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Introduction To Process Design and Simulation

This document provides an overview of the EMS510U module on Process Design and Simulation. It includes the module expectations, assessment details, weekly topics, objectives, and introductions to key concepts like process design, simulation, and the stages of the design process. The module will cover mass balances, process flow diagrams, ancillary equipment, lab workshops, and using ASPEN to simulate a process. Students will complete an individual assessment on design principles and a group project analyzing a piping and instrumentation diagram.

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100% found this document useful (2 votes)
292 views43 pages

Introduction To Process Design and Simulation

This document provides an overview of the EMS510U module on Process Design and Simulation. It includes the module expectations, assessment details, weekly topics, objectives, and introductions to key concepts like process design, simulation, and the stages of the design process. The module will cover mass balances, process flow diagrams, ancillary equipment, lab workshops, and using ASPEN to simulate a process. Students will complete an individual assessment on design principles and a group project analyzing a piping and instrumentation diagram.

Uploaded by

DMRI
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

EMS510U: Process Design and

Simulation

Introduction to Process Design and Simulation


Dr Sanaa Hafeez
Format
Module expectations
• Asynchronous activities – Self study (~1 hour)
• Weekly Lecture (2 hours) and in class Kahoot quiz
• IT class, Friday 11am – 1pm, Bancroft:1.23 (weeks 1, 3 – 9)
• Practical labs, (weeks 9 & 10)

Assessment
• Extended individual assessment on design principles (60%)
• Deadline: Friday 22nd March, 23.59pm
• Piping and Instrumentation Diagram analysis (40%)
• Friday 5th April, 6pm (group)
Weekly programme
Week Content
1 Introduction to process design and simulation
2 Introduction to Chemical Process diagrams
3 Mass balances (Hand calculation, simulation and flowsheets)
4 Introduction to project + Principles of Design
5 Environmental, Social and safety considerations
6 Introduction to ancillary equipment: Pumps, Valves and compressor
7 SKEMP week
8 Introduction to lab (design and planning)
9 LABS workshop, design feedback
10 LABS workshop, Q & A
11 LABS workshop
12 No lecture
Module Objectives
• By the end of the module, you will be able to:
– Design and size unit operations to accomplish a specific
process step
– Integrate and arrange process units according to
industrially accepted standards and hazard review
procedures to achieve an overall processing objective
– Develop an understanding on Chemical Process Diagrams
– Build simulate a process in ASPEN plus
What is process design?

“The creative activity whereby we generate


ideas and translate them into equipment and
processes for producing new materials or for
significantly upgrading the value of existing
materials.”
Design: synthesis analysis
• Design tasks are open ended!
• Highly under-specified
– Assumptions are necessary during this stage
• Process units to use must be selected
• Interconnection of process units must be selected
• Operating conditions must be specified
Design: synthesis analysis
• Process synthesis
– Identification of the optimal choice of units and
the connections between them, Selection of
solvents etc.
• Process design and simulation
– Establishment of the optimal operating
conditions and definition of each unit operation
• Process analysis
– Study of the effectiveness of design in the light
of operational considerations (safety,
environmental etc)
Design: synthesis analysis
• Your role as an engineer:
– To consider safety environmental constraints
– Simplicity of start-up/operation/shut-down
– Use rules-of-thumb to eliminate some alternatives from
consideration, and to design a number of alternatives for
comparison
Stages of Design Process
• Feasibility study
• Conceptual Design
• Process and Detailed design
• Construction
• Start-up operations
Step 1 – Feasibility study
• Gathering data for quick estimates
– Availability of suppliers, specifications and raw
material costs
– Thermodynamic/kinetic data for reactions
– Facilities equipment available
– Safety requirement
– Chemical and physical properties of all reactants
Step 2 – Conceptual Design
• Process development
Process Development
• The collection of additional reaction and physical property data (after
preliminary design) to increase the accuracy of the quick-estimate
generated from the feasibility survey
• May include lab research and/or pilot operations as necessary to obtain
missing information
• Design data is collected, including accurate material and energy balances,
an understanding of the effects of various process conditions data.
Step 2 – Conceptual Design
• Process development
• Flowsheet definition
• Cost estimation
• PFD
• Simulation
• Specification sheets
• Environmental safety review
Step 3 – Process Design
• Equipment design
• Piping layout
• Plot plan
• Instrument loop diagrams
• Safety review
• Environmental permitting
• Stages
• Iterative process
Step 4 - Construction
• Site prep
• Vessel fabrication
• Facilities erection
• Piping conduit/wiring
• Control loop checkout
• Safety review
• Operator training
Step 5 – Start up Operation
• Pressure testing
• Flow testing / instrument calibration
• Closed loop operation
• Start-up
• Start-up safety review
• Operation
• Environmental monitoring
What is simulation?
“A process of designing an operational model of
a system & conducting experiments with this
model for the purpose either of understanding
the behaviour of the system or of evaluating
alternative strategies for the development or
operation of the system… “
Introduction to simulation
Real- A set of assumptions
world Modeling
concerning the behavior of a system & Analysis
process

