I GENERAL ASPECTS OF POLYMERS 9

Classification of polymers - natural and synthetic, thermoplastic and thermosetting; types and
mechanism of polymerization reactions; polymerization techniques; Polymer properties -
degree of polymerization, molecular weight determination, glass transition temperature,
crystallinity, thermal, electrical and mechanical properties.

UNIT II POLYMER PROCESSING 9

Process additives and significance; types of additives; mixing processes; Types of moulds;
mould cooling and ejection techniques; moulding - extrusion moulding, injection moulding,
blow mouldind and other moulding techniques.

UNIT III ELASTOMERS AND APPLICATION ORIENTED POLYMERS 9

Natural Rubber and synthetic rubber; unit operations; styrene – butadiene, polyisopropane –
neoprene, silicone rubber, thermoplastic elastomers; Resins – epoxy, phenol formaldehyde,
urea formaldehyde; fibrous Polymers - Nylon 66, PAN; PVC, Silicon Oil.

UNIT IV POLYMER TESTING AND CHARACTERIZATION 9

Analytical tests - determination of specific gravity, water absorption; Non-destructive testing -
ultrasonic testing, Acoustic emission (AE) testing, thermal stability, X-ray fluorescence, FT-IR,
XRD, SEM, AFM, etc.

UNIT V POLYMER COMPOSITES 9

Polymer composites and general concepts; structure and components of polymer composites;
classification of polymer composites; hybrid composites; usage areas of composites in daily
life.
TOTAL: 45 PERIODS

51
COURSE OUTCOMES:
CO1: Recall the fundamentals of polymers and mechanism of polymerization techniques
and polymer properties.
CO2: Apply the mechanism and effectiveness of polymerization in making finished
materials.
CO3: Demonstrate the knowledge of elastomers and its processing.
CO4: Construct the knowledge of analytical characteristics of polymer.
CO5: Assess the general aspects of polymer composite materials.

REFERENCE BOOKS:
1. Birley, Haworth, Batchelor, “Physics of Plastics – Processing Properties and Materials
Engineering”, Hamer Publication, 1992.
2. Billmayer F.W., “Text Book of Polymer Science” 3rd Ed., John Wiley and sons, New York,
2002.
3. Richard G. Griskey, “Polymer Process Engineering”, Chapman and Hall, 1995.
4. Vishu Shah, “Hand book of Plastics Testing and Failure Analysis”, 3rd Ed., John-Willey
&Sons, New York, 2007.
5. Sabu Thomas, Kuruvilla Josep, “Polymer Composites: Volume 1” 1st Ed., Wiley, 2012.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recall the fundamentals of - 1 - 2 3 3
polymers and mechanism of
polymerization techniques and
polymer properties.
CO2 Apply the mechanism and 3 3 1 3 3 3
effectiveness of polymerization in
making finished materials.
CO3 Demonstrate the knowledge of 3 3 1 3 3 3
elastomers and its processing.
CO4 Construct the knowledge of - 3 1 - 3 3
analytical characteristics of
polymer.
CO5 Assess the general aspects of 3 3 1 3 3 3
polymer composite materials.
Average CO 2 2.6 1 2.75 3 3

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3007 BUSINESS ANALYTICS L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to learn the basics of Business Analytics
 To enable the students understand and analyze descriptive analytics and Hypothesis
testing
 To impart knowledge on Data Analytics and Data Visualization
 To enable the students understand and analyze Predictive Analytics
 To enable the students understand and analyze Prescriptive Analytics

52
UNIT I INTRODUCTION TO BUSINESS ANALYTICS (BA) 9
Business Analytics - Terminologies, Process, Importance, Relationship with Organisational
Decision Making, Analytics in Decision Making, BA for Competitive Advantage- Organisational
Structures aligning BA. Managing Information policy

UNIT II DESCRIPTIVE ANALYTICS AND HYPOTHESIS TESTING 9

Data and Technology- data quality and change in BA- Descriptive and Inferential Statistics-
Mean/Nledian/Mode-Standard Deviation/Covariance/Correlation - Sampling And Estimation -
Probability Distribution For Descriptive Analytics - Analysis Of Descriptive Analytics-
Hypotheses testing

UNIT III DATA ANALYTICS AND DATA VISUALIZATION 9

An introduction to Data Analytics- Role of Analytics in the Modern World-Types of Analytics:
Descriptive, Diagnostic, Predictive, Prescriptive-Data Analytics and Ethical Issues, Data
visualizations : Create Visual Representations Of Data In Excel - Create Scatter Plots And
Calculate The Correlation Coefficient, Create Boxplot, Create, Historgram and line chart

UNIT IV PREDICTIVE ANALYTICS 9

Introduction to Predictive analytics - Logic and Data Driven Models - Predictive Analysis
Modeling and procedure - Data Mining for Predictive analytics. Analysis of Predictive analytics.

