Technical Standard - TS

Title: Analyser Sampling System Reference: GTL-64-05

Revision: 4
Effective date: 20/08/2020
Total pages: 18
Revision date: 20/08/2023
Classification: Public

Custodian: Signature Date

Projects Services Manager- Hussain Abdulla H A Al- Digital signature 20/08/2020

Sada verified

Approved by:

Chief Engineering and Projects Officer- Ali Abdulrahman Digital signature 20/08/2020
A A Al-Mohannadi verified

Endorsed By

Sr. No. Endorsed By Endorsed Date

1 Head of Quality- Mooza Abdulla 20/08/2020

Mubarak A Ali
2 Lead Discipline Engineering- Khemais 20/08/2020
Besbes

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 Reviewed By

Sr. No. Reviewed By Position Reviewed Comments

Date
1 Melvin Bryan Arellano Chief Secretary 11/08/2020 [Action Taken - Review
Ebreo Started]This Technical
Standard has been updated as
per the new Technical Standard
Template only. No revision to
its contents. Please review and
accept. Currently, the CDMS
document Viewer is not working
properly. Kindly download the
softcopy if you want to view the
document on its original format.
2 Khemais Besbes Lead Discipline 11/08/2020 [Action Taken - Approved]
Engineering
3 Hussain Abdulla H A Projects Services 11/08/2020 [Action Taken - Approved]
Al-Sada Manager
4 Ali Khedher Projects Manager 12/08/2020 [Action Taken - Approved]
5 Omer Farooq Integrated 16/08/2020 [Action Taken - Approved]
Management
Specialist
6 Melvin Bryan Arellano Chief Secretary 16/08/2020 [Action Taken - Review
Ebreo Completed]No comment.

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Content
Page
1 Supporting Clauses ...................................................................................................................2
2 Introduction ................................................................................................................................5
3 Analyser Sampling System........................................................................................................5
4 Roles and Responsibilities.......................................................................................................17
5 Authorisation............................................................................................................................18
6 Revisions .................................................................................................................................18

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1 Supporting Clauses

1.1 Scope

1.1.1 Purpose

This standard covers the basic minimum requirements to be followed for sample transport and sample
conditioning system for process stream analyser for the ORYX GTL plant. In-situ analyser sensors are
not covered under this standard.

1.1.2 Applicability

This document shall apply throughout ORYX GTL.

1.2 Normative/Informative References

Parties using this document shall apply the most recent edition of the documents listed herein.

1.2.1 Normative
International Codes:
Code/ Standard No/
Title of Document
Rev/ Date

API RP 555, 2013 Process Analysers

Third Edition
ASME B1.20.1, 2013 Pipe Threads, General Purpose (Inch)

ASME B16.5, 2013 Pipe Flanges and Flanged Fittings NPS 1/2 Through NPS 24 Metric/Inch
Standard.
ASME B16.10, 2009 Face to Face and End-to-End Dimensions of Valves

ASME B16.34, 2013 Valves – Flanged, Threaded & Welding Neck

IEC 60079-1 Explosive atmospheres - Part 1: Equipment protection by flameproof

2014 Edition 7.0 enclosures “d”
IEC 60079-2 Explosive atmospheres – Part 2: Equipment protection by pressurized
2014 Edition 6.0 enclosure “p”
IEC 60079-7 Explosive atmospheres - Part 7: Equipment protection by increased
2015 Edition 5.0 safety "e"
IEC 60079-11 Explosive atmospheres – Part 11: Equipment protection by intrinsic
2011 Edition 6.0 safety "i"
IEC 60079-15 Explosive atmospheres – Part 15: Equipment protection by type of
2010 Edition 4.0 protection "n"
IEC 60529 Degree of Protection Provided by Enclosure (IP Code)
2013
IEC 61000-4-2 Electromagnetic compatibility (EMC) – Part 4-2: Testing and
2008 measurement techniques – Electrostatic discharge immunity test
IEC 61000-4-3 Electromagnetic compatibility (EMC) – Part 4-3: Testing and
2010 Edition 3.2 measurement techniques – Radiated, radio-frequency, electromagnetic
field immunity test
IEC 61000-4-4 Electromagnetic compatibility (EMC) – Part 4-4: Testing and
2012 Edition 3.0 measurement techniques – Electrical fast transient/ burst immunity test
IEC/TR 61831 On-line analyser systems – Guide to design and installation

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Edition 2.0 2011-08

NACE MR0175/ISO Petroleum, petrochemical, and natural gas industries - Materials for use
15156 , 2015 in H2S-containing environments in oil and gas production

Reference Standards:

GTL-01-01 Site Conditions

GTL-02-01 Units of Measurement
GTL-05-03 Classification of Hazardous Chemicals
GTL-51-02 Piping Material Specification
GTL-61-01 General Instrumentation Specification
GTL-63-01 Instrument Piping Material Specification
GTL-64-01 Instrument Installation Specification
GTL-64-04 Analyser Shelter and Analyser Local Panel Specification
GTL-64-07 Installation of Instrument in Piping System