• The imitation of the operation of a real-world process or


system over time
– to develop a set of assumptions of mathematical, logical, and symbolic
relationship between the entities of interest, of the system.
– to estimate the measures of performance of the system with the
simulation-generated data
Introduction to simulation
Real- A set of assumptions
world Modeling
concerning the behavior of a system & Analysis
process

• Simulation implies modelling, as well as tuning of models on


experimental data. A simulation model serves to conduct
“virtual experiments”
– as an analysis tool for predicting the effect of changes to existing
systems
– as a design tool to predict the performance of new systems
Design & analysis through simulation
A chemical plant is our real world

Divider

Mixer Reactor Separator


Design & analysis through simulation
Main steps
Develop
process
model

Define Divider
Collect
problem additional
data

Mixer Reactor Separator


Analyze
results

Solve model
equations
Design & analysis through simulation
What information do we need?

Divider

Stream
Mixer Reactor Separator data

Equipment
Mixture Unit Process data
Known data
compounds operations flowsheet
Operating
data
Design & analysis through simulation
What do we need to select (from a simulator)?

Divider

Unit
Mixer Reactor Separator models

Thermo-
Mixture Unit Process models
Library
compounds operations flowsheet
Methods
of
solution
What is a Process Simulator
• An Engineering tool which performs:
– Automated calculations
– Materials and/or energy balance
– Physical property estimations
– Design/rating calculations
– Process optimization
Steps in simulation
study
Benefits of process simulation
• Process knowledge
– Verification of the process operating conditions and plant
specifications
– Information on intermediate streams (not measured)
– Enthalpy balances information
– Validation of phase equilibrium models for the real
systems to be used in similar conditions
– Process de-bottlenecking for each individual section
Why is this important?
• It represent with high accuracy the real world
• It allows to focus on the interpretation of the results rather
than the method for obtaining them
• It allows a global vision on the process engineering by
assembling theories and models
• It is essential in the design of new and existing processes
• It is essential in the analysis of existing plants in terms of
environmental impact
Common sources of problems?
• Model/program does not apply to your problem
• Errors in input data, inappropriate defaults
• Over complication: keep it simple!
• Units of measurement
• Convergence problems: ignoring error and warning messages
• Applying models or data outside their range of validity
When is simulation appropriate?
• Simulation enables the study of, and experimentation with, the internal
interactions of a complex system, or of a subsystem within a complex system.
• When organizational and environmental changes can be simulated, and the effect
of these alterations on the model’s behaviour can be observed
• The knowledge gained in designing a simulation model may be of great value
toward suggesting improvement in the system under investigation.
• By changing simulation inputs and observing the resulting outputs, valuable insight
may be obtained into which variables are most important and how variables
interact.
• Simulation can be used to experiment with new designs or policies prior to
implementation, so as to prepare for what may happen.
• Simulation can be used to verify analytic solutions.
When is NOT simulation appropriate?
• When the problem can be solved using common sense.
• When the problem can be solved analytically.
• When it is easier to perform direct experiments.
• When the simulation costs exceed the savings.
• When the resources or time are not available.
• When system behaviour is too complex or can’t be defined.
• When there isn’t the ability to verify and validate the model.
Application of process simulations
Process Industries Applications
Oil & Gas Offshore exploration, Surface treatment, Pipeline
transport, Underground storage, Gas processing
Refining Gasoline and fuels
Petrochemicals Hydrocarbon based chemicals, Methanol, Monomers
Basic Organic Intermediates, Solvents, Detergents, Dyes
Chemicals Ammonia, Sulphuric Acid, Fertilisers
Inorganic Chemicals Pharmaceuticals, Cosmetics
Fine Chemicals Food and bio products
Biotechnology Steel, Aluminium, Copper, etc.
Metallurgy Polyethylene, PVC, Polystyrene, fibres, etc.
