Fourth Year Second Semester

Semester: 4th year 2nd Type: Theory Full Marks: 100 Credits: 3.0

Course Title: Organometallic Chemistry Course Code: CHEM-4201

Rationale: The understanding of chemistry of metal-organic framework (MOF) which is

important for the practical use of them in industries and laboratories. Therefore, student should

learn the variable properties of MOF, synthesis methods and reaction mechanism of MOF

compounds.

Course Learning Outcomes (CLOs): To study organometallic chemistry in a systematic way

for relating molecular structures to the number and nature of the valence electrons, and

develop a clear concept of sigma and pi bonding donor-acceptor model of metal-carbon bonds,

and achieving knowledge of significant reactivities of various organometallic complexes

including some general and important synthetic methods as well as their characterization and

stability.

Unit Learning Outcomes (ULOs) Course Content Teaching- Assessment

Learning Strategy of
Strategy SLO

 Describe a preview of 1. Introduction: Historical  Lecture  Short

historical progress developments in  Assignment question/M
 Explain different types of organometallic chemistry, CQ
ligands along with their Demarcation and  Essay
structures classification question
of organometallic  Assignment-
compounds, 18 electron Report
rule and classification of  Quiz
ligands.  spot Test
 Describe the methods of 2. Metal -Carbon sigma  Lecture  Short
preparation bonds: Metal carbonyl,  Assignment question/M
 Write down the physical and nitosyl and phosphine CQ
chemical properties complexes- Synthesis,  Essay
 Explain metal-CO/NO structure, bonding and question
bonding reactivity. Metal alkyl  Assignment-
 Describe the reactivity, complexes: Structure and Report
synthesis and stability Stability; Synthesis and  Quiz
reactivity  spot Test
 Describe the methods of 3. Metal -Carbon pi bonds:  Lecture  Short
1
 preparation a. Metal alkene  Assignment question/M
 Write down the physical and complexes Structure and CQ
chemical properties bonding, Synthesis and  Essay
 Explain reactivity question
metal-alkane/alkene/alkyne/ b. Metal-alkyne  Assignment-
ferrocene complexes: Synthesis, Report
bonding and reactivity.  Quiz
c. Metallocenes:  spot Test
 Explain the nature of Synthesis, bonding and
bonding , synthesis, reactivity with special
characterization and emphasis on Ferrocene.
reactivities
 Explain the stability of 4. Organometallic  Lecture  Short
various complexes, general chemistry of main group  Assignment question/M
synthesis as well as elements: Energy, Parity CQ
industrial applications and Reactivity of M-C  Essay
bonds, Stability of M-C question
bonds, Thermodynamic  Assignment-
and kinetic stability, Report
Methods for the  Quiz
preparation of main group  spot Test
organometallics: Oxidative
addition, Reductive
elimination, Exchange
reaction and Insertion
reaction.
 Describe the synthesis, 5. Metal Organometallics:  Lecture  Short
applications and important Structure and Bonding,  Assignment question/M
uses Properties of CQ
Organolithium,  Essay
Organomagnesium, question
Organoaluminium,  Assignment-
organotin and Report
organosilicon compounds,  Quiz
their applications in  spot Test
synthetic chemistry.
 Explain the various 6.Organometallic Catalysis  Lecture  Short
applications of : General principles of  Assignment question/M
organometallic complexes Catalysis, Homogeneous CQ
in organic synthesis and in and Heterogeneous  Essay
industrial processes based Catalysis, Catalytic Steps. question
on catalysis a) Catalytic reactions and  Assignment-
the 16/18 VE rule. b) Report
Arylation /Vinylation of  Quiz
olefins (Heck Reaction). c)  spot Test
Alkene metathesis d)
2
 Oligomerization and
Polymerization. e) Olefin
oxidation (Waker Process).
f) Hydrogenation of
Alkenes g)
Hydroformylation (Oxo
Reaction. h) Methanol
Carbonylation.

