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Certificate of Analysis

This document provides a certificate of analysis for a batch of the product Deltamethrin with batch number BCCC3146. It specifies details such as the product name, number, expiration date, and quality release date. It also lists the results of tests performed on the batch for specifications like appearance, purity, specific rotation, melting point, and proton NMR spectrum. The tests confirm the batch properties match specifications and the purity is 98.6% by HPLC area percentage.

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Basha Yazn Anjak
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378 views2 pages

Certificate of Analysis

This document provides a certificate of analysis for a batch of the product Deltamethrin with batch number BCCC3146. It specifies details such as the product name, number, expiration date, and quality release date. It also lists the results of tests performed on the batch for specifications like appearance, purity, specific rotation, melting point, and proton NMR spectrum. The tests confirm the batch properties match specifications and the purity is 98.6% by HPLC area percentage.

Uploaded by

Basha Yazn Anjak
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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3050 Spruce Street, Saint Louis, MO 63103 USA

Email USA: [email protected] Outside USA: [email protected]

Certificate of Analysis
Product Name: Deltamethrin
PESTANAL, analytical standard
Product Number: 45423
Batch Number: BCCC3146
Brand: Sigma-Aldrich
CAS Number: 52918-63-5
Formula: C22H19Br2NO3
Formula Weight: 505.20
Expiration Date: OCT 2024
Quality Release Date: 12 NOV 2019

TEST SPECIFICATION RESULT


APPEARANCE (COLOR) WHITE TO FAINT BROWN AND FAINT OFF-WHITE
BEIGE AND FAINT YELLOW

APPEARANCE (FORM) POWDER OR CRYSTALS CRYSTALS


PURITY (HPLC AREA %) ≥ 98.0 % 98.6 %
SPECIFIC ROTATION (20/D) 22.0 ± 3.0 DEGREES 23.3 DEGREES
CONCENTRATION -- C=1.4 IN CHLOROFORM
MELTING POINT 98 - 103 C 101 C
WATER ≤ 1.0 % 0.1 %
PROTON NMR SPECTRUM CONFORMS TO STRUCTURE CONFORMS

Dr. Reinhold Schwenninger


Quality Assurance
Buchs, Switzerland

Sigma-Aldrich warrants that at the time of the quality release or subsequent retest date this product conformed to the information contained in this publication. The current

specification sheet may be available at Sigma-Aldrich.com. For further inquiries, please contact Technical Service. Purchaser must determine the suitability of the product

for its particular use. See reverse side of invoice or packing slip for additional terms and conditions of sale.

Sigma-Aldrich Certificate of Analysis - Product 45423 Lot BCCC3146 Page 1 of 2


3050 Spruce Street, Saint Louis, MO 63103 USA
Email USA: [email protected] Outside USA: [email protected]

Certificate of Analysis

45423 Deltamethrin

Lot Number: BCCC3146 Sample Name: T60225_001

Dionex Ultimate 3000 RSLC


Pump : LPG-3400RS Injection Time: 04.11.19 12:29
Autosampler: WPS-3000 Processed By: murthale
Detector: VWD-3400 Vial Number: RA6
Column: Supelco Ascentis Express C18, 2.7 um Column S/N: -
Column Dim.: 150 x 2.1 mm Sample Type: Unknown
Mobile Phase: Injection Volume: 1.0 µl
%A : Acetonitril Flow: 0.50 ml/min
%B : %B Column Temp. (°C): 35.0
%C : %C Run Time: 20.00 min
%D : H3PO4 0.01 M
Gradient : see Figure 1
Sample Prep.: 1 mg sample in 1 ml methanol

Figure 1: Zoomed Chromatogram

No. Ret.Time Peak Name Area Height Amount Rel.Area


min mAU*min mAU %
1 1.917 0.07915 1.95782 n.a. 0.07
2 3.315 0.05291 0.81650 n.a. 0.05
3 6.483 0.06902 1.07593 n.a. 0.06
4 11.507 Deltamethrin 115.14977 2009.47734 n.a. 98.61
5 11.595 1.38856 44.01272 n.a. 1.19
6 12.187 0.01372 0.26951 n.a. 0.01
7 14.640 0.02173 0.51892 n.a. 0.02
Total: 116.77486 2058.12875 100.00
Table 1: Integration

Sigma-Aldrich Certificate of Analysis - Product 45423 Lot BCCC3146 Page 2 of 2

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