1.2.2 Informative

Should there be any conflict between this Technical Standard and the below codes/standards/
regulations/specifications and requirements, the more stringent shall apply. The User shall inform
ORYX GTL of any conflict:
 This Technical Standard
 Qatar statutory law and regulations
 RLIC Regulations
 ORYX GTL HSE Regulations
 OSHA United States Occupational Safety & Health Administration Regulations
 Approved technical exception / deviation list (as applicable)
 Amendments to National/International codes and standards
 National/International codes and standards
 Qatar Construction Specifications 2014

1.3 Definitions

Item Definition

CONTRACTOR Shall mean any person or persons, firm, partnership, corporation or

combination thereof (including its Subcontractors) employed for the
performance of services by ORYX GTL.
VENDOR Shall mean any person, firm or company having a purchase order for the
performance of any item of work.
OWNER Shall mean the responsible ORYX GTL representative for which services
are being rendered by the CONTRACTOR
Plant Shall mean ORYX GTL Gas to Liquids Facility
Shall Refers to a requirement

Should Refers to a recommendation

May Refers to one acceptable course of action.

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1.4 Abbreviations and Acronyms

Abbreviation/Acronym Expanded Name

ANSI American National Standards Institute

API American Petroleum Institute
ASME American Society of Mechanical Engineers
ATEX ATmosphere EXplosive
EMC Electromagnetic Compatibility
EMI Electro Magnetic Interference
IEC International Electrotechnical Commission
IP Ingress Protection
ISO International Organization for Standardization
NACE National Association of Corrosion Engineers
NPS Nominal Pipe Size
NPT National Pipe Thread
OD Outer Diameter
PMI Positive Material Identification
P&ID Piping and Instrumentation Diagram
RFI Radio Frequency Interference
RP Recommended Practice
SS Stainless Steel

1.5 Implementation Date

The implementation date is July 2020.

1.6 Process for Monitoring

The Custodian of the Document along with other Users within ORYX GTL shall monitor compliance
with the requirements of this Standard. Any revision to the Standard shall be processed in accordance
with ORYX GTL- IMS Procedure for “Update Engineering Technical Standards”.

1.7 Related/Supporting Documents

Not Applicable

1.8 Key Words

Sampling System, Sample Tap, Sample Probe, Sample Transport System, Sample Return Point,
Sample conditioning System, Sample connection, Sample pre-conditioning.

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2 Introduction
This standard defines the basic design criteria and the application of Analyser Sampling System within
the ORYX GTL plant. Referenced codes and standards also provide requirements for each type of
Analyser Sampling System.

3 Analyser Sampling System

3.1 General
3.1.1 The analyser sampling system shall be designed to extract, transport, and condition
representative process samples for delivery to the analyser under conditions that are required
for proper operation and function of analysers.
3.1.2 The sampling system shall be designed to minimise the consumption of process sample,
thereby reducing wastage and alleviating potential hazard in the event of a leak.
3.1.3 The sampling system shall be designed to provide ease of operation and maintenance,
protection from hazards, and long-term reliability.
3.1.4 The sampling system shall be designed so that failure or maintenance of one system does not
affect the operation of another system.
3.1.5 Simplicity shall be a prime consideration in the design of the sampling system.
3.1.6 The sample transport, conditioning, and disposal shall not create a hazard to personnel, the
environment, the process, or the plant that is being monitored.

3.2 Configuration
3.2.1 In general, the analyser sampling system shall be installed outside the analyser shelter.
3.2.2 In some cases, the analyser and sampling system shall be installed together in remote
enclosures or on remote freestanding racks, having separate sections.
3.2.3 The optimum installation configuration for each analyser based on the requirements for the
particular application shall be determined during detailed engineering.
3.2.4 As a preference, analyser sampling system should be installed adjacent to the analyser
shelter or local panel and provide all the necessary facilities for appropriate panel installation,
operation, and maintenance.
3.2.5 The complete sampling system is considered to have the following basic segments:
 Sample tap with sample probe
 Sample pre-conditioning system, if required (to be located as close as possible to
sample tap)
 Sample transport line from the sample tap/probe to the analyser location
 Sample conditioning with bypass/ fast loop stream and sample bomb facilities
 Analyser process sample inlet with calibration introduction and stream switching
 Sample/ effluent return and/or vent
3.2.6 The complexity and organisation of these segments with the analyser depends on the
particular application.
3.2.7 Only the minimum flow of sample required by the analyser for measurement shall be routed
inside the enclosure.
3.2.8 A suitable means of restricting the sample flow to approximately 2 times the normal flow shall
be included in the sample line outside the enclosure. (Restriction orifice or excess flow valve).

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3.2.9 The same type of restriction or restriction as per specific safety standards, whichever is more
stringent shall be used in other lines that contain hazardous material (flammable, toxic or
noxious).

