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e2695_2475 MSG Qualification Summary

The document summarizes the results of an automated qualification test and a manual qualification test that were performed on a liquid chromatography system. The automated tests assessed various parameters of the system including precision, accuracy, sensitivity, linearity and drift. The manual tests evaluated column temperature, flow rate accuracy, signal to noise and sample temperature. All tests showed passing results.

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Riad Manamanni
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0% found this document useful (0 votes)
49 views2 pages

e2695_2475 MSG Qualification Summary

The document summarizes the results of an automated qualification test and a manual qualification test that were performed on a liquid chromatography system. The automated tests assessed various parameters of the system including precision, accuracy, sensitivity, linearity and drift. The manual tests evaluated column temperature, flow rate accuracy, signal to noise and sample temperature. All tests showed passing results.

Uploaded by

Riad Manamanni
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

QUALIFICATION SUMMARY REPORT

System Name: e2695_2475 MSG


Processing Node: Wgsqd-s4alnbz
Project Path: RC2_SQT _e2695_2475 final

Automated Qualification Tests Summary


Qualification Test Qualification Test Qualification Test
Parameters Specifications Pass / Fail
1 System Precision Area %RSD < or = 0.50 PASS
2 System Precision Height %RSD < or = 1.5 PASS
3 System Precision Retention Time %RSD < or = 1.0 PASS
4 Emission Wavelength Accuracyy 700 + or - 6nm PASS
5 Excitation Wavelength Accuracy 350 + or - 6nm PASS
6 Detector Linearity Area R^2 > or = 0.990 PASS
7 Detector Linearity Height R^2 > or = 0.990 PASS
8 Detector Area Sensitivity %RSD < or = 5.0 PASS
9 Detector Height Sensitivity %RSD < or = 5.0 PASS
10 Gain Linearity Area %RSD < or = 4.0 PASS
11 Gain Linearity Height %RSD < or = 4.0 PASS
12 Injector Linearity R^2 > or = 0.9990 PASS
13 Injector Accuracy < or = 1.0 µL PASS
14 Injector Carry Over < or = 0.1 % PASS
15 Compositional Precision RT %RSD < or = 3.0 PASS
16 Detector Noise < or = 5 EU PASS
17 Detector Drift < or = 10 EU/Hr PASS

Manual Qualification Tests Summary


Qualification Test Qualification Test Qualification Test
Parameters Specifications Pass / Fail
1 Column Temperature Set Point 1 ± 2.0 °C of Set-Point Temperature PASS
2 Column Temperature Set Point 1 ± 2.0 °C of Set-Point Temperature PASS
3 Flow Rate Accuracy for 0.5 mL/min 0.494 to 0.506 mL/min PASS
4 Flow Rate Accuracy for 2.0 mL/min 1.98 to 2.02 mL/min PASS
5 Flow Rate Accuracy for 5.0 mL/min 4.94 to 5.06 mL/min PASS
6 Signal to Noise > 1000 PASS
7 Sample Temperature Set Point 1 ± 4.0 °C of Set-Point Temperature PASS
8 Sample Temperature Set Point 2 ± 4.0 °C of Set-Point Temperature PASS

Waters Project Name and Version: SQT_E_2695_2475 v4.00 © 2007 - 2017 Waters Corporation. All rights reserved.
Date: Monday, February 20, 2017
Printed: 11:12:35 AM US/Eastern Page: 1 of 2
QUALIFICATION SUMMARY REPORT

System Name: e2695_2475 MSG


Processing Node: Wgsqd-s4alnbz
Project Path: RC2_SQT _e2695_2475 final

Automated Qualification Sample set details


Sample Set Id Result Set Id Sample Set Name Sample Set Start Date
1 7877 7887 System Precision 100uL SSM Friday, February 10, 2017 12:35:36 PM EST
2 7914 7927 EM Wavelength Acc SSM Friday, February 10, 2017 1:01:25 PM EST
3 7928 7950 EX Wavelength Acc SSM Friday, February 10, 2017 1:14:42 PM EST
4 7967 7973 Detector Lin Sens SSM Friday, February 10, 2017 1:28:03 PM EST
5 7986 8003 Gain Linearity SSM Friday, February 10, 2017 1:40:55 PM EST
6 8022 8032 Injector Lin Acc SSM Friday, February 10, 2017 1:55:55 PM EST
7 8053 8066 Injector Carryover SSM Friday, February 10, 2017 2:16:54 PM EST
8 8098 8112 Compositional Prec SSM Friday, February 10, 2017 2:56:31 PM EST
9 8151 8168 Noise and Drift SSM Friday, February 10, 2017 3:53:10 PM EST

Manual Qualification Sample set details


Sample Set Id Result Set Id Sample Set Name Sample Set Start Date
1 7817 7832 CH Temperature Acc SSM Friday, February 10, 2017 12:14:06 PM EST
2 7837 7846 Flow Rate Acc SSM Friday, February 10, 2017 12:14:44 PM EST
3 7853 7861 Signal to Noise SSM Friday, February 10, 2017 12:15:28 PM EST
4 8181 8186 SHC Temperature Acc SSM Monday, February 13, 2017 7:55:02 AM EST

Waters Project Name and Version: SQT_E_2695_2475 v4.00 © 2007 - 2017 Waters Corporation. All rights reserved.
Date: Monday, February 20, 2017
Printed: 11:12:35 AM US/Eastern Page: 2 of 2

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