UNIT V PRESCRIPTIVE ANALYTICS 9

Introduction to Prescriptive analytics - Prescriptive Modeling - Non Linear Optimisation -
Demonstrating Business Performance Improvement.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recall the basics of Business Analytics
CO2: Analyze and apply descriptive analytics and Hypothesis testing
CO3: Illustrate Data Analytics and Data Visualization
CO4: Formulate Predictive Analytics
CO5: Evaluate Prescriptive Analytics

REFERENCE BOOKS:
1. Fundamentals of Business analytics, 2nd Edition,R.N.Prasad and Seema Acharya,
wiley india pvt ltd, 2016.
2. Business analytics,U.Dinesh kumar, wiley publisher, 2017.
3. Business analytics-data analysis and decision making with mind map, 7th edition, S.
Christian Albright and Wayne L. Winson, 2022.
4. Business analytics methods, models and decisions, 3rd edition, James R Evans,
2017.
5. Business analytics for decision making, 1st edition, Regi Mathew, 2020.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recall the basics of Business 3 1 2 3 3 1
Analytics
CO2 Analyze and apply descriptive 3 1 2 3 3 1
analytics and Hypothesis testing

53
 CO3 Illustrate Data Analytics and Data 3 1 2 3 3 1
Visualization
CO4 Formulate Predictive Analytics 3 1 2 3 3 1
CO5 Evaluate Prescriptive Analytics 3 1 2 3 3 1
Average CO 3 1 2 3 3 1

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3008 CHEMICAL PROCESSES AND POLLUTION CONTROL L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to understand the pollutants released from various chemical
industries.
 To familiarize the students on options for pollution prevent in chemical processes.
 To impart knowledge on pollutant measurement techniques.
 To develop student’s ability to frame management strategies for the control of pollution.
 To make the students understand the regulation pertaining to pollutant discharge.

UNIT I INDUSTRIAL POLLUTANTS ITS MEASUREMENT 9

Introduction- pollution from chemical process industries, characterization of emission and
effluents, standards for ambient air, noise emission and effluents; Analysis of pollutant;
Pollutant measurement- Fundamental Units of Measurement – Mass Concentration Parts Per
Million and mg/l, Mass Percentage and Mass Fraction, Mass Flow Rates, volume Fraction and
Volume Concentration; Converting Volume and Mass Concentration in Gases – Molar Mass
and Molar Concentration – Equivalent Weights

UNIT II POLLUTION PREVENTION FOR CHEMICAL PROCESSES 9

Pollution Prevention for Unit Operations; Preventing Fugitive and Secondary Emissions;
Flowsheet Analysis for Pollution Prevention; Management of Pollution Prevention Activities at
Industrial Facilities - Process modification, alternative raw material, recovery of by co-product
from industrial emission effluents; recycle and reuse of waste- energy recovery and waste
utilization; Material and energy balance for pollution minimization; Water use minimization.

UNIT III ELEMENTS OF POLLUTION PREVENTION PROGRAMS 9

The Waste Management Hierarchy and the Definition of Pollution Prevention; An Industrial
Perspective of Pollution Prevention-The Benefits of Pollution Prevention, Barriers to Pollution
Prevention (Industrial Barriers – Regulatory Barriers); The Basic Structure of a Pollution
Prevention Program - Identifying Critical Waste Streams; Waste Audits – Emission Inventories
(Fugitive Emissions – Secondary Emissions) – Prioritizing Waste Streams.

UNIT IV POLLUTION CONTROL 9

Water Pollution Control- Physical treatment, pre-treatment, solids removal by setting and
sedimentation, filtration centrifugation, coagulation and flocculation; Air Pollution Control-
Particulate emission control by mechanical separation and electrostatic precipitation, wet gas
scrubbing, gaseous emission control by absorption and adsorption, Design of cyclones, ESP,
fabric filters and absorbers.

54
UNIT V REGULATIONS GOVERNING POLLUTANT EMISSIONS 9
Regulations concerning water pollution-WATER (P&CP) ACT, 1974; air pollution- AIR (P&CP)
ACT, 1981; solid waste -hazardous Wastes-Hazardous and other Wastes (Management &
Transboundary Movement) Rules, 2016; Pollution Prevention Case Study.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Identify importance of pollutant measurement and different types of pollution
CO2: Classify pollution control options for different chemical processes.
CO3: Design Hierarchy of Pollution Prevention strategy.
CO4: Choose equipment for pollution control.
CO5: Illustrate regulations governing pollution prevention preventive

REFERENCE BOOKS:
1. Nancy J. Sell, Industrial pollution control: Issues and techniques.
2. Berthouex, P. M., Brown, L. C. (2017). Chemical Processes for Pollution Prevention
and Control. United Kingdom: CRC Press
3. "Pollution Control Acts, Rules, Notifications issued there under" CPCB, Ministry of Env.
and Forest, G.O.I., 3rd Ed. 2006.
4. Allen, D. T., Rosselot, K. S. Pollution Prevention for Chemical Processes: A Handbook
with Solved Problems from Refining and Chemical Processing Industries (1994).
5. Bishop P.E. Pollution Prevention: Fundamentals and Practice, McGraw Hill