Books Recommended:
1. S. Z. Haider : Advanced Inorganic Chemistry
2. Cotton, Wilkinson and Gaus : Basic Inorganic Chemistry
3. Cotton and Wilkinson : Advanced Inorganic Chemistry
4. James E. Huheey : Inorganic Chemistry
5. Douglas, McDaniels and Alexander:Concepts and Models of Inorganic Chemistry
6. W. L. Jolly : Inorganic Chemistry
7. P. Poweell : Principles of Organometallic Chemistry
8. M. Bochmann : Organometallics 1, Oxford university press ,1994
9. M. Bochmann : Organometallics 2, Oxford university press,1994
10. Ch. Elschenbroich, A. Salze r : Organometallics; A concise introduction, VCH, 1992
11. D.F. Schriver, P.W. Atkins,
C.H. Langford : Inorganic chemistry, OUP, 1994

Semester: 4th year 2nd Type: Theory Full Marks: 100 Credits: 2.0

Course Title: Bioinorganic Chemistry Course Code: CHEM 4203

Rationale: The understanding of chemistry of different organic compounds is important for the

practical use of them in industries and laboratories. Therefore, student should lean the

properties, synthesis methods and reaction mechanism of several organic compounds.

Course Learning Outcomes (CLOs): Synthesis and analyze important organic compounds.

Unit Learning Outcomes Course Content Teaching Assessment

(ULOs) Learning Strategy
Strategy

 Write the name of Essential elements: General  Lecture,  Short

essential elements. aspects, availability of elements,  Reading, Question,
 Explain the role of roles of essential trace metal ion  Exercise,  Observation
essential elements in - Na+, K+, Ca2+, Mg2+, Co2+, Zn2+  Case study ,
biosystem. etc. and non metals, ion pumps  Class
 Explain the and polymorphism. participatio
mechanism of ion n
pumps.
 Describe the properties Functional value of the  Lecture,  MCQ,
of biomolecules. Chemical elements in  Assignment  Essay
3
  Discuss the function of Biological Systems: Major , Question,
chemical elements in chemical properties of chemicals  Exercise,  Assignment
living process. in aqueous solution, biochemical  Group Report,
 Explain the flow of functions of the chemical discussion  Observation
elements in biology. elements, the living process,
chemical flow in biology.
 Comparison porphyrin Metalloporphyrin, photosynthesis  Lecture,  Short
ring and corrin ring. and respiration: Porphyrin ring  Assignment Question,
 Explain the structure system, chlorophyll, cytochromes, ,  Assignment
of hemoglobin, oxygen transport and storage,  Project, Report,
myoglobin and oxygen carriers model compounds,  Exercise
chlorophyll. Iron porphyrins, hemoglobin and
 Describe the function myoglobin functions.
of biomolecules.
 Discuss the non haem Biological chemistry of Iron:  Lecture,  MCQ,
iron in biosystem. Introduction to iron biological  Exercise,  Assignment
 Explain the role of iron chemistry, non haem iron - iron  Assignment Report,
on human health. uptake, non- haem iron proteins, ,  Observation
 Describe the function rubredoxins and ferrodoxins,  Group ,
of electron transfer Haem iron - properties of discussion
protein. isolated haem units, haem
protein functions-electron
transfer, oxidases and
dioxygenases. Effects of
deficiency on human health.
 Evaluate the role of Metalloenzymes: Non redox  Lecture,  MCQ,
metalloenzyme. metalloenzymes, peroxidase and  Assignment  Assignment
catalase, the role of copper. , Report,
 slide show,
 Mention the sources of Biomolecules of Zinc: Sources  Lecture,  Assignment
zinc. and RDA, effects of deficiency  Assignment Report,
 Evaluate the roles of and remedy, Zinc fingers and ,  Observation
zinc in biological super oxide dismutase.  Exercise
system.
 Name the common Principle of bioinorganic  Lecture,  MCQ,
inorganic drugs. medicine: Inorganic drugs,  Assignment  Assignment
 Describe the chelating antibiotic and related , Report,
therapy. compounds, chelate therapy,  slide show,  Observation
 Explain the platinum cisplatin, carboplatins, platinum  Exercise ,
anti cancer activity. anticancer drugs,  Viva
radiopharmaceuticals.