Polymers Paper pulp
Paper & Wood Power plants, Coal gasification
Energy Waste treatment, Safety
Nuclear industry Water cleaning, Biomass valorisation
Environment
What is AspenPlus?
• AspenPlus is a market-leading process
modelling tool for conceptual design,
optimization and performance monitoring for
the different industrial applications
AspenPlus approach
• Sequential Modular (SM)
• Each unit operation “block” is solved in a certain
sequence
• Each block computes its outlet streams
• When recycles are present, iterative solution is
required
• Used to solve a large number of blocks
• Can be time consuming for certain types of problems
AspenPlus approach
• Equation Oriented (EO)
• All equation are solved simultaneously
• A good starting point is necessary
• Combination
• Use SM approach to initialise and/or get close to a solution to then
use EO approach to solve flowsheet more precisely
• Use SM approach to get an initial solution, then use EO approach
to do optimisation or model tuning
SM vs EO approach
• SM approach
• Large number of unit operations with few recycle loops
• For initial PFD design problems
• First step of rigorous modelling using EO approach
• EO approach
• Highly heat-integrated processes
• Highly recycled processes
• Process with many design specification specifications
• Process optimization
• Process model tuning through data reconciliation and parameter estimation
Steady state vs Dynamic simulations
• Steady-state simulation is used to determine
optimal design parameters and operating
condition of the systems.
• Dynamic simulation, modelled based on
steady-state simulation, is used to examine
dynamic behaviours of the systems.
Steady state simulation
• General starting point: Process description and design specifications
• Convert to BFD -> PFD -> PSD
• General problem analysis steps in PSD:
• Input/output streams
• Thermodynamic issues
• Reactor and separation systems
• Recycle systems
• Control of flowsheet specifications
• Transformation of real units into simulation units
• DOF analysis
• Tear streams and computational sequence
Good flowsheeting practices
• To build large flowsheets, start by putting few
blocks at a time and solve them
• By joining small pieces together it is easier to
troubleshoot

• Solve for single pass process before joining


recycle loop
Good flowsheeting practices
• Keep in mind the end use of the model
• Build simple flowsheet (will run faster)
• Add details later if required
• Ensure flowsheet inputs are reasonable
• Check that results are consistent and realistic
Summary
• AspenPlus is an AID in making calculations and
decisions -> YOU must ensure that it is “fit for
purpose”
• YOU are responsible for any results you
generate
• YOU are required to make sound engineering
judgements
EMS510U: Process Design and
Simulation

Introduction to Process Design and Simulation


Dr Sanaa Hafeez

Common questions

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The iterative nature of process design enhances the final system outcome by allowing continuous refinement of each stage based on previous findings, ensuring a thorough review and optimization of designs . Iterations enable the incorporation of new data, feedback, and insights, leading to a more accurate and efficient design . This approach facilitates adjustments to design errors, improves parameter estimations, and aligns the process with safety and operational criteria, ultimately leading to a well-optimized and reliable system . Additionally, iterative design supports effective troubleshooting by providing opportunities to test and correct assumptions at every stage, resulting in a robust final outcome .

The primary stages of the design process include: Feasibility Study, Conceptual Design, Process and Detailed Design, Construction, and Start-Up Operations. Each stage contributes uniquely: Feasibility Study involves gathering data for quick estimates like raw material costs and safety requirements . Conceptual Design focuses on collecting detailed reaction and physical property data, defining flowsheets, and estimating costs to increase accuracy . Process and Detailed Design involves creating equipment designs, piping layouts, and conducting safety reviews . Construction includes site preparation, vessel fabrication, and operator training . Start-Up Operations cover pressure testing and environmental monitoring to ensure successful plant operation . Together, these stages contribute to a comprehensive and effective industrial process design.