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Identify importance of pollutant
measurement and different types - 3 1 2 - -
of pollution
CO2 Classify pollution control options
1 1 1 2 - -
for different chemical processes.
CO3 Design Hierarchy of Pollution
- 3 1 2 3 -
Prevention strategy.
CO4 Choose equipment for pollution
3 1 1 3 2 -
control.
CO5 Illustrate regulations governing
1 2 1 - - -
pollution prevention preventive
Average CO 1 2 1 2 1 -

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3009 RISK ANALYSIS AND MANAGEMENT L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to learn the principles and terminology related to risk management
 To enable the students to understand the basic quantitative methods on risk identification
and risk management

55
 To impart knowledge on the concepts of risk analysis and management in chemical
industries
 To impart knowledge on emergency planning and insurance
 To impart knowledge on handling risk analysis in chemical industries

UNIT I INTRODUCTION 9
Identify key risks; measure probability and impact; risk types; root cause analysis and decision
making.

UNIT II RISK ASSESSMENT AND HAZARD IDENTIFICATION 9

introduction and available methodologies - quantitative risk assessment, rapid risk analysis,
comprehensive risk analysis; risk identification; evaluation and control of risk; uncertainty in
risk assessment; hazard identification - hazard assessment, probabilistic hazard assessment,
fault tree analysis, event tree analysis, zero infinity dilemma.

UNIT III RISK MANAGEMENT 9

Risk management plan; mandatory technology option analysis; risk management alternatives;
risk management tools; risk management plans; risk index methods; precautionary principles;
risk perceptions and communication; behavioral decision making.

UNIT IV EMERGENCY PLANNING AND INSURANCE 9

Overall risk contours for different failure scenarios; disaster management plan; emergency
planning; onsite and offsite emergency planning; overview of insurance and risk transfer-
property insurance, transport insurance, liability insurance, pecunious insurance.

UNIT V RISK ANALYSIS IN CHEMICAL INDUSTRIES 9

Handling and storage of chemicals; process plants; personnel protection equipments;
environmental risk analysis; international environmental management system; corporate
management system; environmental risk assessment; total quality management; paradigms
and its convergence.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recall the general aspects of risk analysis and management.
CO2: Apply different tools to aid the risk assessment analysis
CO3: Identify characteristics of risk management system
CO4: Assess onsite and offsite emergency planning.
CO5: Analyze risk in Process industries and manage the risks.

REFERENCE BOOKS:
1. Srivastav, S., “Industrial Maintenance Management”, Sultan Chand & Co., 1998.
2. Crowl, D. A. and Louvar, J. F., “Chemical process safety; Fundamentals with
applications”, Prentice Hall Publication Inc., 2002.
3. Fawcett, H. H., “Safety and Accident Prevention in Chemical Operations” John Wiley
& Sons, 1982.
4. Kind, R. W., “Industrial Hazard and Safety Handbook” Butterworth, 1982.
5. Steiner, H. M., “Engineering Economic Principles”, McGraw Hill Book Co., New
York,1996.
Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recall the general aspects of risk 2 3 2 - - 1
analysis and management.

56
 CO2 Apply different tools to aid the 2 3 2 3 2 3
risk assessment analysis
CO3 Identify characteristics of risk 2 3 2 3 2 3
management system
CO4 Assess onsite and offsite 3 3 2 1 2 3
emergency planning.
CO5 Analyze risk in Process 3 3 2 3 2 3
industries and manage the risks.
Average CO 2.4 3 2 2.5 2 2.6
1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

CL3010 PROJECT ENGINEERING OF PROCESS PLANTS L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to understand the scope of project engineering
 To enable the students to learn the procedures for procurement and operations
 To enable the students to learn design and selection of pumps, compressors and
their accessories
 To impart knowledge on design and selection of piping and building constructions
 To enable the students to learn the evaluation techniques in project engineering

UNIT I SCOPE 9
Scope of project engineering – the role of project engineer – R & D – TEFR – plant location
and site selection – preliminary data for construction projects – process engineering – flow
diagrams – plot plans – engineering design and drafting. Planning and scheduling of projects
– bar chart and network techniques.

UNIT II PROCEDURES 9
Business and legal procedures: Procurement operations, Organization and operation of
procurement department, Procurement procedure, General purchaser-vendor practices,
contracts and contractors, project financing, statutory sanctions.

UNIT III DESIGN AND SELECTION – I 9

Details of engineering design and equipment selection – design calculations excluded -
Vessels, heat exchangers, process pumps, compressors and vacuum pumps, motors and
Turbines, other process equipment.

UNIT IV DESIGN AND SELECTION - II 9

Details of engineering design and equipment selection II – design calculations excluded –
piping design, thermal insulation and buildings, safety in plant design, plant constructions, start
up and commissioning.

UNIT V EVALUATION 9
Critical path method (CPM) and Programme evaluation and review technique (PERT) in
project engineering.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Recognize the scope of project engineering.
CO2: Analyze and apply the procedures for procurement and operations.
CO3: Choose pumps, compressors and their accessories.