Books Recommended:
1. Hughes : Inorganic Chemistry in Biological process

4
2. J. E. Huheey : Inorganic Chemistry
3. Y. Satake, S. Mido : Bioinorganic Chemistry
4. Douglas, McDaniel and Alexander : Concepts and Models of Inorganic Chemistry
5. R. W. Hay : Bioinorganic Chemistry
6. S. J. Lippard and J. M. Bereg : Principles of Bioinorganic Chemistry
7. Sally Solomon : Introduction to General, Organic and Biological
Chemsitry,McGraw Hill Book Company. NY.
8. J.B. Taylor and P. D. Kennewell : Modern Medicinal Chemistry, Ellis Horwood,
NY, - 1st edn.
9. J. L. Jain : Fundamentals of BioChemistry - Chand Company
LTD. New Delhi.
10. O.P. Agarwal : Chemistry of Organic Natural Products Vol. II –
Geol Publication, India, 15th edn.
11. I. L. Finar : Organic Chemistry, Longman, Vol. 2 - 5th edn.

Semester: 4thyear 2nd Type: Theory Full Marks: 100 Credits: 3.0

Course Title: Medicinal and Pharmaceutical Chemistry Course Code: CHEM-4205

Rationale: This course has been planned to provide knowledge on fundamental properties and

activities of medicine along with their synthesis and quality control process.

Course Learning Outcomes (CLOs): Development of theoretical concept on phase

equilibrium and surfactant properties with their application.

Unit Learning Course Content Teaching- Assessment

Outcomes (ULOs) Learning Strategy of SLO
Strategy

 Define drug, 1. General Principles in Medicinal  Lecture  Short

prodrug. Chemistry: Definition, sources of Drugs  Assignmen question/MC
 Describe the and its Classification,Prodrugs and Raw t Q,
classifications, raw materials; Physico-chemical properties,  Essay
materials, biological activity, pharmacological question
properties, activities activity and metabolism of drugs;  Assignment-
and sources of drug. Theoretical aspects of drug design, Report
 Describe drug drug discovery and drug development;
design and importance of pharmaceutical chemical
development. and products.

 Describe drug 1. Pharmacology a) Basic concept  Lecture  Short

action and binding of drug action. b)Physico-  Assignmen question/MC
forces. chemical nature of drugs. c) t Q,
 Describe drug- Drug receptors. d) Binding  Essay
receptor interaction forces in drug-receptor question
and mechanism. interaction e) Receptor and non  Assignment-
5
 receptor mechanisms of drugs. Report
(f) Toxicology. Introduction,
classification, chemistry, mode
of action, routs of
administration, mechanism,
structure-activity relationship,
pharmacokinetics, indications,
contraindications, dose, adverse
effects and drug interactions of
different group of drugs. e.g.
antibiotics.
 Describe tablets, 3. Pharmaceutics :Tablets and Tablet  Lecture  Short
their properties and Coating: Definition, component of  Assignmen question/MC
preparation. tablets, Formulation of different types t Q,
 Mechanism of of Tablets, Granulation technique,  Essay
action of tablets. Hardness measurement, weight question
 Describe capsules, variation tests, thickness and diameter, Assignment-
their properties and friability, disintegration time, Report
preparation. dissolution time, mechanism of tablet
disintegration and dissolution. In-
process quality control, study of
common tableting problems.Different
methods of coating and their
comparison.Capsules:Definition and
classification, properties, advantages
and limitations of capsule dosage form,
manufacture of hard and soft gelatin
capsules and their shells, formulation
of capsules, importance, stability test.

