Elastic Recovery of Impression Materials
Elastic Recovery of Impression Materials
Abstract Aim: The aim of the study was to investigate the effect of disinfection and steam autoclaving on the elastic
recovery of three different elastomeric impression materials.
Settings and Design: In vivo - comparative study.
Materials and Methods: Ninety dumbbell‑shaped specimens of commercially available two addition‑cured
silicones (AFFINIS and AQUASIL) and one condensation‑cured silicone (SPEEDEX) impression materials were
prepared and treated with chemical disinfectant and steam autoclaving. Specimens were seal packed and
sent to laboratory for testing elastic recovery. After the specimen had been pulled to failure, the broken
parts were fitted back together, and the distance between the marks was measured using an electronic
Vernier caliper.
Statistical Analysis Used: one‑way analysis of variance test and Tukey post hoc test for multiple
comparisons.
Results: The result showed significant difference in elastic recovery of AFFINIS when it was disinfected and
steam autoclaved whereas elastic recovery showed no significant difference when SPEEDEX and AQUASIL
were disinfected and steam autoclaved. Similarly, results were alike when AFFINIS, SPEEDEX, and AQUASIL
were compared on disinfection. However, significant difference was noted on steam autoclaving, highest
being the mean value of AFFINIS.
Conclusion: Within the limitations of this in vitro study, conclusion was made that the elastic recovery
of AFFINIS was the least which improved with disinfection and autoclaving. Elastic recovery of
SPEEDEX and AQUASIL was similar. However, all the three materials used in the study can be safely
sterilized after clinical use and before being sent to the laboratory without significantly affecting
their elastic recovery.
Address for correspondence: Dr. Garima Gothwal, H‑3 Hetnagar, Udhasar Fanta, Jaipur Road, Bikaner ‑ 334 003, Rajasthan, India.
E‑mail: [email protected]
Received: 2nd August, 2019, Revision: 3rd September, 2019, Accepted: 20th September, 2019, Publication: 10th October, 2019
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How to cite this article: Gothwal G, Meena S, Padiyar UN, Sharma HK,
DOI: Kaurani P, Singh DP. Comparative evaluation of elastic recovery of three
10.4103/jips.jips_277_19 different elastomeric impression materials on chemical disinfection and
autoclaving: An in vitro study. J Indian Prosthodont Soc 2019;19:345-52.
© 2019 The Journal of Indian Prosthodontic Society | Published by Wolters Kluwer - Medknow 345
Gothwal, et al.: Comparative evaluation of elastic recovery of three different elastomeric impression materials
materials that have received a lot of attention are irreversible withstand the sterilization procedure and yet can produce
hydrocolloids, polyethers, polyvinyls, and polysulfides.[1] an accurate cast.[7] A survey was done by dentists and
found that 50% of the dental professionals would favor an
In the clinical scenario, a set impression is a pool for
nYQp/IlQrHD3i3D0OdRyi7TvSFl4Cf3VC1y0abggQZXdtwnfKZBYtws= on 11/28/2024
fitted back together and the distance between the marks was sterilization group. On the other hand, one way ANOVA and
measured using an electronic caliper with a resolution of Tukey test evaluated no significant difference in the mean
0.01 mm after 2 h [Figure 11]. The change in length (Δ L) values of elastic recovery of AQUASIL and SPEEDEX
was measured, and percentage deformation was calculated when they were disinfected, sterilized, and left untreated in
which ultimately provided the elastic recovery. Tables 3, 4 and Graph II and III .