3.3 Sample Phase Considerations

3.3.1 The sample shall be transported to the analyser as either a gas or liquid depending on the
types of Analyser.
3.3.2 Under no circumstances shall a mixed phase sample be used.
3.3.3 Special considerations shall be given to sample streams for which temperature and pressure
control are critical to maintain conditions above the dew point or below the bubble point to
prevent deterioration of the sample.
3.3.4 High pressure gas samples (i.e. greater than 7 bar) shall have a pressure reducing regulator
mounted at the sample tap immediately on the outlet of the sample probe. (This does not
apply to measurements made at line pressure).
3.3.5 Liquid samples with a boiling point below 65°C at reduced pressure (i.e. less than 7 bar) shall
be vaporised at the sample tap with a vaporising pressure reducing regulator and transported
as a gas, unless the analysis requires otherwise.
3.3.6 Liquid sample with a boiling point above 65°C at reduced pressure shall be transported and
analysed as a liquid or vaporised at the analyser, unless the analysis requires otherwise.
3.3.7 The pressure reducing regulator shall meet design condition of main process stream/ service.

3.4 Sample Temperature Considerations

3.4.1 Liquid Sampling System

In general and as a preference, liquid sampling system should be operated at as low a

temperature above ambient as possible for safe and convenient operation.
Operating at low temperature shall also be considered to eliminate the possibility of vaporising
light ends if pressure is reduced. If pressure reduction is required, care must be taken to
prevent vaporising.
Liquid samples with a high viscosity shall be maintained hot or heated as required to assure
the proper sample flow throughout the system.

3.4.2 Gas Sampling System

In general and as a preference, gas sampling system shall be operated at as low a pressure
above atmospheric as possible to allow safe and convenient operation.
A low operating pressure is preferred to provide a low sample dew point and minimise
potential condensation, where applicable.
If heating of gas sampling systems is required to maintain the sample temperature above the
dew point, the sampling system components shall be installed in a heated enclosure.
Electrical heaters should be used. Steam heating coils may be considered.
Heat tracing of components shall not be used for gas sample systems.
If required, cooling of gas samples (other than for condensation) shall be accomplished with a
sufficient length of bore tubing in ambient air.
High temperature tubing (above 65°C) shall include a suitable guard and warning for
personnel protection.

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3.5 Heated Sampling System Enclosures

3.5.1 Sample lines shall be terminated inside the heated enclosure with a union and not at bulkhead
fittings on the enclosure wall. Heated sample lines shall enter the sample-conditioning
enclosure via heat shrink entry seals to ensure that the sample temperature is uniformly
maintained.
3.5.2 Penetrations into the enclosure for sample tubing shall provide adequate insulation to prevent
heat loss to the enclosure surface.
3.5.3 Heated enclosures shall be designed with consideration to heat loss during the operation and
inspection of components mounted within.
3.5.4 If opening the enclosure door is required for normal operation or inspection, and if excessive
heat loss occurs when the door is opened for these short periods, then the enclosure shall
include a double-pane viewing window and access ports or extended handles for making
external set point adjustments or valve actuation.
3.5.5 If heating above 65°C is required, a special enclosure shall be designed with appropriate
insulation. The enclosure shall include an inside stainless steel liner to enclose the insulation.
The door shall close with a flush seam to minimise heat loss.
3.5.6 Heating coils or elements inside enclosures shall include a suitable guard and warning for
personnel protection.
3.5.7 All sample system components in the enclosure shall be suitably specified and selected for
heated enclosure temperature.

3.6 Sample Tap and Probe

3.6.1 All samples shall be extracted from process lines or vessels with a low volume sample probe
inserted through the primary process sample tap, isolation valve.
3.6.2 The process isolation valve shall be a 1" Flanged, full-ported gate valve for 6mm and 8mm
tubing probes. Larger gate valves should be used for tubing 12mm or greater in size.
3.6.3 The size of the sample probe shall be determined according to the application to minimise
internal volume.
3.6.4 The size shall be consistent with the design of the sample transport and conditioning system
to provide the required transport delay time.
3.6.5 The sample probe shall have sufficient mechanical strength to maintain rigidity in the flowing
process stream and allow insertion/ extraction. (Heavy-wall tubing, 1.25 mm minimum, is
preferred).
3.6.6 Sample taps shall be located at least 12 pipe diameters from the junction of two streams to
ensure proper mixing. Sample taps shall be at least 12 pipe diameters downstream of a
pressure reducer where two phase flow can exist.
3.6.7 When a sample must be extracted from the process, transported, and conditioned, a sample
probe shall be installed in lines 3 inches or greater in diameter. The sample point shall be
selected to provide easy access, maintainability, fast response time, and a representative
sample. Sample points that could be multi-phase must be avoided.
3.6.8 Probe shall be sized for approximately 30% immersion beyond the inside pipe wall up to a
maximum immersion of 3 inches. A typical fixed flange sample probe is shown in Annex A of
IEC/TR 61831. However, specific installation drawing for the sampling system, sample probe
connection to process and sample collection to be developed during detail engineering stage
with VENDOR information.
3.6.9 The sample probes shall have the mechanical strength to withstand high-velocity flow
conditions. The harmonic calculations shall be performed to predict the mechanical breakpoint
of the sample probe during detailed engineering.

