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XRay Analysis Introduction

This document outlines a course on X-ray analysis. The course will cover topics like crystallography, X-ray interactions with matter, X-ray diffraction methods including powder XRD and X-ray fluorescence. Students will learn how to obtain molecule structures using X-ray crystallography and analyze samples using different X-ray techniques. The course will be assessed through assignments, presentations, tests and a final exam. It provides a week-by-week schedule covering each chapter and recommended references to support student learning.

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uyoi ona
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236 views13 pages

XRay Analysis Introduction

This document outlines a course on X-ray analysis. The course will cover topics like crystallography, X-ray interactions with matter, X-ray diffraction methods including powder XRD and X-ray fluorescence. Students will learn how to obtain molecule structures using X-ray crystallography and analyze samples using different X-ray techniques. The course will be assessed through assignments, presentations, tests and a final exam. It provides a week-by-week schedule covering each chapter and recommended references to support student learning.

Uploaded by

uyoi ona
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd

ZCE 451/3

X-RAY ANALYSIS
X-RAY ?
X-RAY ?
X-RAY CRYSTALOGRAPHY
POWDER XRD
XRF

X-RAY ANALYSIS ?
X-RAY DIFFRACTION
Older method

Latest method
LESSON OUTCOME
Upon completion of this course, students should be able to:
• understand how the structure of a molecule obtained by X-ray
crystallographic methods.
• apply and analyze the analysis of X-ray Diffraction in powder,
fluorescence and other related methods.
• sketch, label and analyze X-ray analysis component.
• explain and justify the role of each method in analysis of X-ray.
CHAPTERS
Chapter TOPIC
1 The Concept of Microstructure
2 X-Rays Interactions with matter
3 Crystallography and Crystal Structure
4 X-Ray Diffraction (XRD) Method
5 Systematic Absences in Crystal Data
7 Structure Determination
8 Powder XRD (PXRD)
9 X-Ray Flourescence (XRF)
COURSE ASSESSMENT
1. Continuous assessment: 40%
a. Assignment = 10%
b. Presentation = 5%
c. Test (2) = 20%
d. Pop-Quizzes = 5%
2. End of semester examination: 60%
ZCE451
1:30- 2:50 pm
Week Date Class Course Content
begin-end
1 09.09.2019 - 15.09.2019 Lecture 1 Outline
2 16.09.2019 - 22.09.2019 Lecture 1 Introduction Crystallography
3 23.09.2019 - 29.09.2019 Lecture 2 X-Ray Interactions With Matter
4 30.09.2019 - 06.10.2019 Lecture 2 X-Ray Interactions With Matter
5 07.10.2019 - 13.10.2019 Lecture 3 Crystallography and Crystal Structure
6 14.10.2019 - 20.10.2019 Lecture 3 Crystallography and Crystal Structure
7 21.10.2019 - 27.10.2019 Lecture 4 X-Ray Diffraction
TEST 1
8 28.10.2019 - 03.11.2019 Mid-Semester Break
9 04.11.2019 - 10.11.2019 Lecture 4 X-Ray Diffraction
10 11.11.2019 - 17.11.2019 Lecture 4 X-Ray Diffraction
11 18.11.2019 - 24.11.2019 Lecture 5 Absences in Crystal Data
12 25.11.2019 - 01.12.2019 Lecture 6 Structure Determination
13 02.12.2019 - 08.12.2019 Lecture 7 Powder X-Ray Diffraction
14 09.12.2019 - 15.12.2019 Lecture 7 X-Ray Fluorescence
15 16.12.2019 - 22.12.2019 Lecture 8 Presentation Week
TEST 2
16 23.12.2019 - 29.12.2019: Revision Week

17-19 30.12.2019- 9.01.2020: Examination Weeks

20-23 20.01.2020 - 16.02.2020 : Semester Break


Recommended Study Sources
 Ooi L-L. Principles of X-ray crystallography, Oxford University Press, 2009.
 Giacovazzo C. Fundamentals of Crystallography (IUCr), Oxford University Press, 1992.
 Ladd M.F.C. & Palmer R.A. Structure determination by X-ray Crystallography, Plenum
Press, 1993.
 Jenkins R. & Snyder R.L. Introduction to X-Ray Powder Diffractometry. John Wiley and
Sons, 1996.
 Jenkins R, Gould RW & Gedcke D. Quantitative X-ray Spectrometry, CRC press, 1995.

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