PM/ IS 1117/1 June 2021

[Link]

उत्पादमानुयल
LABORATORY GLASSWARE – SINGLE - VOLUME PIPETTES
IS: 1117:2018/ISO 648: 2008 केअनुसार

PRODUCT MANUAL FOR

LABORATORY GLASSWARE – SINGLE - VOLUME PIPETTES
ACCORDING TO IS 1117:2018/ISO 648: 2008

भारतीय मानक �ूरो - िविनयम की �ीम ( अनु �पता मू �ां कन)I के तहत यह उ�ाद मानु यल प्रमाणीकरण के
प्रचलन मे रीित और पारदिश� ता के सुसंगता सुिनि�त करने के िलए सभी �े त्रीय शाखा काया� लयों एवं लाइसे�
धा�रयों �ारासंदभ� सामग्री के �प मे उपयोग िकया जाएगा। बीआईएस लाइसे� प्रमाण पत्र प्रा� करने के इ�ु क
भावी आवेदकों �ारा भी इस द�ावेज़ का उपयोग िकया जा सकता है ।

This Product Manual shall be used as reference material by all Regional/Branch Offices &
licensees to ensure coherence of practice and transparency in operation of certification under
Scheme-I of Bureau of Indian Standards (Conformity Assessment) Regulations, 2018 for
various products. The document may also be used by prospective applicants desirous of
obtaining BIS certification licence/certificate.

उत्पाद
1. : IS 1117:2018/ ISO 648 : 2008
Product
शीषर्क
: Laboratory Glassware - Single- Volume Pipettes
Title
संशोधनसंख्या
: Nil
No. of Amendments

नमन
ु ाकरण�दशा�नद� श
2.
Sampling Guidelines:

Single-volume pipettes shall be manufactured from glass

कच्चामाल of chemical resistance and thermal properties at least to
a) :
Raw material HGB3 in accordance with ISO 719, shall be as free as
possible from visible defects and reasonably free from
internal stress.
सम�ू हकरण�दशा�नद� श कृप्या ANNEX – Aदे ख�
b) :
Grouping guidelines Please refer Annex- A

1
 PM/ IS 1117/1 June 2021

नमूनेकाप�रमाण
c) : 6 Nos
Sample Size

पर��णउपकरणोक�सच ू ी कृप्या ANNEX – B दे ख�

3. :
List of Test Equipment Please refer ANNEX –B

�नर��णवपर��णस्क�म
कृप्या ANNEX – Cदे ख�
4. Scheme of Inspection :
Please refer ANNEX –C
and Testing

5. एक�दनम� संभा�वतपर��ण/Possible tests in a day :

All tests except Material as per cl.7.1

6. लाइसेन्सकाकायर्�ेत्र/Scope of the Licence :

IS1117:2018/ISO 648:2008 के अनुसार मानक मुहर का उपयोग करने के �लए लाइसेन्स
�नम्न�ल�खत कायर्�ेत्र के �लए प्रदान �कया जाता है
Licence is granted to use Standard Mark as per IS 1117:2018/ ISO 648 : 2008 with the
following scope:
Name of the product Laboratory Glassware - Single- Volume Pipettes
Class A/AS/B
i) For which no waiting time is specified (Classes A and B)
Types
ii) For which waiting time of 5 s is specified (Class AS)
0.5, 1,2,5,10,20,25,50,100 or any other intermediate capacity
Capacity (in ml)
between 0.5 to 100 ml
Any other aspect
required as per the One-Mark/Two-Mark Pipettes
Standard

BUREAU OF INDIAN STANDARDS

ManakBhawan, 9, Bahadur Shah ZafarMarg,
New Delhi – 110002
 PM/ IS 1117/1 June 2021

ANNEX A TO THE
PRODUCT MANUAL FOR
LABORATORY GLASSWARE - SINGLE-VOLUME PIPETTES
ACCORDING TO IS 1117:2018

GROUPING GUIDELINES

IS 1117:2018/ISO 648:2018 classifies two types of Single -Volume Pipettes :-

1) Those for which no waiting time is specified (Class A & B)

2) Those for which a waiting time of 5s is specified (Class AS)

The following Accuracy classes have also been specified:-

1) Class A & AS for the higher grade

2) Class B for the lower

Based upon the above classification, the following grouping guidelines shall be considered for
the purpose of GoL/Inclusion:-

1) One sample of each Accuracy class and Type of a Pipette shall be drawn and tested to
cover all the Accuracy classes and Types intended to be covered in the scope of the licence.

However, the above samples shall also include samples of the lowest and highest capacity (in
ml) of the Pipettes intended to be covered in the licence.

2) If sample of accuracy class A/AS is tested, Class B may also be covered in the scope of the
licence.

3) Firm shall declare the varieties of the Pipettes they intend to cover in the licence and the
scope of licence shall be restricted based on the manufacturing and testing capabilities of the
manufacturer.