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3.6.10 The flow direction shall be stamped on sample probe for Installation of sample probe on
process line.
3.6.11 The sample probe shall include a packing gland to allow insertion/extraction from the process
stream and closure of the primary isolation valve, if necessary.
3.6.12 The packing gland shall be designed according to the process stream operating conditions
and provide adequate sealing under these conditions for insertion/extraction.
3.6.13 The sample probe shall include a welded stop or equivalent at the tip to prevent complete
extraction from the packing gland.
3.6.14 For liquid streams the tip of the sample probe shall be cut square, reamed and filed smooth.
3.6.15 The sample probe shall include a shutoff valve immediately after the packing gland to allow
isolation of the sample line at the tap.

3.7 Sample Transport Lines

3.7.1 The sample transport lines shall be designed to deliver process samples to the analyser with a
minimum flow and minimum transport time. Maximum allowable transit time shall be decided
as per process requirements.
3.7.2 The size of the sample line shall be determined to optimise these conditions based on the
process conditions and length of run.
3.7.3 In general, the velocity of gas samples in small diameter tubing (i.e. less than 12mm OD) shall
be approximately 3-6 meters per second (higher velocity for larger diameter tubing).
3.7.4 In general, the velocity of liquid samples in small diameter tubing (i.e. less than 12mm OD)
shall be approximately 0.5-1.5 meters per second (higher velocity for larger diameter tubing).
3.7.5 Sample transport tubing is considered part of the sampling system design and should be fully
sized and specified by the sample system VENDOR.
3.7.6 Tube support shall be provided according to requirement. Manufacturer’s documentation shall
be referred for proper installation of electrically heated and/or pre-insulated sample lines and
bundles, particularly for instructions on minimum bending radius, spacing between bundles,
maximum spacing of supports, use of terminator kits, connections to electrical supply,
penetrations through enclosures, and safety precautions.
3.7.7 Sampling transport systems shall be designed and fabricated without low spots, loops, or
pockets that can form traps.
3.7.8 The number of tubing union needs to be reduced through use of continuous tubing run
wherever possible.

3.8 Sample Transport Line Tracing

3.8.1 The requirements for tracing shall be identified on the individual sampling system specification
data sheet.
3.8.2 Sample transport tubing requiring heating shall be pre-insulated, steam traced tubing bundles.
3.8.3 Tracing shall be either critical or non-critical depending on the application.
3.8.4 Critical tracing applications shall be for high temperature (above 65°C) systems or systems
where temperature maintenance is required significantly above the normal ambient to prevent
sample condensation.
3.8.5 Critical tracing applications shall include temperature control with local indication and deviation
alarm.
3.8.6 Non-critical tracing applications shall be for freeze protection or where temperature
maintenance is required to prevent sample condensation but not significantly above the
normal ambient.
3.8.7 Temperature monitoring and control is not required for non-critical tracing applications.

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3.8.8 High temperature sample lines or tracers shall be insulated or guarded for personnel
protection.
3.8.9 Both ends of heat-traced sample tubing shall be sealed to prevent moisture/ corrosion
damage.
3.8.10 The circuit for electrically heat-traced tubing shall include equipment for ground fault
protection.

3.9 Sample Transport Lag Time/By-pass Stream

3.9.1 The sample transport and conditioning system shall be designed to deliver a representative
process sample to the analyser with a minimum transport lag time and minimum consumption
of sample.
3.9.2 The maximum transport lag time from the process stream to the analyser shall be one minute,
unless otherwise specified.
3.9.3 In general, the sample system shall incorporate a fast-flow bypass stream to minimise
transport lag time.
3.9.4 Fast Loop sampling system consisting of the sample tap, the return tap and any pipe or tubing
between them and the sample conditioning system. Fast loops are designed to deliver
samples to the sample conditioning system with acceptable lag times and to return unused
sample to the process or other disposal location. The side stream connects the fast loop to the
analyser.
3.9.5 In side stream, a small quantity of the process sample that has been conditioned (filtered,
cooled, de-pressurised, etc.) as required to make it compatible with the analyser to which it is
delivered. This stream is usually taken from the fast loop.
3.9.6 The sample return point selected directly influences fast loop design.The sample return point
shall be selected to minimize sample conditioning and maintenance.
3.9.7 Analysers that require or can properly operate with total stream flow shall include a separate
analyser bypass to allow isolation of the analyser while maintaining stream flow.
3.9.8 Effluent from the bypass stream shall be preferably routed back to a process return point or to
the low pressure, effluent return system (refer section 3.14).