 Describe synthesis, 4. Chemistry, application mode of  Lecture  Short

application, mode action of some important drugs:  Assignmen question/MC
of action, advantage a)Supha-drugs (antibacterial t Q,
and disadvantage of agents): sulphanilamide,  Essay
some specific sulphapyridine, sulphadiazine, question
important drugs. sulphaguanidine. b)Antimalarials:  Assignment-
 Describe brief Pamaquine, Chloroquine, Report
concept on Camoquine c)Antipyretic
anesthetics, Analgesics: Paracetamol, Aspirin,
anticancer, cardiac Phenacetin. d) Brief concepts of
and related agents. Anesthetics, Anticancer, Cardiac
and related agents

 Describe 5. Quality control and Quality  

importance of assurance: Importance of

6
 quality control and pharmaceutical analysis in the quality
quality assurance of control of drugs, sources of quality
drugs. variation, control of quality variation.
 Process of quality Set up of a quality control laboratory
control. for pharmaceutical analysis, personnel,
 Conceptualize the equipment, environments, etc. Types
basic concepts of of specifications, sampling, testing
GMP, ISO 9000, program and methods. Concept of
ISO 9001 and quality assurance, selection and testing
TQM. of major raw materials input. Methods
of drug sampling, statistical quality
control of major categories of dosage
forms, QA activities, theory and basic
concepts of cGMP, ISO 17025:9000, ISO
9001, TQM. and BSTI (DA), BP, EN
policies for quality in pharmaceutical
industries. Management of Quality
Assurance: Quality management
consideration, quality motivation, total
quality management,S.Q.C.charts.

Books Recommended:

1. M. Shah Nawaz Khan : Assurance of Quality Pharmaceuticals

2. A.H. Beckett, and J. B. Stenlake : Practical Pharmaceutical Chemistry Vol. I & II
3. K. A. Connors : A Textbook of Pharmaceutical Analysis
4. L.G. Chatten : Pharmaceutical Chemistry Vol. I & II
5. L. Lachman, H.A. Liebernan, J.L. Kanig : The Theory and Practice of Industrial Pharmacy
6. S. J. Carter : Cooper and Gunn’s Dispensing for Pharmaceutical
student

7. M. E. Aulton : Pharmaceutics, the Science of Dosage For Design

8. H. P. Rang, M. M. Dale and J. M. Ritter : Pharmacology
9. R. S. Satoskar and S. D. Bhandarkar : Pharmacology and Pharmacotherapeutics Vol. I & II
10. M. Misbahuddin and M.R. Islam : General Principles of Pharmacology
A. Goldstein, L. Aronow and S.M. Kalman : Principles of Drug Action, The Basis of

Pharmacology

11. Ashutosh Kar : Medicinal Chemistry

Semester: 4th year 2nd Type: Theory Full Marks: 100 Credit: 2.0

Course title: Green and Sustainable Chemistry Course code: CHEM 4207

Rationale: This course is designed to give an understanding on the concept of green chemistry

7
and chemical synthesis in a sustainable way, explain the concepts of various forms of renewable

energy resources.

Course Learning Outcomes: Students will be able to understand about the ideal synthetic

methods and to design green reagents and green solvents for chemical synthesis, learn about the

hazardous waste minimization, management and treatment and disposal, understand the

importance of renewable energy resources and its utilization.

