‘embe Wes experiment (titration) Distrie\/2024 02 August 2024 LIMPOPO PROVNCUL GOVERNMENT || WRRCO UWA Iaith coroasrwert oF i$] 9 | 35] so EDUCATION aoe | VHEMBE WEST DISTRICT NCES PRACTICAL WORKSHEET GRAGE 12 PRESCRIBED EXPERIMENT 2 OF 2024 | PHYSICAL SCI BATION The outcomes! skills being instilled and evalueted: Ability to, Handle apparatus Make observations Follow instructions Record data Fresent data + Manipulate data in carrying out the necessary calculai The experiment aims to demonstrate the accuracy of the titration method in determining the ncentration of an unknown acid or base, using the standard solution. 't is also intended to determine the concentration (in mol.dm*) of a given solution of sodium hydroxide by titration with the prepared standard solution of oxalic acid.Grade 12 Practical experiment (titration) Nsc Vhembe West District/2024 tod blow The spor hemicals available to you are ‘odium hydroxide solution of unknown concentration xalic acid solution of known concentration tte in stand + Pipette Nash Bottle + Phenoiphthalein and Bromothymo! Blue indicators Beaker juratte stand and @ ciamp Experimental Set-up 1 Apparatus A filed to the mark with acid Apparatus B ith base + indicator Procedure Rinse a conical flask with distilled water. 2. Collect about 120 mi of the NaOH solution in Use @ pipette to place 25 cm? of the NaQH,rade 12 Practical experiment (tity Add 5 drops o' Note ; ation) Nsc /hembe 1 Distriet/2024 t Phenolphthatein indic the colour of t ator alkali with the indicator ’ me coal - es 4 of known concentration (a standard solution) . 2G2Qx acid solution and allow a small amount to drip out so as to tap and the outlet he level of the acid must be exactly on the 0 ml mark on the burette for just below if you wi Note the initial level of the HoC20. in the burette 1 Titrate the H2C.0; acid into the flask which must be swirled constantly. Add about 1 cm’ ata time as a test run. Note the volume when the solution changes colour. Calculate the approximate volume of H2C20, acid required for neutralisation of the 25 cm*® NaOH. Re-fill burette and once again note the initial level of the H2C2O. acid. Repeat the titration accurately so that the addition of a final drop changes the colour of the indicator. Note the final evel 12. Repeat the titration 3 times, taking accurate readings, and then find the average reading 13. Calculate the concentration of the NaOH solution Additional Instructions: Fay careful attention during the pre-practical talk and take notes so that you are sure of must do when you carry out the investigation. The NaOH solution. of unknown concentration, will be in a ‘li carried to determine its concentration by making use of th All work must be done in the spaces provided in theseResults 3 TCT So [Average | | 1 Initial burette reading burette reading acid used Volume of base used V | Answer the following questions Give the colour of the solution with the indicator before the start of titration activities ) + Give the c olour of the mixture after reaching the end-point 3) Explain why the indicator phenolphthalein was used instead of bromothymol blue What was the use of the pipette in this experiment? 4) Identify apparatus A and apparatus 8 (5) Identify the dependent and the independent variable in this experiment Dependent Independent. 6) Give the safety measures in conducting this kind of experiment (7) Inthe event that a chemical has spilled on someone's hand what action would be necessary to take immediately? (8) Give the balanced reaction equation (9) Do the calculation to determine the concentration of NaOH Copyright Reserved 4Hint Ca x Va = Cox Vp Ca = » = conc. of acid = cone. of alkali Va = vol. of acid Vb = vol. of alkali |NOTES TO LEARNERS (1) The answers to the questions above and below must be put neatly. They form Part of information the learners must know to answer question in the Practical | Test The answers are mainly based on what learners observed. particularly if the | experiment is practically conducted. Few may be based on content understanding At the end learners must write a report as guided by rubric by which it will be assessed. The report has to include title, aim, variables, list of \ apparatus, method, results, results analysis and conclusion. Learners who do not conduct the experiment will automatically lose 5 marks (5) In short, learner assessment in this practical will occur in three parts or stages. | Part 1 or stage 1 allows a teacher to assess the learners’ skills in conducting | the experiment. The second, Part 2, is the evaluation of learners’ report about the experiment. The two parts are credited 5 and 10 marks respectively. Schools are expected to be done with part 1 and 2 assessment by the 12" August 2024. Part 3 of the task will be in form of a short test. It will be administered out of 35. The total will remain 50 marks. The practical test will be administered on the 16" of August 2024EPARVWENT OF EDUCATION VHEMBE WEST DISTRICT Grade 12 Phigueal Sciences Practical Acsossmant 1 Tool: EXPERIMENT 2 School: Learner's name: .. Date: - Apparatus Handling Assessment / Marking Tool Skills | Criteria | Mark | Total | | : Only few or All the relevant | dentification of | none of the apparatus / chemicals apparatus | apparatus / are correctly | chemicals are identified | | known by the | : learner [0] 1] |_ 4 The | The setting up have The set-up is correct. | | | arrangements of | been correctly The | | Setting of | Equipment are | attempted but there | apparatus/chemical s | | apparatus | are is mistakes which | are correctly located in | | the set up cannot | can default the | the set up. | give readings / —_| readings Pa (2 | 2 | | results {0} The learner positions himself well and take | Data collection | The learner does /readings | not know how to | taking | take readings or accurate readings | | | make the (make correct | | observations are observations) (1 ‘1 aan incorrect. [01 A | The learner The learner works with | | works carelessly | care and disconnects / | Observation of {| without any | dismantles the set up | precautions | consideration of after making the | | precautions | observations (11 i (0) | % ad Total : ne Peck cali. ah eaNot given oF not related to the [experiment [0] No variable or incorrect | Variables | | Variables | | identified (0) __| | Procedure is not | given or is given | in a way that | does not lead to | the end of the | experiment [0] No table of data | is given Data is presented ina | manner difficult to interpret [0] Method | | — | | Results | No analysis | attempted. Analysis attemptedis | irrelevant [0] Analysis or | Interpretation | = L [ Conclusion | No conclusion | attempted / Conclusion attempted is irrelevant. | {0} ment / Marking Tool - Exp 2 V same | Tout | Criteria et Tells what the experiment intend to find out a | | jee Two variables | Ali variables identified — | f identified and | and correct (2) correct. [1] | | foam Procedure is | Procedure is logically and | given butnot | completely described —_—_| logically. It is fa | not complete | 1 | is a ~~} Correct data is weil recorded in suitable | tables | | Columns have suitable | j | headings with correct | | units. (1 il 4 Relevant Results for th | | analysis done | experiment well analysed | but [2] | | incomplete. | | | ie | | the experiment | experiment has been “Handling ‘Apparatus Mark Experiment Report Mark Practical Test Mark Learner’s Final Experiment Mark Copyright Reserved | has been | drawn and it connects drawn without | well with the variables | | connecting | | | 2 with the | | variables. (1) |; ? | PTO