57
CO4: Design and selection of piping and building constructions.
CO5: Evaluate the reviewing techniques in project engineering.

REFERENCE BOOKS:
1. Peter Watermeyer , Handbook for Process Plant Project Engineers, Wiley, 2002
2. Howard F. Rase, M. H. Barrow, Project engineering of process plants, Wiley, 1957
3. Peter S. Max &Timmerhaus, Plant design and economics for chemical engineers, Mc
Graw Hill, 2002.
4. B. C. Punmia & K. K. Khandelwal, Project Planning and Control with PERT & CPM,
Firewall Media, 2002
5. Srinath L. S., PERT AND CPM, 3rd Edn Affiliated East Press Pvt. Ltd., New York, 2001.
6. Perry J. H,”Chemical engineering handbook” 7th ed. McGraw Hill, 1997.
7. Ernest E. Ludwig, Applied project engineering and management, Gulf Pub. Co, 1988.
8. R K Sinnott, Chemical Engineering Design: Chemical Engineering Design, Chemical
Engineering Technical Series, Elsevier, 2014.

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Recognize the scope of project 1 3 3 3 3 3
engineering.
CO2 Analyze and apply the 3 2 3 3 3 3
procedures for procurement and
operations.
CO3 Choose pumps, compressors and 3 1 3 3 3 3
their accessories.
CO4 Design and selection of piping 3 1 3 3 3 3
and building constructions.
CO5 Evaluate the reviewing 3 3 3 3 3 3
techniques in project
engineering.
Average CO 3 2 3 3 3 3

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively.

58
CL3011 OPERATIONS RESEARCH L T P C
3 0 0 3
OBJECTIVES:
 To enable the students to solve linear programming problem and solve using graphical
method.
 To enable the students to solve LPP using simplex method
 To enable the students to solve transportation, assignment problems
 To enable the students to solve project management problems
 To enable the students to solve scheduling problems

UNIT I LINEAR PROGRAMMING 9

Introduction to Operations Research – assumptions of linear programming problems -
Formulations of linear programming problem – Graphical method

UNIT II ADVANCES IN LINEAR PROGRAMMING 9

Solutions to LPP using simplex algorithm- Revised simplex method - primal dual relationships
– Dual simplex algorithm - Sensitivity analysis

UNIT III NETWORK ANALYSIS – I 9

Transportation problems -Northwest corner rule, least cost method, Voges’s approximation
method - Assignment problem -Hungarian algorithm

UNIT IV NETWORK ANALYSIS – II 9

Shortest path problem: Dijkstra’s algorithms, Floyds algorithm, systematic method -
CPM/PERT

UNIT V NETWORK ANALYSIS – III 9

Scheduling and sequencing - single server and multiple server models - deterministic
inventory models - Probabilistic inventory control models
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Formulate linear programming problem and solve using graphical method.
CO2: Practice LPP using simplex method
CO3: Solve transportation, assignment problems
CO4: Analyze project management problems
CO5: Evaluate scheduling problems

REFERENCE BOOKS:
1. Harvey M Wagner, Principles of Operations Research: Prentice Hall of India 2010.
2. Hitler Libermann, Operations Research: McGraw Hill Pub. 2009.
3. Pant J C, Introduction to Optimisation: Operations Research, Jain Brothers, Delhi,
2008.
4. Pannerselvam, Operations Research: Prentice Hall of India 2010.
5. Taha H A, Operations Research, An Introduction, PHI, 2008

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Formulate linear programming
problem and solve using 1 2 2 2 3 3
graphical method.

59
 CO2 Practice LPP using simplex 1 1 3 1 3 3
method
CO3 Solve transportation, assignment 1 1 3 2 3 3
problems
CO4 Analyze project management 1 2 3 2 3 3
problems
CO5 Evaluate scheduling problems 1 2 3 2 2 3
Average CO 1 2 3 3 2 3

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively.

CL3012 SAFETY AND ENVIRONMENT IN CHEMICAL INDUSTRIES L T P C

3 0 0 3
OBJECTIVES:
 To make the students analyze the Root causes of accidents and effects on human beings
and materials
 To enable the students to understand the theories, structures and prevention of accidents
 To impart knowledge on industrial safety of a chemical process plant.
 To enable the students to understand the applications and advantages of good house
keeping
 To enable the students to learn the Disaster managements and various issues

UNIT I LEGISLATION AND POLICY 9

Safety, safety responsibility and organization, OHS, safety policy, safety inspection,
employees participation in safety, safety legislation, plant siting and layout, utilities and safety,
regulatory agencies with safety in India and Abroad, types of accidents in industry, case study.

UNIT II INDUSTRIAL HAZARD AND ASSESSMENT 9

Industrial hazard, hazard management program, hazard identification and assessment,
Material hazard: Toxicity, Radiation, Flammability, fires, explosion, runaway chemical reaction,
MSDS sheet, list of industries involving hazardous process, Factory Act, 1948

UNIT III HAZARD CONTROL 9

Environment, Need for environment control, lighting, importance of adequate lighting, lighting
design, colour codes used in industry, heat control, ventilation and air conditioning, legal
requirements, noise, noise measurement and control, vibration, industrial fatigue, EIA

UNIT IV WASTE CLASSIFICATIONS AND PPE 9

Industrial waste, waste classification, waste water treatment, waste disposal, storage,
transportation of hazardous materials occupational health problems, Fire management,
medical examination in industry, PPE, Training & Maintenance of PPE.