3.10 Sample Conditioning Design

3.10.1 In general, the sample conditioning system shall be designed to provide filtration and control of
the sample temperature, pressure and flow, as required, for continuous, proper operation of
the analyser as specified and/or recommended by the analyser manufacturer.
3.10.2 The sample conditioning system shall not alter the concentration of measured component.
3.10.3 Other special features shall be included as may be required for a particular analyser and/or
process stream.
3.10.4 Although each sample conditioning system must be specifically designed for the particular
application, standardised approaches should be used for identical or similar situations to
provide consistency and uniformity.
3.10.5 Components of all sample-conditioning systems, whether enclosed or plate mounted, shall be
mounted in such a way that each can readily be removed for maintenance without removing
any others.

3.11 Component Selection

3.11.1 Sampling systems shall be designed and assembled using discrete components to facilitate
convenient maintenance and/or replacement.
3.11.2 Uniformity of component selection shall be a prime consideration to minimise the stocking of
spares and allow convenient substitution.

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3.11.3 Standard sizes and ranges shall be established for components that are available with a wide
variety of sizes and ranges (e.g. gauge ranges and valve orifices).
3.11.4 It is desirable to minimise the number of versions of the same component that can be used for
similar applications.
3.11.5 ORYX GTL Spare Parts Interchangeability records (SPIR list) should be considered when
selecting sample system components

3.11.6 All materials, flange type, pipe fittings, valves, class rating, branch connection details, welding
details and heat treatment shall comply with relevant piping material specifications standard
no. GTL-51-02.

3.12 Materials of Construction

3.12.1 All materials in contact with process samples shall be corrosion resistant for the particular
application.
3.12.2 As a minimum, these materials shall be stainless steel (type 316 preferred), with VITON,
TEFLON, KALREX, or EPR gaskets and seals.
3.12.3 The material of elastomer, packing, O-ring, seal, gasket etc. shall be compatible with process
stream/ service.
3.12.4 No copper, zinc or silver-bearing alloys shall be allowed in contact with process streams.
3.12.5 All special materials that are not standard for the particular component shall be identified on
the sampling system schematic diagram and bill of material.
3.12.6 No mixing of tube fittings of dissimilar metals or different manufacturers is acceptable.

3.13 Sampling System Assembly

3.13.1 Sampling systems shall be designed and assembled as composite units for convenience of
installation and operation.
3.13.2 Sampling systems shall be assembled on panels or in enclosures.
3.13.3 All sampling systems to be installed outdoors shall be assembled in IP65, stainless steel
enclosures, unless otherwise specified.
3.13.4 Sampling system panels shall be 3mm stainless steel plate.
3.13.5 Sampling system enclosures, where required, shall include a door handle and latch kit.
3.13.6 Enclosures shall also include a window (safety glass) for convenient viewing of operating
conditions, unless otherwise specified.
3.13.7 The design and assembly of sampling systems shall give proper consideration to the logical
and consistent organisation and configuration of component parts.
3.13.8 All sampling systems with a similar design shall be assembled similarly.
3.13.9 Components and sample lines shall be organised and assembled to prevent pockets or traps.
3.13.10 Liquid sampling systems shall include high-point vents and low-point drains and enclosures
shall be furnished with a drain point.
3.13.11 Gas sampling systems that might contain condensed liquid shall be designed and assembled
so that liquid is trapped at a low point for draining.
3.13.12 Sampling systems shall not include dead-end pockets, unless required for the particular
component or situation (e.g. pressure, gauges or switches). When required, components with
a dead-end design shall be close-coupled to a flowing stream and located at a point where
possible effects of a dead-end pocket are minimised.

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3.13.13 Sampling systems shall be designed and assembled to prevent cross-contamination of

different sample or calibration streams. 3-way switching valves and double block and bleed
valves are preferred to minimise possible cross-contamination.
3.13.14 Components shall be installed with maximum accessibility for operation and maintenance.
Individual components shall be installed and connected for convenient removal without
disturbing other components.
3.13.15 Filter elements shall be readily accessible for convenient replacement.
3.13.16 Threaded connections shall be minimised in the assembly of sampling systems. Components
with tube fitting connections are preferred.
3.13.17 Brackets and supports for components and tubing shall be minimised to allow maximum
accessibility for removal. However, components that require operation shall be secured and
include a bracket.
3.13.18 The layout and installation of sampling system components shall minimise the complexity of
interconnecting tubing. As a preference and wherever possible components and connections
should be close-coupled. Tubing port-connectors and adapter fittings should be used
whenever possible. However, close coupling should not impede the accessibility of
components for operation, maintenance, or removal.
3.13.19 Remote parts of sampling systems (e.g. field pressure reducing stations) shall be supplied as
completely assembled units to minimise field installation complexity.
3.13.20 Pressure relief valves should be included in the system design if required to prevent the fluid
pressure from rising to a value that would cause analyzer system hardware failure, resulting in
a loss of fluid containment.
3.13.21 All sample handling systems shall be provided with flow and pressure indicators on the fast
loops and inlets to the analysers.

