Date

Page No..(32
Expt. No. . 3
62)
Am To dettt the prcgenct of idicand basic
hadical In Ggiven Salt.

Clou >bue dlou 0douylessAlali (yslallne

1et for aidicradica
Expenmemt Obseryahony nteremce
Tadko
Salt+ d M,O No gaserolvcd L group absent

Salt + Conc. H SO4 ungnt Sntlling Lgroue prsent

aybc
3: Watr enractt onc White pht, okuble CConfhrmed
HNO AgNO a) intccss NH,OH

Test for basic ndical:

boherment Obseryathon 4nference

Salt NaOM NoShmell of dmmoria 0 Grauh absent

0S+ dil HC No bt grou absent

3 Abovc So divyde
mto barle
mo pp T grou abset

T art +NH,CtNM, O ppt L I qrou abscnt

Teacher'sSigngture
 (32
On

2HU+ So
2u+M S04
ConC
tunn
AqC t NOg
AgNO WAite Fpt

Ag C
NA3
Souble Comple
Rehion for
CoR
ion
Co+ s
CoS
CoS+2Ml-O CoCt0+S
(aqa nega)

(o+4Nn,NS Nh4 Co (CNS)

8&ue Calour Complexk
 Date

Expt. No. Page No.---.

33
Aot So+ HSt M 6ock pp T Qroup þreseat
t NHOn

S Above bpt. t, aqua reqia pt dissolvg N2 or Co*

may be.

Aboc +actone 6luc Colour Co Corimed

NMN 4s

Acidic Yadical
ResuRt Co2t
Bosic
 Date

Expt. No. 14 Page No.

(34)
Aini o detect the restnce OF u dic and basic
radicaIn givem Salt and jckmthfy hem
(alo _qreen odou clate Bystalln
Ocidic r a d i c a ) : Odouwle
Teat for

Dxpcrtm Cnt Observahon feremCe

Salt+ di h,so no as evolrcd Lgrouh ksent
Br
Salt+ ConC ,SOP4 bYOwnqa NO3aybt.
3Waterentratt t asly Brownnng N onfirmed
praredeso, so" +
ormed a
Con H SO (ot ongle unchon of
tost tube Hwo uids
of 6o along

1est or ocidic radical

xtnmenT
Observathon 4nftrcnCC
Salt NoOn NoSvnell Of NHg Ogrou obsca
No p grou bsent
[Link]
into
3 Above Solh dividt
2 barts: graup absert
I Port t H2 S
Teacher's Signature
Rachon fo 34
(34
NO3 ior

NO HT MNO

2nNO3 6FS0 4 T3,so 4 3FSOu)3

t 4M0 tANO

Fe SO + NO fesOy. NO. S H,
5M Bro
 Date

Expt. No.. Page No..2

(35
Thart t NM,OM No p L greu abstnt
tNHCtConc HNO

4AbortSol" NnC Black ppt TYgrouppreaemt

N2c maybe
Abore ppt0ua diusolvcs
hega
AboYc so divide into
2 6arteNHyOH
T art f dimethyl Qlyonng red ppt N2 Confimed
no ppt
art tommoniwm
thiocyae

Regul Audio odical NO

Ni
Bagic
Rachon r
N
2
On
35
2-
N2 S NiS
Nack pp

NS+ t LO NCT H0+S

QH
NOH N
N 2 CM N
N-C-
C=NOM ,C-C=EN N-C-
OH

Ped
CH NON
 Date
Expt. No.. 5. Page No..36
36)
Am lo detrmine the molarnts_ogiven oluhon
NaOM by tiatin9it gam8t gandard olution
o Oxalic acid

Theor y 1he itatmg beteen Oxalic gud dnd NaO Is

on exanmble of dcd- base eacton.
M,GO4 t R1,0t 2NaOH Na,O+ 4hOo
indicgtor n thishenolphthalein s 0std 08 gn indicator
At the end oint the Colour changes fror
colour Peb8 to bink.

MoteriaReauired 8ure teipette Conical Xoak_beaker

Uhne Burete sand oxalic acid
NaOH phetolphrthalein
Ohaer vation
Stto burette Reding Vounne Of NaO Consordant
Inihia) fmal(y) -V)
2u-5m
Reada
O.0 245
22.0n 22-0 mnl a2.0
O-o 22.0
22 0 m
O.0

Volune of OKalc ocid token 25 m

Molaty is alulatcd tsing orrlila

CaloWghon
Teacher's Signature:
Oxalt cd/NaOM GRudahons
M,V
(7
2
oOXnÁ2R
MaX8 2

M
 Date

Expt. No.. Page No.