Data were entered in Microsoft Office Excel. Appropriate Effect on control groups of each material
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statistical tests were used to find significant association with In Table 5 and Graph IV, when the three impression
the help of Mini Tab Version 18 software (Headquartered in materials were compared among each other using one‑way
State College, Pa., Minitab, LLC. operates offices in Phoenix, ANOVA test and Tukey test, no significant difference was
Arizona, Chicago). P < 0.05 was considered as statistically
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a b c
Figure 5: (a‑c) Loading of impression material in the die
348 The Journal of Indian Prosthodontic Society | Volume 19 | Issue 4 | October-December 2019
Gothwal, et al.: Comparative evaluation of elastic recovery of three different elastomeric impression materials
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nYQp/IlQrHD3i3D0OdRyi7TvSFl4Cf3VC1y0abggQZXdtwnfKZBYtws= on 11/28/2024
a b
Figure 8: (a and b) Autoclaving elastic recovery specimens
a b
Figure 9: (a and b) Disinfection of elastic recovery specimens
Effect of sterilization
The comparison was done among three test specimens
for elastic recovery on sterilization using one‑way
Figure 11: Broken elastic recovery specimen
ANOVA test and Tukey test. According to Tables 7 and
8 and Graph VI, a significant difference was found in DISCUSSION
the mean values of elastic recovery of AFFINIS when
compared to SPEEDEX and AQUASIL. AFFINIS The increasing risk of cross‑infection from patient to
being the highest while AQUASIL and SPEEDEX were clinicians which is carried forward to the dental technicians
almost alike. through the dental impressions is a topic of interest these
The Journal of Indian Prosthodontic Society | Volume 19 | Issue 4 | October-December 2019 349
Gothwal, et al.: Comparative evaluation of elastic recovery of three different elastomeric impression materials
99 98.8
98.5 98.75
(I)Descriptive (II) Descriptive
Statistics of 98.7 Statistics of
98
Elastic 98.65 Elastic recovery
97.5 recovery of of SPEEDEX (%)
98.6
AFFINIS (%)
97 98.55
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96.5 98.5
1A 2A 3A 1B 2B 3B
98.7 99
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98.55 97
1C 2C 3C 1A 1B 1C
99 99
Graph (I, II, III, IV, V, VI): Descriptive statistics of elastic recovery of AFFINIS, SPEEDEX, and AQUASIL
Table 5: Descriptive statistics of elastic recovery of AFFINIS, laboratory directors in 2000 revealed that the majority of
SPEEDEX and AQUASIL (%) impressions were made of PVS (57%) or polyether (27%)
Group n Mean SD P
materials. Only 44% of the respondents said that they
Group 1A 10 97.6 0.318 >0.05
Group 1B 10 98.7 0.3128
knew if the received impressions were disinfected or not.
Group 1C 10 98.7 0.1823 Whereas, 23% had no idea about the methods used for
SD: Standard deviation disinfection and 47% did not know about the length of time
involved in disinfection. About 45% of the respondents
Table 6: Descriptive statistics of elastic recovery of AFFINIS, stated that they received inadequate information regarding
SPEEDEX, and AQUASIL on disinfection (%) the disinfection procedure. Thus, it shows that there was
Group n Mean SD P
definite lack of communication between team members,
Group 1A 10 97.6 0.318 >0.05
Group 1B 10 98.7 0.3128
and also, the problem was not only associated with the
Group 1C 10 98.7 0.1823 material being used for making impressions but the
SD: Standard deviation disinfection technique which was being used.[12]
Table 7: Descriptive statistics of elastic recovery of AFFINIS, Holtan et al. in 1991 conducted a study in which PVS
SPEEDEX, and AQUASIL on sterilization (%) impression material (President) was sterilized using
Group n Mean SD P steam autoclave and an ethylene oxide gas autoclave. He
Group 3A 10 99.0 0.2976 <0.05
Group 3B 10 98.6 0.2161
established that models made from ethylene oxide sterilized
Group 3C 10 98.6 0.2808 impressions were acceptable to use in fabricating fixed
SD: Standard deviation or removable prosthesis, while the models made from
impressions sterilized in a steam autoclave can be used for
days. To protect the dental clinicians, a standard protocol the fabrication of diagnostic casts and some transitional
for disinfection and sterilization of dental impressions prostheses, but not for routine construction of crowns or
is recommended.[11] A survey documented in U.S. dental fixed partial dentures.[7]
350 The Journal of Indian Prosthodontic Society | Volume 19 | Issue 4 | October-December 2019
Gothwal, et al.: Comparative evaluation of elastic recovery of three different elastomeric impression materials
Table 8: Tukey pairwise comparisons grouping information an impression from mouth and cast is easiest in light bodied
using the Tukey method and 95% confidence of AFFINIS, silicones followed by light‑bodied polysulfides, heavy body
SPEEDEX, and AQUASIL on sterilization (%)
silicones, heavy body polysulfides, and polyethers. According
Factor n Mean Grouping Factor
3A 10 99.0 * 3A
to fracture mechanics theory, failure of an impression is due
3B 10 98.6 3B to the stresses at a critical or weak point. Therefore, modulus
3C 10 98.6 3C of elasticity and tear strength are related.[17,18]
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with AFFINIS showing the best results steam autoclave sterilization. J Prosthet Dent 1991;65:519‑25.
8. Giammanco GM, Melilli D, Rallo A, Pecorella S, Mammina C,
3. On steam autoclaving, AFFINIS showed a remarkable
Pizzo G. Resistance to disinfection of a polymicrobial association
improvement in its elastic recovery, whereas there was contaminating the surface of elastomeric dental impressions. New
no significant change in elastic recovery of SPEEDEX Microbiol 2009;32:167‑72.
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4. Considering the importance of need for sterilization Dent J 1992;37:346‑52.
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of impressions, the three impression materials tested 10. ASTM International. ASTM D412‑06ae2, Standard Test Methods for
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the elastic recovery from a clinical point of view. Conshohocken, PA: ASTM International; 2006.
11. Infection control recommendations for the dental office and the dental
laboratory. Council on dental materials, instruments, and equipment.
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