3.14 Effluent Sample Return/ Disposal

3.14.1 Continuous direct venting or draining of process samples is prohibited except in special
situations.
3.14.2 All effluent samples from analysers and sampling systems shall be returned to process or
routed to a low pressure, effluent system, unless otherwise specified.
3.14.3 Liquid samples that cannot be returned to process shall be accumulated in a low pressure,
collection system and pumped back into the process
3.14.4 Gas samples that cannot be returned to process shall be vented to the low pressure flare
system.
3.14.5 Gas sample effluent from analysers that must be operated at atmospheric pressure shall be
routed to the safe atmospheric vent system (refer section 3.15). The flow of effluent sample to
the atmospheric vent system shall be minimised.
3.14.6 Effluent drain lines shall be located below analysers and sampling systems to allow draining.
3.14.7 Effluent vent and drain lines shall be sized to prevent backpressure. In general, pipe headers
shall be used for common effluent collection.
3.14.8 Effluent vent and drain lines shall slope to a low point and include a manual drain valve.
3.14.9 Effluent vent lines that may accumulate liquid carry-over on a regular basis shall include an
automatic liquid drain. This effluent shall be disposed of in a safe manner.
3.14.10 Effluent vent lines that may have liquid condensation shall include an automatic liquid drain or
heat tracing.
3.14.11 Effluent vent or drain lines that may freeze shall be heat traced.
3.14.12 All vent lines going to the flare system or low pressure process lines, shall be fitted with non-
return valves.

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3.14.13 Sample return/ disposal connection shall have permanently fasten corrosion resistance label
to identify service including tag number.

3.15 Atmospheric Vent System

3.15.1 The atmospheric vent system shall be provided if effluent samples from analysers or sampling
systems must be discharged at atmospheric pressure.
3.15.2 The flow of process sample to the atmospheric vent system shall be minimised.
3.15.3 Safe atmospheric vent system shall be approved and certified by relevant departments:
Process, Safety, and Environmental.

3.15.4 Unless otherwise specified, the atmospheric vent system shall consist of piping to route the
sample effluent away from the occupied area for discharge directly into the atmosphere.
3.15.5 The atmospheric vent lines shall be sized to prevent back pressure. In general, pipe headers
shall be used for common atmospheric vent collection.
3.15.6 The atmospheric vent lines shall slope to a low point and include a manual drain valve.
3.15.7 The atmospheric vent lines that may accumulate liquid carry-over on a regular basis shall
include an automatic liquid drainer.
3.15.8 The atmospheric vent lines that may have liquid condensation shall include an automatic liquid
drain or heat tracing.
3.15.9 The atmospheric vent lines that may freeze shall be heat traced.
3.15.10 The atmospheric vent discharge shall meet local/plant environmental requirements.
3.15.11 The atmospheric vent discharge line shall be terminated with a flame arrester, unless
otherwise specified.
3.15.12 The atmospheric vent lines shall be designed to avoid pressure fluctuations other than those
caused by normal atmospheric pressure variations.

3.16 Calibration Sample Introduction

3.16.1 All sampling system shall include facilities for introduction of calibration samples, unless
otherwise specified.
3.16.2 Calibration sample introduction shall be manual unless automatic calibration is specified in the
individual analyser specification data sheet.
3.16.3 Calibration sample introduction shall be made under the same conditions as process sample
is introduced to the analyser, unless otherwise specified.
3.16.4 The calibration sample introduction facilities shall prevent contamination of the calibration
sample by the process stream, by the use of double block and bleed.
3.16.5 Calibration samples shall resemble the process stream, unless otherwise specified.
3.16.6 In general, calibration samples shall be supplied from cylinders.
3.16.7 Cylinder standard samples shall not be used for components that deteriorate or are unstable.
3.16.8 If a permeation system is used to supply calibration samples, it shall be designed as a
permanent part of the sampling system.
3.16.9 Permeation systems shall be designed to operate continuously to provide a stable calibration
supply source.

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3.17 Lab Sample Connection

3.17.1 Where the OWNER requires sample take-off facilities, the extent of these requirements for
each sampling system and sample stream shall be agreed during detailed engineering to
include components for connection of a low pressure laboratory sample cylinder.
3.17.2 The laboratory sample cylinder shall be connected in a flow-through configuration on the
sample bypass stream.
3.17.3 Block and bypass valves shall be included to allow removal of the sample cylinder without
interruption of the bypass stream flow.
3.17.4 The sampling system shall be designed to accommodate the laboratory sample cylinder under
the required operating conditions. This may require a separate cabinet for the sample
cylinder.
3.17.5 The sample handling system shall be designed such that taking of a laboratory sample shall
not affect the performance of the analyser.