UNIT V SAFETY STANDARDS AND AUDIT 9

Quality standards, ISO 9000, ISO9000 : 2000 Quality Management principles, Benefits,
workplace emergency, emergency planning, on–site and offsite planning, fire emergency
procedure, safety symbols, safety signs and colour at work, training, safety audit.
TOTAL: 45 PERIODS
COURSE OUTCOMES
CO1: List the importance of industrial safety and safety regulations all over the world.

60
CO2: Discuss the effect of material hazard Evaluate the importance of EIA in chemical
industries
CO3: Classify the industrial waste and recommend the relevant PPE
CO4: Describe quality management principles and the importance of emergency
planning.
CO5: Practice industrial safety, environmental impact, rules and regulations

REFERENCE BOOKS:
1. Industrial Safety and Environment, Amit Kumar Gupta, Laxmi Publications Ltd., 2006
2. Chemical process industrial safety, KSN Raju, McGraw Hill, 2014
3. M.N.Vyas, Safety and hazards management in chemical industries, Atlantic
publishers,2020
4. Lees' Loss Prevention in the Process Industries: Hazard Identification, Assessment
and Control, Volume 1, edited bySam Mannan, third edition, 2005
5. Pravin M. Pathak , Jayant P. Khairnar Industrial Safety Management : Safety
Health And Environment Management, 2022

Course Articulation Matrix:

Course Statement Program Outcomes

Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 List the importance of industrial
safety and safety regulations all 1 3 1 2 1 1
over the world.
CO2 Discuss the effect of material
hazard Evaluate the importance 1 1 1 2 1 1
of EIA in chemical industries
CO3 Classify the industrial waste and
2 3 1 2 3 1
recommend the relevant PPE
CO4 Describe quality management
principles and the importance of 3 1 1 3 2 1
emergency planning.
CO5 Practice industrial safety,
environmental impact, rules and 1 2 1 1 2 1
regulations
Average CO 1.6 2 1 1.8 1.8 1

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively.

61
CL3013 BIOMASS CONVERSION TECHNIQUES L T P C
3 0 0 3
OBJECTIVES:
 To enable the students to understand the classification of biomass and composition of
biomass.
 To enable the students to understand different type of pre-treatment techniques.
 To impart knowledge on various methods of bio energy generations.
 To impart knowledge on the various biomass conversion techniques.
 To enable the students to understand the concept of bio refinery process.

UNIT I INTRODUCTION 9
World energy scenario, consumption pattern, fossil fuel depletion and environmental issues,
Biomass availability and abundance, Biomass conversion processes – Biological – Thermal –
Chemical – Hybrid conversions – Application of biomass conversion products – Biomass
properties for conversion process – Physical properties, Proximate, Ultimate and heating
value analysis.

UNIT II BIOMASS PRETREATMENT 9

Barriers in lignocellulosic biomass conversion, role of pretreatment in bioenergy conversion,
pretreatment technologies such as chemical, physical and physic chemical methods, hybrid
methods, Torrefaction – products obtained – properties of torrified biomass – Physical and
chemical – composition changes – torrefaction as pretreatment process, Briquetting: types of
Briquetting – merits and demerits.

UNIT III BIO FUEL GENERATION 9

Bioethanol and Biobutanol generation from lignocellulosic biomass, microorganisms for
fermentation, current industrial ethanol production technology, cellulases and their role in
hydrolysis, advanced fermentation technologies, ABE fermentation pathway and kinetics,
product recovery technologies. Biohydrogen generation, metabolic basics, feed stocks, dark
fermentation by strict anaerobes, facultative anaerobes, thermophilic microorganisms,
integration of biohydrogen with fuel cell; fundamentals of biogas technology, fermenter
designs, biogas purification, methanol production and utilization.

UNIT IV BIOMASS CONVERSION TECHNIQUES 9

Biomass combustion Process, Biomass gasification – chemistry – types of gasifiers – gasifier
design, Biomass Pyrolysis process, various reactor used for biomass combustion, Gasification
and Pyrolysis process. Factors affecting biooil, biochar production, fuel properties, bio-oil
upgradation. Biodiesel: Diesel from vegetable oils, microalgae and syngas; transesterification;
FT process, catalysts; biodiesel purification, fuel properties

UNIT V BIOREFINERY 9
Basic concept, types of biorefineries, biorefinery feed stocks and properties, economics,
Concept, corn/soybean/sugarcane biorefinery, lignocellulosic biorefinery, aquaculture and
algal biorefinery, waste biorefinery, hybrid chemical and biological conversion processes,
techno- economic evaluation, life-cycle assessment.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Classify types of biomasses and estimate the composition of biomass.
CO2: Explain different type of pre-treatment techniques.
CO3: Analyze the various methods of bio energy generations.
CO4: Describe the various biomass conversion techniques.
CO5: Assess the concept of bio refinery process.