Unit Learning Outcomes Course Content Teaching- Assessment

(ULOs) Learning Strategy of SLO
Strategy

 Learn about the concept 1.Green Chemistry:  Lecture  Short

and goals of green Principles and concept of  Assignment questions.
chemistry green chemistry, the  Essay type
 Learn basic principles of fundamental of green questions.
green chemistry chemistry, 12 principles of  Assignment
 Learn about to design Green chemistry, problems report
alternative reagents, and finding of solutions for
solvent media and energy sustainable development,
sources for chemical pollution abatement,
process ecology, green molecular
 Know how chemical modelling and green
process (synthesis) can be reaction, EPA, role of
designed and run in a IPCS, IRPTC, IPCC, green
sustainable way.
chemistry takes the grand
 Design of chemical products
challenges.
and processes that
eliminate the use and
generation hazardous waste
 Identify and classify 2. Hazardous materials:  Lecture  Short
hazardous materials and Hazardous materials,  Assignment questions.
waste history, legislation, sources,  Essay type
 Understand the classification, flammable questions.
environmental problems and combustible substance,  Assignment
associated with hazardous reactive substances, report
waste corrosive substances,
 Understand how hazardous physical forms and
materials enter into the segregation of wastes,
environment environmental chemistry of
 Identify the sources, hazardous waste, hazardous
characteristics and waste in geosphere,
environmental effects of hydrosphere, atmosphere,
hazardous waste water
biosphere, environmental
from various chemical
8
 industries aspects of some industries:
fertilizer, pulp and paper,
tannery, textile, food etc.,
disposal of hazardous
materials with special
reference to toxic chemicals:
H2S gas, HCl fume, HNO3
fume, toxic metals: Pb, Cd,
As, Hg, Ni, Cu etc.,
pesticides, chlorinated
hydrocarbon, aromatic
hydrocarbon.
 Explain the techniques of 3. Reduction, Treatment  Lecture  Short
hazardous waste and disposal of Hazardous  Assignment questions.
minimization, management waste: Waste reduction and  Essay type
and treatment minimization, recycling, questions.
 Explain the principle of physical methods of waste  Assignment
waste water treatment and treatment, chemical report
apply knowledge in the treatment, photolytic
process design reactions, thermal treatment
 Evaluate the main methods, biodegradation of
technologies (methods) waste, land treatment and
associated with hazardous composting, preparation
waste treatment and wastes for disposal, ultimate
disposal disposal of wastes, leach ate
 Describe the physical,
and gas emissions, in-situ
chemical and biological
treatment, sewerage
methods of treating
treatments and ETP, Nuclear
hazardous waste
waste recycling, hazardous
 Describe the processes
waste management,
associated with the
integrated solid waste
municipal solid waste and
management and air quality
industrial waste water
management concept.
treatment.
 Identify factors that should
be considered for
hazardous waste
management plan
 Define and classify 4. Chemical Toxology:  Lecture  Short
toxicology Toxicology, types of  Assignment questions.
 Define how the toxicity, toxic and  Essay type
characteristics of a chemical micronutrients, questions.
influence its toxicity classification of toxicology,  Assignment
 Identify relationship tolerance limit and TLV, report
between chemical exposure impact of toxic chemicals on
and effects on physiological enzymes, genetic toxicology
9
 systems and design and chemical carcinogens,
strategies for study of dose-response relationship
dose-response relationship of toxicants (MLD, LD50,
 Learn about the LD100), impact of toxic
biochemical effects, toxicity chemicals (Ag, Hg, Pb, Cd,
and toxicology of toxic CO, SO2, pesticides etc).
elements

 Explain the concept of 5. Renewable energy and  Lecture  Short

various forms of renewable green technology:  Assignment questions.
energy and analyze the Definition of renewable  Essay type
environmental aspects energy, types: wind power, questions.
renewable energy hydropower, solar energy,  Assignment
resources. biomass, biofuel, report
 Describe the use of solar geothermal energy,
energy and the various recycling. Water and air
components used in the purification. Alternative and
energy production clean power : cellulosic
 Understand the concept of
ethanol, hot-dry-rock
biomass energy resource,
geothermal power, and
their use and classification,
types of biogas plants and
ocean energy, carbon-
applications
neutral and negative fuels,
 Acquire knowledge of fuel enhanced geothermal
cells, wind power, systems, thermoelectric,
hydropower and or "thermo voltaic" devices,
geothermal principles and artificial photosynthesis.
applications Green nanotechnology.
 Design of safer chemicals Design of new green
and products and introduce chemicals and materials,
basic principle of green sustainable resources,
engineering applied to biotechnology alternatives,
product design and evaluation of environmental
manufacturing process impact, environmentally
 Develop a thorough improved routes to
understanding of the important products. Green
concept of green chemistry technology and energy
towards clean production conservation efficiency.
and sustainability. Nuclear energy. Renewable
energy resources, Biomass
energy.

Books Recommended:
1. G. S. Sodhi : Fundamental concepts of Environmental Chemistry.
10
2. Colin Baird : Environmental Chemistry
3. S.E. Manahan : Environmental Chemistry (6th Ed.)
4. A. K. De : Environmental Chemistry
5. P. T. Anastas, J. C. Warner : Green Chemistry: Theory and Practice, Oxford University
Press

6. Vaughn Nelson : Introduction to Renewable Energy, CRC press.

Semester: 4th year 2nd semester Type: Theory Full Marks: 100 Credits: 3.0

Course Title: Nanochemistry Course Code: CHEM-4209

Rationale: The understanding of nano-sized materials and their tremendous applications in

technology.