3.18 Hazard Prevention

3.18.1 Sampling systems shall be designed and assembled to minimise exposure of personnel to
hazards during operation and maintenance.
3.18.2 Sampling systems operating at high temperature or pressure shall be avoided, unless that is a
must as per design.
3.18.3 Sampling systems that must operate at high temperature or pressure shall be installed in
enclosures with warning nameplates.
3.18.4 All sampling systems shall include appropriate vents and drains to allow purging of sample
lines before maintenance is performed.
3.18.5 Liquid sampling systems shall be installed inside enclosures with drain connections or include
a spill trough to minimise propagation of leakage.
3.18.6 Sampling systems that contain abnormally hazardous material shall include provisions for
purging the entire system with an inert gas or liquid to a closed vent or drain system.
3.18.7 No direct connection of plant utilities shall be made to sample, unless approved by OWNER.
3.18.8 If connection to plant utilities is required, the connection shall be made with a temporary hose
and check valve and include a double-block-and-bleed valve arranged at the process
connection.
3.18.9 Cylinder gas is preferred for purging sampling systems instead of plant utilities.
3.18.10 Sampling systems for process samples that present severe health and safety hazards shall be
installed in gasketed enclosures and include a continuous purge (air or inert gas) with the
purge effluent routed to a closed vent system. If inert gas is used, a warning nameplate should
be placed on the sampling system to indicate this.(refer 3.23.1.2).

3.19 Additional Requirements for Chromatographs

3.19.1 Chromatograph sampling systems shall include a low sample flow switch at the analyser Inlet,
unless specified otherwise.
3.19.2 Chromatographs with gas inject valves shall include a sample shutoff-vent to atmosphere
valve arrangement to allow effluent return to a low pressure.
3.19.3 Chromatograph sampling systems shall include automatic introduction of a quality control
standard sample. This system may be manual if this better meets the requirements.

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3.20 Utilities
3.20.1 The utilities required for operation of the sampling system are to be shown on a sampling
system schematic diagram, developed by the sampling system vendor.
3.20.2 The sampling system VENDOR shall confirm the utilities required for operation.
3.20.3 The sampling system VENDOR shall confirm the anticipated consumption of utilities under
both start-up (maximum) and normal operation.
3.20.4 In general, utilities shall be supplied from pipe headers.
3.20.5 All utility connections shall include a shut-off valve unless otherwise specified.
3.20.6 The utility shut-off valve shall be located on the supply and return header unless the header is
not located adjacent to the sampling system. In this case shut-off valves shall be provided
both at the sampling system and the header tap.

3.21 Gas Cylinders

3.21.1 Cylinder racks shall be equipped with safety chains.
3.21.2 Each cylinder shall be supplied with its own pressure regulator.
3.21.3 Provision shall be made for changing over manually from the operating to standby service gas
cylinders by means of valve manifolds. This requirement does not apply to calibration gas
cylinders.
3.21.4 All cylinders shall be installed at grade.

3.22 Electrical Area Classification

3.22.1 The electrical area classification for the sampling system shall be as specified in the Analyser
Shelter and Local Panels Specification standard no. GTL-64-04.
3.22.2 All alarm switches shall be hermetically sealed contacts, unless otherwise specified.
3.22.3 All electrical devices connected to process streams shall include conduit seals or suitable
barrier glands to prevent process leakage into the electrical system.

3.23 Identification and Tagging

3.23.1 Nameplates

3.23.1.1 Standard nameplates shall be black and white laminated plastic with information engraved
into the white core.
3.23.1.2 Warning nameplates shall be red and white laminated plastic with information engraved into
the white core.
3.23.1.3 Nameplates installed outdoors and exposed to the weather shall be attached with stainless
steel screws, wire or bands (tie-wraps). Rivets are not permitted.

3.23.2 Identification

3.23.2.1 Sampling systems and related subsystems shall be identified with the corresponding
analyser tag number and stream identification.
3.23.2.2 The sample probe and tap shall be identified with the corresponding analyser tag number
and stream identification.
3.23.2.3 All termination points for field connection shall be identified.
3.23.2.4 All valves shall be identified with their function.

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3.23.2.5 All sampling system control components shall be identified with the service and normal
operating setpoint.
3.23.2.6 Heated systems shall be identified with the normal operating temperature.
3.23.2.7 Warning nameplates shall be included at sources of high temperature and pressure (both
inside and outside enclosures, if applicable).
3.23.2.8 Warning nameplates shall be provided to identify sample stream components that may
present abnormal or serious health and safety problems if released from the sampling
system.
3.23.2.9 Warning nameplates shall be provided to identify applications where the sampling system
must be drained and/or purged prior to opening or disassembly for maintenance to prevent
exposure to hazardous or sampling components.