62
REFERENCE BOOKS:
1. Sergio C. C. Introduction to Biomass Energy Conversions , First Edition, CRC Press,
2019.
2. David .B, Bio Energy Technology Thermodynamics and costs, Prentice Hall Europe,
1984
3. Sergio C. C., Introduction to Renewable Energy Conversions, CRC Press,2019.
4. Were Ko-Brobby C. Y., Hagan. E. B., Biomass Conversion and Technology, John
Wiley & Sons, 1996
5. Mahaeswari, R.C. Bio Energy for Rural Energisation, Concepts Publication,1997

Course Articulation Matrix:

Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Classify types of biomasses and 3 2 2 1 1 1
estimate the composition of
biomass.
CO2 Explain different type of pre- 3 2 2 1 1 -
treatment techniques.
CO3 Analyze the various methods of 3 2 - 1 - 1
bio energy generations.
CO4 Describe the various biomass 3 2 2 1 1 1
conversion techniques.
CO5 Assess the concept of bio refinery - 2 2 1 1 -
process.
Average CO 3 2 2 1 1 1

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively.

EV3051 ELECTROCHEMICAL ENVIRONMENTAL TECHNOLOGY L T P C

3 0 0 3
OBJECTIVES
 To understand wastewater characteristics and its importance
 To understand basic mechanism in electrochemical cell
 To learn basic electrochemical techniques to treat the gas, liquid and soil pollutant.
 To obtain knowledge about different electrochemical reactors in treating wastewater
 To Analyze the application of electrochemical engineering in various industries

UNIT I ELETROCHEMISTRY 9
Definition and classification of pollutants, Physical and chemical Characteristics of
wastewater, method of pollutants analysis role of sensors in environmental pollution.
Introduction to Electro chemistry and Electrochemical Engineering. Electrochemical potential-
Butler-Volmer, Tafel equation

UNIT II ELECTROCHEMICAL PROCESS AND ITS IMPORTANCE 9

Conventional methods for pollution control, incinerator, pyrolysis, air stripping, microbial
treatment, precipitation coagulation, adsorption, membrane process. Advanced techniques of
pollution treatment, Direct electro oxidation, Indirect electro oxidation, , Advantages of Electro
oxidation Process, pollutant treatment using electro oxidation process, Electro coagulation
process, Advantages of electro coagulation process, Electro flotation process, Application of
electrochemical process for waste water Treatment.

63
 UNIT III PHOTOELECTROCHEMICAL REACTOR 9
Comparison of Chemical and Electrochemical Process- Production of hydrogen by water
electrolysis. current efficiency, selectivity and energy consumption for electro organic
synthesis. Photo- electrochemical cells for conversion of light energy to electrical energy-
Photo electrochemical Conversion mechanism. Pollutant treatment using photo
electrochemical reactor

UNIT IV TYPES OF ELECTROCHEMICAL REACTOR 9

Electrochemical reactors; two dimensional and three dimensional electrodes; Tank cell- Filter
press cell-Packed bed – Fluidized bed electrochemical reactor-Applications; Batch;
Continuous Stirred Tank Electrochemical Reactor and Plug flow electrochemical Reactor-
Design Equation. Modeling of batch with recirculation, Electro oxidation-Electro coagulation,
Application of electrochemical reactors for waste water Treatment.

UNIT V HYBRID ELECTROCHEMICAL REACTOR 9

Application of AOPs for VOC reduction, biologically toxic or non-degradable and odour
treatment, Case studies - textile , pharmaceuticals and petroleum industries Characterization
techniques XRD, SEM,TEM,UV-DRS,FTIR
TOTAL: 45 PERIODS
COURSE OUTCOMES
CO1 Report the physical and chemical characteristics of wastewater and their
measurement
CO2 Discuss basic electr ochem ical engineering concept to treat the industrial
pollutants.
CO3 Compare various photo electrochemical method for treating pollutant
CO4 Classify various electrochemical processes in wastewater treatment.
CO5 Analyze various hybrid electrochemical reactors used in industries.

REFERENCE BOOKS
1. Scott, K., “Electrochemical Process for Cleaner Technology”, Academic Pres, 1990.
2. Kirkwood, R. C. And Longley, A.J., “Clean Technology and Environment”, Chapman &
Hall, 1995.
3. Rajeshwar, K. and Ibanez, J.G., “Environmental Electrochemistry”, Academic Pre, 1997.
4. Pletcher, D., and Walsh, F., “Industrial Electrochemistry”, 2 Edition Chapman and Hall,
1990.
5. Keith B.Oldham, Jan C Myland,” Electrochemical Science and Technology,
Fundamentals and applicaton”, Wiley 2011.