Course Learning Outcomes (CLOs): Methods of synthesis, analysis and characterization of

nanomaterials.

Unit Learning Outcomes Course Content Teaching- Assessment

(ULOs) Learning Strategy of SLO
Strategy

 Describe a preview of 1. Introduction to  Lecture  Short

historical progress nanomaterials: History and  Assignment question/MCQ
 Classification of scope, nanosize and  Essay question
different types of properties, classification,  Assignment-
nanomaterials quantum dots, nanowires, Report
 Explain the nanosize nanorods, nanoshells,  Quiz
natural molecules and nanotubes, nanofluids,  spot Test
their applications nanofantasies, applications of
nanomaterials, nature: the
best nanotechnologist,
challenges and future
prospects.

 Describe the methods of 2. Synthesis Routes: Bottom  Lecture  Short

preparation –up approaches: Physical  Assignment question/MCQ
 Explain advantages and vapor disposition (PVD),  Essay question
disadvantages of one Chemical vapor deposition Assignment-
synthesis method over (CVD), spray conversion Report
others processing, sol-gel
process, wet chemical  Quiz
synthesis, self-assembly;  spot Test
Top- Down approaches:
mechanical alloying and
nanolithography.

11
 Describe the principle of 3. Tools to characterize  Lecture  Short
nanomaterial Nanomaterials: Microscopic,  Assignment question/MCQ
characterization spectroscopic and diffraction  Essay question
techniques techniques.  Assignment-
 Explain the relation of Report
one technique with  Quiz
others  spot Test
 Describe the process of 4. Nano particles:  Lecture  Short
metal nanoparticles,  Assignment question/MCQ
a) Metal nanoparticles:
metal oxide  Essay question
Synthesis, properties and
nanoparticles ,  Assignment-
applications of gold and
nanorods, nanowires and Report
silver nanoparticles.
nanotubes synthesis  Quiz
b) Metal oxide
 Describe the important  spot Test
nanoparticles: Synthesis,
uses of carbon and
properties and applications
inorganic nanomaterials
of iron oxide, zinc oxide and
titanium oxide nanoparticles.
c) Nanorodes and
Nanowires: Synthesis,
properties and applications
of gold, silver, zinc oxide and
titanium oxide nanorodes
and nanowires.
d) Nanotubes:
Classifications, synthesis,
properties, and applications
of carbon and inroganic
nanotubes.
 Describe the 5. Applications of  Lecture  Short
fundamentals of nano- Nanomaterials:  Assignment question/MCQ
electronics, nanosensors, Nanoelectronics, Micro and  Essay question
nanobiosensors nano- electromachanical  Assignment-
 Describe the systems, Functionalization of Report
applications and nanomaterials (CNTs and  Quiz
important uses of Graphene), nanosensors,  spot Test
nanomaterials in various Nanocatalysts, food and
fields agriculture industry, cosmetics
and consumer goods,
structure and engineering,
water treatment and the
environment, nano medical
applications, textiles, paints,
energy, defense and space
applications, structural

12
 applications.

Books Recomended:

1. Murty, Sankar, Baldev Raj, Rath and Murday : Textbook of Nanoscience and Nanotecnology,

Univrsity Press (india)

2. Charles P. Poole, Jr., Frank J. Owens : Introduction to Nanotechnology, Wiley India edition.

Semester: 4th year 2nd Type: Practical Full Marks: 100 Credits: 1.5

Course Title: Pharmaceutical Chemistry Lab Course Code: CHEM 4212

Rationale: The understanding of pharmaceutical chemistry of different medicinal compounds is

important for the practical use of them in health science and laboratories. The study of different

techniques of advanced chemistry is also very essential for research and industrial purposes.

Student must lean the properties, synthesis methods, estimation of the ingredients from

medicinal compounds and principle, instrumentation and determination of analytes by advanced

techniques.