Accurate data collection in the conceptual design stage is crucial as it forms the basis for defining accurate material and energy balances, understanding process conditions, and designing effective systems . This stage includes collecting reaction and physical property data to refine feasibility estimates and define process flowsheets . Accurate data supports reliable simulations and cost estimations, influencing decisions in equipment design, safety reviews, and environmental permitting in later stages . Faulty or insufficient data can lead to incorrect assumptions and designs, causing inefficiencies or failures in the Process and Detailed Design, Construction, and Start-Up Operations phases . Thus, thorough data collection ensures a solid foundation for subsequent design work, reducing risks and maximizing system efficiency.

Process simulation enhances understanding and improvement of industrial systems by allowing for detailed analysis of system behavior and performance through virtual experiments . It verifies operating conditions and specifications, provides information on intermediate streams, and facilitates de-bottlenecking for plant sections . Additionally, it offers insights into important variables and their interactions, enabling improved system designs or policies before implementation . Simulation provides a global vision of process engineering by assembling theories and models, aiding in both new and existing process designs .

Process simulation and real-world experimentation complement each other by creating a comprehensive approach to process design. Simulations provide a cost-effective, risk-free environment for testing system behavior, conducting virtual experiments, and gaining insights into process dynamics that might be impractical to explore physically . They allow designers to refine processes, optimize parameters, and predict outcomes under different scenarios, guiding experiments to be more focused and informed . Real-world experimentation, on the other hand, validates simulation models, revealing practical limitations and providing precise empirical data for calibration and validation of simulations . Together, they enable a more robust design process where simulation-driven hypotheses are rigorously tested and refined through experimentation, achieving reliable and efficient system designs .

Safety and environmental considerations are integral across all process design stages. During the Feasibility Study, gathering data on safety requirements and environmental constraints is crucial . In the Conceptual Design stage, an environmental safety review is conducted alongside flowsheet definitions and cost estimations to ensure compliance and minimize risk . The Process and Detailed Design stage involves a more thorough safety review and obtaining environmental permits . Construction activities include safety reviews and training for operational readiness, emphasizing safe site preparation and system operation . Finally, in Start-Up Operations, environmental monitoring ensures ongoing compliance and safety standards are met . These considerations help prevent accidents and minimize environmental impact throughout the design and operational phases.

The benefits of process simulation include the ability to run virtual experiments to understand system behavior and test alternatives without the cost and constraints of physical experiments . It allows for studying complex interactions within the system and aids in designing new systems or improving existing ones through simulated experiments . It is also beneficial for extending a global vision of engineering processes with high accuracy . However, simulation has limitations, such as potential model mismatches, input errors, and excessive complexity; challenges arise when models exceed their validated range or don't account for practical nuances that direct experimentation might capture . Simulation should also be avoided when common sense or simple analytical solutions are possible, or when constrained by resource and cost considerations .

Effective strategies for troubleshooting and optimizing large flowsheets in process simulations include starting with a few blocks at a time to simplify troubleshooting and gradually joining these pieces to form a complete system . It's recommended to build simple flowsheets first for speed and ease of computation, later adding necessary details . Ensuring that inputs are reasonable and checking results for consistency and realism help avoid convergence and data validity issues . Additionally, using the Sequential Modular approach initially for easier problems, followed by switching to the Equation Oriented approach for optimization and tuning, aligns the process with the specific needs and complexities of the system .

AspenPlus promotes efficiency in process design by offering tools for conceptual design, optimization, and performance monitoring, which streamline the design process across various industrial applications . The Sequential Modular (SM) approach solves each unit operation block in sequence and is ideal for initial PFD design problems, while the Equation Oriented (EO) approach solves all equations simultaneously, which is suitable for highly heat-integrated or recycled processes requiring optimization or model tuning . The SM approach is used to get an initial solution, and EO can be employed for refining the solution, handling complex designs, and ensuring precision .

Potential common problems in process simulations include model or program mismatches, errors in input data, inappropriate default settings, and overcomplication of the model . These issues can lead to incorrect predictions of system behavior, affecting design reliability and performance . They might result in convergence problems if error or warning messages are ignored, complicating the tuning and validation of models . Moreover, using models outside their valid range can distort results, misguiding design and operational decisions . Such problems can compromise system efficiency, safety, and environmental compliance, highlighting the need for careful model selection, data accuracy, and process simplification where applicable .

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