No
M- Molartho of oxalit acid
M. .2 uho = vekume ot
nolarnty of Naon sal
V6lume of
seniyy NaoH 1
mol

Reult The Brthgth of

recaution: Rmse he burette and [Link] ith the s01
o be taken in it
Take the burettc readinq Carefully.
Expt. No. 6 Date

Am: 8 Page No. 33.

loþrelare
mmonLw
1/s 8tandard solution ofkrrous
olanty Of gven SuRphate. Using Saluhon and find
ind out
KMnO oluthon out
Atharahi8 Weighng tube, Weigh box, masuring
buret ibette Conicallask ask
stand
Malenal Reauired Mohr
dil H,SO,, sa!tFeso4.(N, SO4 6H0
dish2led water KMnO430"
4ndicstov KMnO4 is a Sef indicator.
Thegry kMnO4 Oxidses fe* Fe in
Ocidic medum
nd
teeqets neduced to olourless Mn
O + 5R*+ 8t MnatMn25F3+41,0
eare 250 of M2s Mohr's salt
Weight of Salt requiled Ix Mohr galt
25x
392 3:92 9

Obgervation: ()
4070
wt of mphy weghing tube =
s
) Wt of embty weghng ube Mohr's sat
7.9912
Salt
Wt of Mohr's 392g
olume of Prepored RSOm
Teacher's Signature:-
 Date
Expt. No.. Page No. 39)
(39
Malarty o Mohr's çalt M/25
Obseyvation talble

StN Surette Regding orCondat

Inial Friod (a KMinO ed[V,-v,) readng

2-8 28 20:3
3. 20.3 293 m
20 3 m
20 3

Volume o Mohs galt 80" token ts 25m

Forla vsed
(alcuwahon 5 No
25 LO
MV Mohr 8alt ol
wheren- bXarity Mohr's 3alt go
V Volume of M,51
Molgrity of KMnO4 5T 20 3) 4o
V Volunc Of M0.O097
Molanity of_KnOy o is 0.0097 / L
Reaut
he buette
Rinse the
K
ipete with so to
PreCouhoni (i) taken in it
be
(i) lake the
burette readings Corefully
 Date

Expt. No. 7 Page No.

Hn: detect cldic nd basic radical in qven

Sat
odous- odoulosu a l i
Tcs tor aCidic [Link]:
xperiment Obaervatn reren(e
Salt+ dil H,S04 Brisk effenestence Coa maybe

Ahorc q08+ aOH2- So turs mky CO2 nfrmed

1egt for_ basic rgdica:

Obser vatihon gnerence

No Smele o O qrau ahsent

Salt + NaoH
drmmonia

OS-+ d HC No pt group absert.

3Abore pI" diiide mto

2arts grou oksent
T ort t NHOn Ao ppt. lI grou absent

NH
Above Sal:divide

Teacher's Signature
Tet fo
(
(40
O*+ so SO tHO + CO
dil

CO+ CaP Cco,+ h0

Reachion for
2+

HPO4+NH, g (NM)PO4
Cryst. uhte pT.
+H
 Date

Page No.
Expt. No.
(
exe3
No ht N grou absent
No p 1 qroub absemt
Tart (N),P
Above t ystol Whtt pt. Vgrou bresent
Na,HPO4 and Ma onfirmed.
serh innr Jartaf ksfbe
h

CO
Auidic radicali CO
Rezult
basio adical Mg2+
 Date
Expt. No. 18 Page No..(42)

Test for Carbon Hd Hycroge

Experiment Ohsery0tion fertne
Brisk cffervcs CenCe mayhe

fbove aQs Whitep regem

Cebu
3Pbovc So+ SIm turns bluc Hhresent

Test for Ntrogem

benmnt
bservahon erence
u Sodun tuaion extract rupean blue Nitrogen 1s
+ Lolour
ConC
Reaction fos
C 42
+2GuO +CO,CO2
A
CuO Cu+H,O
CO+ OM)
5h,o+ CSO4 CusO. 5H20
white

Reachon
N

6CN Fe2 FeC)

3 Fe(CN) +4Fe 3
x HO Fe FeCN),. n
Prus s on ue

fervi fero yce

 Date
Expt. No...19.
Page No..(43).
egt orSwphur
4,
xemmt Obseahom

Sodfupian exhract+ Wack pbt Sushuri

Cchc acud + cad pregent
OCctatc

(2Soduw fuzjian Cxhroct Vio Ret Sulhhur is

Sodium NHoprusde Colsur restt

Nrogem nd Suphur both br mt

Test for
b e r l a n Cmt Observaton 4nerence
exfractf Blasd recd N&S oth
Sod u Sion
+FcSCO4 * present
Conc. H2SO4
 Reacho

x Pb+
2 Pb S
lock pt.

2
s2 Fe() elcN), NoS

ViJet colaur

r
eaion
N & S

Na+ C N+S
Na SCN
Sochun hio cyanate

Fe3+ SN
F (sCN131
beod ed elsur
 SCIENCE&TECHNOLOGY
Experiment No...
Experiment No. O PRACTICAL MANUAL Date
Tegt for Halogená 44
Exhermdnt Obseryahgn 4nfereme
O Socd ujion exhact- urdywhte i6 preseat
Conc HNO,+ gN O| pt souble
in NHOH

2 9d fusion Oxtract+ yeo pp Bris restet

con. HNo,t AgNO, orholly selule
in NMOH

Sod fupion extacct+_ YelLs p 1 is þrege

3 inolulc Im
Conc: HNo3+ AgNG
NHOH

Tegt for Phesphorug

Xperlmnt bseryaion
SR is Pis rescnt
Or orp+hLo
ormed

(2) AborcS o + ConC

HNa,t amrmomin

mokabdale
 Reacthon
f o r h ogen

(L4
Aa AgX (s)

Reacnon

Na,PO,+3MNo, hPO+ 3NaNO

Po 12 NH, ,MoO, + 21
HNO
(NM)PO RMoO
+
NH,NO, 4+ I2 HD