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AccuStandard Peak Tailing Factor Certificate

This certificate of analysis summarizes information about a peak tailing factor standard reference material produced by AccuStandard, including: - The catalog number, date certified, expiration date, sample size, solvent, and components of the standard - The certified reference material contains 4 components with certified analyte concentrations ranging from 10.00 to 10.08 μg/mL - The standard is guaranteed to be homogeneous and stable through the expiration date when handled and stored properly according to the certificate

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0% found this document useful (0 votes)
147 views2 pages

AccuStandard Peak Tailing Factor Certificate

This certificate of analysis summarizes information about a peak tailing factor standard reference material produced by AccuStandard, including: - The catalog number, date certified, expiration date, sample size, solvent, and components of the standard - The certified reference material contains 4 components with certified analyte concentrations ranging from 10.00 to 10.08 μg/mL - The standard is guaranteed to be homogeneous and stable through the expiration date when handled and stored properly according to the certificate

Uploaded by

mosalamm6
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

125 Market Street Tel (203)786-5290

New Haven, CT 06513 Fax (203)786-5287


USA [Link]

CERTIFICATE OF ANALYSIS
Catalog No: M-528-PTF Date Certified: Nov 3, 2020
Description: Peak Tailing Factor Standard Expiration: Dec 3, 2022
Lot: 215011299-01 Sample Size: 1 mL
Solvent: Dichloromethane Components: 4
Hazards: Refer to SDS for complete safety information Storage Condition: Ambient (>5 °C)

Certified Reference Material

Signal Word: Warning

Component CAS # Purity % Prepared Certified Analyte


Concentration² Concentration¹
(GC/MS) (µg/mL) (µg/mL)
2,4-Dimethylphenol 105-67-9 100.0 10.04 10.04
4-Nitrophenol 100-02-7 99.9 10.04 10.03
Pentachlorophenol 87-86-5 99.0 10.10 10.00
2-Methyl-4,6-dinitrophenol 534-52-1 100.0 10.08 10.08

A product with a suffix (-1A, -2B, etc. or -01, -02, etc.) on its lot number has had its expiration date extended and is identical to the same lot number without the suffix.
² All weights are traceable through NIST, Test No. 822-275872-11
¹ Certified Analyte Concentration = Purity x Prepared Concentration.
The Uncertainty associated with the certified concentration reported on this certificate is ±2.4%. This value is the combined expanded uncertainty and represents an
estimated standard deviation equal to the positive square root of the total variation of the uncertainty of components. A normal distribution is assumed and a coverage
factor of K=2 is chosen using approximately a 95% confidence level.
Labels and certificates follow U.S. Conventions in reporting numerical values: A comma (,) is used to separate units of one-thousand or greater. A period (.) is used as
a decimal place marker.
The information on this certificate may not be reproduced without the express permission of the manufacturer. See reverse side for additional information
Hazard Information: Please refer to the SDS for information regarding the hazards associated with using this material.
This product was prepared according to in-house procedures and is guaranteed to be homogeneous.

Certified By:
Larry Decker, Organic QC Manager

Page 1 of 1 For use in routine laboratory analysis.

AccuStandard is accredited to ISO 17034, ISO/IEC 17025 and certified to ISO 9001:2015 QR-ORG/INO-001
Rev. 5/18
1. Quality Standards:
ISO 17034:2016 – General Requirements for the Competence of
Reference Material Producers ANAB Certificate Number AR-1463
ISO/IEC 17025:2017 – General Requirements for the Competence of
Testing And Calibration Laboratories ANAB Certificate Number AT-1339
ISO 9001:2015 – Quality Management System – Requirements
Eagle Registrations Certificate Number 3774

2. Intended Use: The product covered by this certificate is designed for calibration or for use in quality control procedures
for the specified chemical compounds listed on the reverse side. This product can be used for quantification and/or
identification. This product can also be used as a reference material to validate analytical procedures, subject to the
conditions under Section 7.

3. Manufacturing: All balances are calibrated daily using an in-house procedure with weights that are compared annually
to master weights and traceable to NIST. The balances are also calibrated annually by an ISO/IEC 17025 accredited
calibration laboratory. Please refer to the NIST test number listed on the front of this certificate. Class A glassware
is used in the manufacture and quality control of all standards. Good Laboratory Practices have been used throughout
the preparation of this Standard.

4. Homogeneity: This product is sufficiently homogeneous and any sample size would be within the uncertainty budget.

5. Stability: The manufacturer guarantees the stability of this solution through the expiration date stated on the label,
when handled and stored according to the conditions stated on the label

6. Uncertainty: The uncertainty values as stated on the face of this certificate have been determined using the
EURACHEM/CITAC Guide. We report a combined expanded uncertainty equal to the positive square root of the total
variance of the uncertainty of the components using the following formula: ua = (u(V))2 + (u(m))2 + (u(IV))2 + (u(RO))2 This
formula represents uncertainty components from the mass, volume, short-term stability, long-term stability and
homogeneity factors associated with the production of this product. The expanded uncertainty, assumes a normal
distribution and a coverage factor of k=2 is chosen using approximately a 95% confidence level.

7. Legal Notice and Limit of Liability: This product is for routine laboratory analysis and research purposes only. The
company’s liability will be limited to replacement of product or refund of purchase price. Notice of claims must be made
within thirty (30) days from date of delivery.

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