MATERIAL TEST CERTIFICATE
AS PER STD EN 10204 TYPE 3.1
Customer : GTN Engineering (India) Ltd Unit-II (PMS) TC No. : EC2192 Date : 26.12.2023
Invoice No.:DWIF/23-24/ Date :
P.O. No.: 4710048186-0 Line Item: 1 PO Date : 07.11.2023 Spec. Ref.: M25070 Rev. : F (Date:16.07.2021)
Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio [Link]. Mill
BODY FORGING, ULT PLUG Forged,
1300-GTN VALVE 2 ULT150 F/UNION P537156 Rev D Normalized 7.21 : 1 106 Nos AISI 4140 BF-EOF-LRF-VD-CCP
ENDS AISI 4140 ALLOY STEEL Quenched &
FMC SPEC M25070 Tempered, - JSW STEEL LTD
Shot Blasted
Heat Code: PAQ DU500006672 Rev B
CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo Ni Grain Size
F19325 0.40 0.89 0.16 0.009 0.012 1.03 0.22 0.025 7
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 - 6
Max. 0.43 1.00 0.35 0.025 0.025 1.10 0.25 - -
HEAT TREATMENT
Procedure :- Q00025 Rev S
Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)
HT Load No. of N :- AH-29 HT Batch No. of Q&T:- AH-34 Qty :- 106 Nos
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 7.21 : 1 900⁰C 3 Hrs 20 Min 870⁰C 3 Hrs 20 Min OIL 30°C 43°C 560°C 5 Hrs (Air Cool)
Forging 7.21 : 1 900⁰C 3 Hrs 20 Min 870⁰C 3 Hrs 20 Min OIL 30°C 43°C 560°C 5 Hrs (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 540⁰C
Max. 925⁰C 900⁰C --- 80⁰C 700⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average
Refer annexure for testing details
Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 8.75 mm Dia, 35 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.
Enclosures: 1) Steel Mill TC 2) Hardness report 3) Dimensional Report 4) Testing Annexure 5) HT Graph 6) Mechanical Testing Reports
Note :- We guarantee that no weld repairs have been performed.
. We certify that the above figures are correct as recorded by the company.
For Heat Treatment batch traceability, the heat treatment batch 'AH-34' is stamped near the Heat code.
The above material meets the requirements of ASTM A788/A788M: 23.
The material is free from radioactive and mercury contamination.
The furnace used for Normalizing and Hardening (CF3) is due for calibration on - 20.02.2024.
The furnace used for Tempering (CF4) is due for calibration on - 24.02.2024.
Furnace calibration has been done as per AMS 2750G and meets the requirements.
Forging Method - Closed Die Forging
Ajay Joshi (HEAD-MQC, HT & NDT)
Authorised Signatory
F-MQC-10 / Rev. 00 / 01-Apr-2016
Works & Registered Office Tel : +91-02137-679819
Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@[Link]
[Link] CIN : U28910PN1981PTC024155
HARDNESS TEST REPORT
Customer:- GTN Engineering (India) Ltd Unit-II (PMS) TC No: EC2192
P.O. No.:- 4710048186-0 Line Item: 1 PO Date : 07.11.2023 Date : 26.12.2023
BODY FORGING, ULT PLUG VALVE 2
Item : ULT150 F/UNION ENDS AISI 4140 ALLOY Material : AISI 4140
STEEL FMC SPEC M25070
Part No : P537156 Rev D Heat No. : F19325
Drawing No.: DU500006672 Rev B Ambient Temp : 25°C
Die No.: 1300-GTN Hardness Range:- 277 - 331 HBW
Qty.: 106 Nos Test Method : Brinell Hardness Test
Vendor [Link].: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: AH-29 QT: AH-34 Sr No.: 19/05/007 | 2017/09
Reference Standard: ASTM E10 Machine Make: SAROJ | FSA
Load Applied: 3000 Kgs Calibration Agency: MTMS | MME
Type of Penetrator: Dia 10 mm Carbide Ball Certificate No.: MME/CAL/337 & 338/23-24
Std Block Details: SH-0344/23 (Hardness value - 303.6 HBW)
SH-0346/23 ( Hardness value - 303.2 HBW)
Calibrated On: 07.08.2023
Entity Performing Test: WIF Sanaswadi Calibration Due On: 06.02.2024
Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 16 & 17.12.2023
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.
Qty. Hardness in HBW
106 Nos 285-321 HBW
Test Performed By Reviewed By Approved By :
Atul Jedhe Satish Gadgil ([Link] HT) Ajay Joshi (HEAD-MQC, HT & NDT)
F-HT-10 / Rev. 00 / 01-Apr-2016
CERTIFICATE OF COMPLIANCE
Customer : GTN Engineering (India) Ltd Unit-II (PMS) TC No.: EC2192
Date: 26.12.2023
Die No. : 1300-GTN Heat Code : PAQ
PO No : 4710048186-0 Line Item No : 1
Offer Qty. : 106 Nos
Part No/ Rev : P537156 Rev D Drg No / Rev : DU500006672 Rev B
BODY FORGING, ULT PLUG VALVE
Part Name : Serial No. : -
2 ULT150 F/UNION ENDS AISI 4140
ALLOY STEEL FMC SPEC M25070
I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25070 Rev No. F (Date:16.07.2021)
C. Material Test Report No : Mill Heat No : F19325
II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 20 Nos.
III. Secondary Process : Heat Treatment
A. Process Name : Normalised
Heat Lot No. : AH-29 Process Spec : Q00025 Rev S
B. Process Name : QT
Heat Lot No. : AH-34 Process Spec : Q00025 Rev S
IV. NDE
A. Process Name : MPI
Certificate No : NA Process Spec : NA
B. Process Name : UT
Certificate No : NA Process Spec : NA
This is certified that the subject material is manufactured from the material mentioned above and
verified by us as per the written sample size, and it is found to conform to the requirements.
For Heat Treatment batch traceability, the heat treatment batch 'AH-34' is stamped near the Heat code.
The above material meets the requirements of ASTM A788/A788M: 23.
Sign with Stamp
Ajay Joshi (HEAD-MQC, HT & NDT)
Mechanical Test Annexure
Die No.: 1300-GTN Material Grade: AISI 4140
Heat No.: F19325 HT Lot No. : AH-34
Heat Code: PAQ TC No. : EC2192
TENSILE TEST
QTC Test QTC Hardness after UTS YS Elg RA
Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW KSI KSI % %
0.5" below
L 321, 321 Ambient I-23-2243-P 1 149.29 130.08 16.43 57.51
HT Surface
277 - 331 Spec. Min. 120.00 100.00 16.00 35.00
IMPACT TEST
QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
94 88 108 96.67
Single - 32 J Min
LE - 0.51 mm Min -29°C I-23-2244-P 1.30 1.23 1.46 1.33
%Shear - Report 65 65 70 66.67
L 1
Avg. - 27 J Min
80 66 74 73.33
Single - 20 J Min
LE - Report -40°C I-23-2245-P 1.16 0.98 1.00 1.05
%Shear - Report 60 55 55 56.67
0.5" below
HT Surface Avg. - 28 J Min
70 64 70 68.00
Single - 18.7 J Min
LE - Report
-29°C I-23-2246-P 0.93 0.85 0.94 0.91
%Shear - Report 60 55 60 58.33
T 1
Avg. - 20 J Min
46 64 58 56.00
Single - 14 J Min
LE - Report -40°C I-23-2247-P 0.63 0.83 0.76 0.74
%Shear - Report 40 55 50 48.33
Ajay Joshi (HEAD-MQC, HT & NDT)
Authorised Signatory