COURSE ARTICULATION MATRIX

Course Statement PROGRAM OUTCOMES
Outcomes PO1 PO2 PO3 PO4 PO5 PO6
CO1 Report the physical and chemical 1 2 2 1 2 2
characteristics of wastewater and their
measurement
CO2 Discuss basic electrochemical 2 2 2 2 2 2
engineering concept to treat the
industrial pollutants.
CO3 Compare various photo 2 2 2 2 2 2
electrochemical method for treating
pollutant
CO4 Classify various electrochemical 2 2 2 2 2 2
processes in wastewater treatment.

64
CO5 Analyze various hybrid electrochemical 2 2 2 2 2 3
reactors used in industries.
AVERTAGE CO 1.8 2 2 1.8 2 2.2

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively.

CL3054 INDUSTRIAL INSTRUMENTATION L T P C

3 0 0 3
OBJECTIVES:
 To enable the students to understand importance and measuring methods of various
measurement parameters.
 To enable the students to understand and apply suitable instruments for measuring
temperature, humidity and others.
 To enable the students to apply suitable analytical instruments for analyzing different
samples.
 To enable the students to understand the necessity of controllers and sensors in
measuring devices.
 To enable the students to analyze the industrial application and positioning of the
measuring instruments.

UNIT I INTRODUCTION 9
Introduction – Variables, Units & standards of measurement, Measurement terms –
characteristic. Data Analysis - why are the measurements of these parameters important in
industry? Different methods for measurement of motion parameters: Displacement, velocity,
acceleration, vibration, torque, force etc. Measurement of straightness, flatness, roundness
and roughness.
Typical case study/design example: Instrumentation system for motion measurement in
industry.

UNIT II MEASURING INSTRUMENTS 9

Process Variables Measurement–Temperature systems– Thermocouples, Thermo resistive
system, Filled-system thermometers, Radiation thermometry, Location of temperature
measuring devices in equipments, Pressure system – Mechanical pressure elements
Pressure Transducers and Transmitters, Vacuum measurement, Resonant wire pressure
Transducer, Flow system – Differential producers, Variable area flow meters, Velocity, vortex,
mass, ultrasonic & other flow meters, positive displacement flow meters, Open – channel flow
measurements, Force systems, Strain gauges Humidity Moisture system, Humidity
Measurement, Moisture measurement system, Rheological system, Viscosity measurement,
Radiation system, Nuclear radiation instrumentation.

UNIT III ANALYTICAL INSTRUMENTS 9

Analytical instrumentation – Analysis instruments, Sample conditioning for process analyzers,
X-ray Analytical methods, Quadrupole mass spectrometry, Ultra violet Absorption Analysis,
Infra-red process analyzers, Photometric reaction product analyzers, Oxygen analyzers,
Oxidation – reduction potential measurements, pH measuring systems, Electrical conductivity
and Resistivity measurements, Thermal conductivity, gas analysis, Combustible, Total hydro
carbon, and CO analyzer, Chromatography

UNIT IV CONTROLLERS AND SENSORS 9

Fundamentals of Automatic process control – Control algorithms-Automatic controllers –
Electronic controllers -Electric controllers (Traditional) - Hydraulic controllers – Fluidics -

65
Programmable controllers. Sensors, Transmitters and control valves - Pressure, Flow, Level,
Temperature and Composition sensors, Transmitters, Pneumatic and electronic control
valves, Types, Actuator, accessories, Instrumentation symbols and Labels.

UNIT V INDUSTRIAL SAFETY AND SPECIFICATIONS 9

Safety: Introduction, electrical hazards, hazardous areas and classification, Non-hazardous
areas. Enclosures – NEMA types, fuses and circuit breakers, protection methods: purging,
explosion proofing and intrinsic safety. Specification of instruments, preparation of project
documentation, process flow sheet, Instrument index sheet, Instrument specification sheet,
panel drawing and specifications.
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1 List different process variables and their measurement units.
CO2 Recognize and recall the principle and working of various process variable
measuring instruments.
CO3 Describe the principle, working and range of various analytical instruments.
CO4 Explain the role of controllers and sensors in industrial instrumentation.
CO5 Rate the need of safety and specifications in Industries.

TEXT BOOKS:
1. R.K.Jain, “Mechanical and Industrial Measurements”, Khanna Publishers, New Delhi.
2. C. D. Johnson, “Process Control Instrumentation Technology”, PHI.
3. S.K. Singh, “Industrial Instrumentation and Control”, Tata McGraw Hill Publishing Ltd.,
New Delhi.
4. Measurement Systems, Ernest O Doebelin & Dhanesh N Manik, McGraw Hill
Education; 6 edition (July 2017).
5. Principles of Industrial Instrumentation, D Patranabis, McGraw Hill Education; 3
edition (July 2017).
6. A Course in Electronic Measurements and Instrumentation, A.K. Sawhney, Dhanpat
Rai & Co. (P) Limited (2015).
7. Instrumentation, Measurement and Analysis, B. C. Nakra and K. K. Chaudhary,
McGraw Hill Education India Private Limited; Fourth edition (1 August 2016).