3.24 Inspection and Testing

3.24.1 Pressure Testing

3.24.1.1 Sampling systems and related subsystems shall be pressure tested at 150 percent above
maximum operating condition.
3.24.1.2 The pressure test shall be performed with instrument quality air or nitrogen for both gas and
liquid sampling system applications.
3.24.1.3 Leak detection shall be performed with a bubbler on the supply source to the system after
initial pressurisation.
3.24.1.4 The acceptable leak rate shall be less than five bubbles per minute.
3.24.1.5 Leak testing on high pressure systems shall be limited to 7 bar. However, the full operating
pressure shall be applied to the system prior to the leak test.

3.24.2 Functional Testing

3.24.2.1 Sampling systems and related subsystems shall be functionality tested on fluids that
resemble the sample streams (specific gravity) under conditions that simulate actual process
conditions (temperature, pressure and flow) to verify proper operation.
3.24.2.2 Coolers and heaters shall be functionality tested to verify proper operation.
3.24.2.3 Pressure reducing regulators shall be tested for proper operation.
3.24.2.4 Temperature, pressure and flow switches shall be tested for proper operation and setpoint
actuation.
3.24.2.5 Remote actuated stream switching valves shall be actuated to confirm proper operation, if
applicable.
3.24.2.6 The sampling system VENDOR shall provide all facilities and equipment to perform the
required tests.

3.25 Inspection
3.25.1 Inspection of the sampling system and witness of functional tests shall be required, unless
otherwise specified.
3.25.2 Inspection shall not be performed until preliminary testing has been performed, and the
sampling system is certified to have no leaks, restrictions, etc.
3.25.3 All work shall be visually inspected to verify mechanical completion and compliance with all
design drawings and specifications.
3.25.4 All nameplates and tagging shall be inspected to verify correct identification and attachment.

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3.25.5 Tubing connections shall be spot checked to verify proper cutting and reaming. (No more than
5% of connections shall be checked. However, if improper workmanship is detected, all
connections may be checked at the discretion of the inspector).
3.25.6 Sampling systems shall be leak checked on a spot basis according to the tubing connections
that were disassembled for inspection.
3.25.7 All functional tests shall be witnessed to verify proper operation.

3.26 Shipment

3.26.1 Preparation

3.26.1.1 All sample lines shall be purged clean and dry with instrument quality air or nitrogen.
3.26.1.2 All open connections shall be covered with suitable caps or plugs that shall remain securely
in place during shipment and not deteriorate in outdoor storage. Adhesive tape shall not be
used for this purpose.
3.26.1.3 Tube fitting connections shall have the nuts and ferrules taped in place to prevent loss during
shipment.
3.26.1.4 All moveable parts shall be secured and supported, if required. Adhesive tape is not allowed
for this purpose. (Plastic tie-wraps or straps are preferred).

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4 Roles and Responsibilities

4.1 Implementation of the Document

The custodian has the responsibility to manage and implement the requirements of this Technical
Standard.
Document Custodian
Document custodian must:
 Custodian of the standard shall ensure that departments mentioned in the standard are involved in
the review cycle as part of the development team.
 Ensure that only latest approved documents are filed
 Work with Quality Section to ensure that IMS Documents are maintained according to the
requirements of the Document Management Standard
 Review all the comments of the Development Team and makes the final decision on what
comments to be included. Communicate the Operational Policies, Standards and Technical
Standards
 Ensure the requirements in the documents are implemented
 Be in compliance with the requirements of the documents
 Identify Development/Review Team Members
 Standard Custodian to resolve any raised dispute with development team members

4.2 Content of the Document

Development/Review Team Members

The Development Team Members must:
 Develop the documents only on approved templates
 Ensure that the latest approved documents are uploaded and filed
 Partake in meetings to discuss and timely review the relevant draft document
 Suggests essential changes, including deletion and addition to the document
Head of Quality
Does a final review before approval of Policies, Standards and Technical Standards to ensure that:
 The development team is aligned with the requirements of the Standards and Technical Standards
 Ensure the completeness of the roles and responsibility clause in the Standards and Technical
Standards
 Ensure the completeness of the Standards and Technical Standards (all required clauses are
completed)
 Review the completeness of the requirements in the Standards and Technical Standards
 The appropriate references to procedures and supporting documentation is made
 There is no duplication of information.
 The document content meets the requirements of the Document and Record Management
Standards
 Possible gaps in the information is identified in liaison with the Development Team.
Information Management Specialist
Does a final review of Procedures and Supporting Documentation to ensure that:
 The structure, template, format, correctness and completeness of the documents
 Keep all the document templates updated and make them available to the users
 Ensure the content of the document is aligned with document type

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5 Authorisation
The Projects Services Manager and Chief Engineering & Projects Officer have seen and approved this
document.

6 Revisions

Date Rev. Remarks

01
02
December-2016 03 Section 3 has been comprehensively revised in-line with latest applicable
codes and best industry practices.
July-2020 04 Template update. No revision to contents

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