4) During the operation of the licence, samples of each variety covered in the scope of the
licence shall be drawn by rotation.
 PM/ IS 1117/1 June 2021

ANNEX B TO THE
PRODUCT MANUAL FOR
LABORATORY GLASSWARE - SINGLE-VOLUME PIPETTES
ACCORDING TO IS 1117:2018

List of Testing Equipment

Sl. No. Tests used in with Clause Test Equipment

Reference
1 Maximum Permissible 1) Weighing balance LC-0.1 mg range 200 g
errors(Cl 6)
2) Stop watch

3) Thermometer LC-0.1 C range -10 to -

110℃

4) Barometer (L.C.1 kPa)

5) Air conditioner (AC)

6) Hygrometer (Range 35% to 85% ± 5%)

7) Distilled Water

8) Conical Flask with ground joint

2 Material (cl.7.1.) 1) Grade 2 water

2) Hydrochloric Acid
3) Acetone
4) Methyl Red Indicator Solution
5) Distilled Water
6) Analytical Balance
7) Burette
8) Pipette
9) One-Mark Volumetric Flasks
10) Conical Flasks, Boiling Flasks
11) Beaker
12) Weighing Bottle
13) Dessicator
14) Magnet
15) Mortar and Pestle
 PM/ IS 1117/1 June 2021

16) Sieves ( 500 μm,300 μm, 600 μm to 1000 μm)

17) 200 mm diameter Square-aperture sieves
18) Stainless Steel Mesh
19) Ball-mill
20) Ultrasonic Cleaner
21) Drying Oven
22) Thermometer
23) Heating Bath
24) Rubber or Plastic Coated Glass Rod

3 Dimensions (cl.7.4) 1)Steel Scale

2) Ball ended micro meter
3) Vernier Calipers
4 Delivery Time (cl.7.7) 1)Stop watch
2)Distilled water
3)Glass Receiving Vessel
3 Graduation line Cl 8 1)Steel Scale
2) Ball ended micro meter
3) Vernier Calipers
4 Setting of meniscus Cl 9 1)Steel Scale
2) Ball ended micro meter
3) Vernier Calipers

4) Protractor

The above list is indicative only and may not be treated as exhaustive.
 PM/ IS 1117/1 June 2021
ANNEX C TO THE
PRODUCT MANUAL FOR
LABORATORY GLASSWARE - SINGLE-VOLUME PIPETTES
ACCORDING TO IS 1117:2018

Scheme of Inspection and Testing

1. LABORATORY - A laboratory shall be maintained which shall be suitably equipped (as per the requirement given in column 2 of Table 1)
and staffed, where different tests given in the specification shall be carried out in accordance with the methods given in the specification.

1.1 The manufacturer shall prepare a calibration plan for the test equipment.

2. TEST RECORDS –The manufacturer shall maintain test records for the tests carried out to establish conformity.

3. LABELLING AND MARKING –The Standard Mark as given in Schedule of thelicense shall be inscribed on each pipette
indelibly/permanently, provided alwaysthe laboratory glass ware single-volume pipettes thus marked conforms to all therequirement of the
specification.

3.1 Marking and packing shall be done as per the provisions of the Indian Standard. If colour coding is used, it shall comply with the
requirements of ISO 1769. In addition, BIS Licence number i.e. CM/L--- and details of BIS website shall be marked permanently and
prominently on the external packaging as follows: “For details of BIS certification please visit www [Link]”

4. CONTROL UNIT – – For the purpose of this scheme, pipettes of the same class and nominal capacity produced in one day shall
constitute a control unit.

4.1 On the basis of test results, decision shall be taken regarding conformity of the control unit as a whole to the requirements of the specification.

5. LEVELS OF CONTROL - The tests as indicated in Table 1 and the levels of control specified therein, shall be carried out on the whole
production of the factory covered by this scheme and appropriate records and charts maintained in accordance with paragraph 2 above.

5.1 All the production which conforms to the Indian Standard and covered by the licence should be marked with Standard Mark.
 PM/ IS 1117/1 June 2021

6. REJECTIONS – Disposal of non-conforming product shall be done in such a way so as to ensure that there is no violation of provisions of
BIS Act, 2016.A separate record providing the detailed information regarding the rejected control units and mode of their disposal shall be
maintained, such material shall in no case be stored together with that conforming to the specification
 PM/ IS 1117/1 June 2021

TABLE 1
LEVELS OF CONTROL

Test Details Test Levels of Control Remarks

Clause Requirements Test Method equipment No. of Frequency
Clause Reference requirement Samples
R:required (or)
S: Sub-
contracting
permitted
6 Maximum Table I IS 1117:2018 R Each - All the samples shall comply
permissible Pipette With the requirements
errors
7.1 Material (Freedom 7.1 IS 1117:2018 R -do- - -
from Visual
defects and
internal stress)
7.1.1 Material IS 2303 S One Each
(Chemical resistance (Pt1/Sec consignment No testing required if the
and thermal 1):2012 / ISO consignment being received is ISI
properties of glass) 719 marked or accompanied by a test
certificate from supplier showing
conformity to the requirements of IS
2303 (Part 1:Section 1):2012/ISO 719.
7.2 Shape 7.2 IS 1117:2018 R Each Pipette - -

7.3 Bulb 7.3 -do- R -do- -

7.4 Dimensions Table 2, -do- R Two Pipettes Every hour
3&4
7.5 Top of pipette 7.5 -do- R -do- -
7.6 Delivery jet 7.6 -do- R -do-
7.7 Delivery time 7.7 -do- R Two Each control
unit
7.8 Waiting Time 7.8 -do- R -do- -do- Applicable for class AS pipettes
8 Graduation line 8 -do- R -do- -do-
 PM/ IS 1117/1 June 2021
9 Setting of the 5.7 IS R -do- -do-
meniscus (Annex 8729:2018/
A) ISO
384:2015
11 Visibility of 11 -do- R -do- -do-
graduation line,
figures and
inscriptions

Note 1: Whether test equipment is required or sub-contracting is permitted in column 2 shall be decided by the Bureau and shall be mandatory. Sub-
contracting is permitted to a laboratory recognized by the Bureau or Government laboratories empanelled by the Bureau.

Note 2: Levels of control given in column 3 are only recommendatory in nature. The manufacturer may define the control unit/batch/lot and submit his own
levels of control in column 3 with proper justification to BO head.