Course Articulation Matrix:

Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 List different process variables and
3 3 3 1 2 2
their measurement units.
CO2 Recognize and recall the principle and
working of various process variable 3 3 3 1 2 2
measuring instruments.
CO3 Describe the principle, working and
range of various analytical 3 3 3 1 2 2
instruments.
CO4 Explain the role of controllers and
3 3 3 1 2 2
sensors in industrial instrumentation.
CO5 Rate the need of safety and
3 3 3 1 2 2
specifications in Industries.
Overall CO 3 3 3 1 2 2

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

66
PP3052 PIPING AND INSTRUMENTATION L T P C
3 0 0 3
OBJECTIVES:
 To Learn the key concepts in piping and instrumentation of process plants.
 To Integrate the piping drawing with the different components and process
equipment’s.
 To Carry out the sizing calculations and develop the drawings
 To Know the importance of safety and implement the control systems
 To Develop the P&ID drawing with all basic requirements

UNIT I BASICS OF P&ID 9

Block flow diagram, process flow diagram, symbols, P&ID, P&ID symbols, line and valve
numbering concept, equipment identification, detailed engineering of the process. Introduction
to piping, Evolution of piping, Manufacturing methods, Piping materials and selection, Pipe
dimensioning, Schedule numbers, Common piping abbreviations, Major organizations for
standards, Commonly American code in piping ASME/ANSI, Common abbreviations.

UNIT II COMPONENTS AND EQUIPMENTS 9

Design principles, insulation concept, manual valves and automatic valves, ease of
maintenance, pumps and compressors, pressure relief devices, heat transfer units, utilities,
plant interlocks and alarms, stress analysis.

UNIT III SELECTION AND DIAGRAMS 9

Types of fluid flow, Friction factor, line sizing, pressure drop and velocity calculation, selection
of material under various condition, codes and standards, selection of pipe fittings, flanges,
fasteners, and gaskets. Piping isometrics, general arrangement drawings-
sections/elevations/ detail drawings, plot plan procedures, vendor data drawings, Case
studies.

UNIT IV CONTROLS 9
P&ID controls, Distributed Control Systems, signal lines, Selection of instruments - pressure,
temperature, flow. P&ID for the given problem statement.

UNIT V SAFETY AND COST ANALYSIS 9

Final Control Elements; safety systems application of P&ID in HAZOP, what – if, Fault tree
analysis, Event tree analysis, & Risk analysis, Management of Change, cost approach.
Practice & produce P&I diagrams using software packages during the period of the course.
Occupational Safety and Health Administration (OSHA) - OSHA 29 CFR 1910.119
TOTAL: 45 PERIODS
COURSE OUTCOMES:
CO1: Classify the materials, codes & standards used for piping the process plants.
CO2: Apply the piping design principle & importance of utilities in industrial process
plants.
CO3: Analyze the isometric drawing and general arrangement drawings.
CO4: Appraise the importance of safety control systems during piping instrumentation.
CO5: Construct a complete Process & Instrumentation Diagram with effective plant wide
control strategies using appropriate heuristics and its application.

REFERENCE BOOKS:
1. Piping Handbook, 6 th edition, M.L. Nayyar, P.E., Mc Graw-Hill, Inc
2. Piping Design Handbook edited by Johan J McKetta, CRC Press, 1992.
3. Luyben, W. L.," Process Modeling Simulation and Control for Chemical Engineers,
McGraw Hill, 1990.

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 4. Moe Toghraei, “Piping and Instrumentation Diagram Development”, Wiley, First
Edition, 2019.
5. Jagadeesh Pandiyan, “Introduction to Smart Plant(R) P&ID: The Piping and
Instrumentation Diagrams (P&ID) Handbook”, APJ Books, 2010.
6. Liptak B.G. Instrumentation in process industries, Chilton book Company, 1994
7. American National Standards Institute (ANSI) - ANSI/FCI 70-2-2003 - Control Valve
Seat Leakage - American Society of Mechanical Engineers (ASME) - ASME Boiler
and Pressure Vessel Code. Section VIII - Pressure Vessels - The Instrumentation,
Systems and Automation Society (ISA) – ISA 5.1, ISA 5.2, ISA 5.3, ISA 84.01

Course Articulation Matrix:

Course Statement Program Outcomes
Outcomes PO PO PO PO PO PO
1 2 3 4 5 6
CO1 Classify the materials, codes &
standards used for piping the 3 3 3 2 1 2
process plants.
CO2 Apply the piping design principle
& importance of utilities in 3 3 3 2 1 2
industrial process plants.
CO3 Analyze the isometric drawing
and general arrangement 3 3 3 2 1 2
drawings.
CO4 Appraise the importance of safety
control systems during piping 3 3 3 2 1 2
instrumentation.
CO5 Construct a complete Process &
Instrumentation Diagram with
effective plant wide control 3 3 3 2 1 2
strategies using appropriate
heuristics and its application.
Average CO 3 3 3 2 1 2

1, 2 and 3 are correlation levels with weightings as Slight (Low), Moderate (Medium) and
Substantial (High) respectively

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