Course Learning Outcomes (CLOs): Synthesis and quantitative determination of the

ingredients from pharmaceutical compounds and other common commercial compounds.

Unit Learning Outcomes Course Content Teaching Assessment

(ULOs) Learning Strategy
Strategy

 Discuss the extraction Experiment No-1: Extraction of active  Lecture,  MCQ,

process. pharmaceutical ingredients from  Assignment,  Assignment
 Describe the principle commercial tablet, acetylsalicylic acid  slide show, Report,
of TLC. from aspirin, its synthesis in  Observation,
 Explain the laboratory and comparison of two  Experiment,
mechanism of samples by melting point and TLC.  Viva
pharmaceutical
ingredients against
diseases.
 State the function and Experiment No-2: Estimation of  Lecture,  Assignment
composition of vitamin C by titrating it against a  Assignment, Report,
vitamin C. solution of 2,6- dicloro phenol indole  slide show,  Observation
dye.  Exercise

 Explain the Experiment No-3: Synthesis of  Lecture,  MCQ,

13
 mechanism of nickel ammine complexes of Ni (II) and its  Group  Assignment
complexes synthesis. ligand exchange reactions (e.g. discussion Report,
bidentate acetylacetone, DMG,  Exercise  Observation
glycine) by substitution method.

 Discuss kinetic and Experiment No-4: Controlled  Lecture,  MCQ,

thermodynamic study synthesis of two copper oxalate  Exercise  Assignment
on rate of synthesis. hydrate complexes: kinetic vs Report,
thermodynamic factors.  Observation
 Explain the Experiment No-5: Study the 200-  Lecture,  MCQ,
mechanism of UV- 5000nm absorbance spectra of  Assignment,  Assignment
Vis spectroscopic KMnO4 and K2Cr2O4 (0.1 Report,
method and its MH2SO4) and determine th max  Observation
spectra. values. Calculate the energies of
the two transitions in different
units(Jmolecules-1,kJ mol-
1
,cm,eV)
 Describe the formula Experiment No-6: Quantitative  slide show,  MCQ,
and preparation of analysis of aspirin.  Exercise  Assignment
aspirin. Report,
 Prepare and explain Experiment No-7: Synthesis of  Assignment,  MCQ,
the methods of silver silver nanopaticles and their  Exercise  Observation
nanoparticles spectroscopic characterization.
synthesis.
 Describe the Experiment No-8: Determination  Lecture,  Assignment
methods. of Fe-content in an iron tablet.  Assignment, Report,
 slide show,  Observation
 Mention major Experiment No-9: Degradation of  Assignment,  MCQ,
pollutants and their pollutants by advanced oxidation  slide show,  Assignment
degradation. process.  Exercise Report,
 Explain the principle Experiment No-10:  Lecture,  Assignment
of UV-Vis Determination of Fe(II) content  Assignment, Report,
spectroscopy. in the supplied solution by UV-  Exercise  Observation
VIS spectroscopy.

Books Recommended:

1. A.I. Vogel : A Textbook of Practical Organic Chemistry

2. Shiriner, Fusion & Curtin : Systematic Organic Analysis

3. H.T. Clarke : Practical Organic Chemistry

4. A.I. Vogel : Elementary Practical Organic Chemistry Part I, II & III

5. J. Bassett & others :Vogel's Textbook of Quantitative Inorganic Analysis

14
6. Skoog & West : Fundamentals of Analytical Chemistry

7. Schwarzenbach & Flaschka : Complexometric Titrations

8. Fahan : Materials chemistry, Springer 2004

Course Code: CHEM 4000 Course Title: Project/Project Design/Intership

Full Marks: 100 Credits: 3.0

Marks Distribution

Report : 60 Marks

Presentation/Viva : 40 Marks

** Examination committee will evaluate the presentation/viva including the report.

Course Code: CHEM 4200 Course Title: Viva Voce

Full Marks: 100 Credits: 1.0

This course includes the assessment of the students through oral examinations (all chemistry courses of
all semesters) by the members of the relevant examinations committee.

15