CONTINUOUS DISTILLATION
PILOT PLANT
DS
Mod. UDC/EV manual
Mod. UDCc/EV manual with data logging
Mod. UDCa/EV automated
CHEMICAL ENGINEERING
INTRODUCTION TRAINING PROGRAM
The solution having to be distilled, stored in a glass tank, is sent This unit enables to deepen
to the distillation column by a metering pump after crossing a the following issues:
pre-heating exchanger. • Distillation of different mixtures (water / ethanol, water /
The distillation column is completely made of glass and it methanol, methanol / propanol, etc...) versus the variation
consists of a reboiler, of a bubble-cap-tray column and of a of the following operational parameters:
condenser with reflux head and valve. - reflux ratio
The bottom product and the distillate are collected into two - feeding flow rate
tanks after being cooled by two heat exchangers. - reboiler heating power
The automated version mod. UDCa/EV is equipped with PID - feeding composition
controller: using two pneumatic valves, this controller can - residual pressure
automatically control the flow rate of cooling water crossing • Mass balance
the condenser and the vacuum degree of the plant. • Energy balance
24B-E-DS-UDC-1
• Flooding
• Calculation of the number of theoretical trays
• Automatic flow and pressure control by PID controller
(for mod. UDCa/EV, only)
• Plant supervision by P.C. (for mod. UDCa/EV, only)
ELETTRONICA VENETA S.P.A. - 31045 Motta di Livenza (TV) Italy - Via Postumia 16 - Tel. +39 0422 765 802 - Fax +39 0422 861 901 - E-mail: [email protected] DS 11
TECHNICAL SPECIFICATIONS: Mod. UDCa/EV
Besides being provided with all the Technical specifications of
Mod. UDC/EV
DS
mod. UDC/EV, this model also includes the following additional
• Framework of AISI 304 stainless steel with castors items:
• Distillation column of borosilicate glass with 7 bubble cap • Oil vacuum pump with flow rate of 4 m3/h
trays, DN50, h = 600 mm • Variable area flowmeter of AISI 304 stainless steel, with
• Reboiler of borosilicate glass, with capacity of 3 l, including range of 20 to 250 l/h and 4-20 mA output signal
electric heater of 1600 W • Pneumatic valve of AISI 316 stainless steel for controlling
the flow rate of the condenser cooling water, Cv = 0.32
• Condenser of borosilicate glass with reflux head
• Pneumatic valve of AISI 316 stainless steel for controlling
• Feeding tank of borosilicate glass with capacity of 5 l
the residual pressure, Cv = 0.32
• Tank of borosilicate glass with capacity of 1 l for the
• 2 electropneumatic converters of 4 to 20 mA/ 0.2 to 1 bar
collection of distillate
• Electronic residual pressure transmitter of stainless steel,
• Tank of borosilicate glass with capacity of 2 l for the range of 0 to 1000 mbar, 4-20 mA output signal
collection of bottom product • Microprocessor digital PID controller with serial card
• 3 tube-in-tube heat exchangers of AISI 304 stainless steel • Supervision software for Windows: it enables to control
• Metering pump with head of AISI 316 stainless steel, flow ON-OFF signals, analog signals coming from the PID
rate of 0 to 8.5 l/h controller, real-time trend and historical trend
• 6 thermoresistances Pt100 with sheath of AISI 316
stainless steel Power supply: 230 Vac 50 Hz single-phase - 2 kVA
• 6 electronic indicators (Other voltage and frequency on request)
Dimensions: 1600 × 700 × 2100 mm
• Thyristor unit for controlling the power of reboiler electric
Weight: 130 kg
heater
CHEMICAL ENGINEERING
• 2 programmable timers for the control of reflux ratio
• Variable area flowmeter of glass and steel, with range of
20 to 250 l/h (for mod. UDC/EV, only)
• Vacuum gauge of AISI 304 stainless steel, with range of
0 to -1 bar
• Vacuum circuit with trap of AISI 304 stainless steel
• Piping and valves of AISI 304 and AISI 316 stainless steel REQUIRED
• Switchboard IP55, complying with EC conformity mark, UTILITIES (PROVIDED BY THE CUSTOMER)
including plant synoptic and ELCB • Tap water: 250 l/h @ 2 bar (valve with ½” hose connector)
• Emergency button • Compressed air (for mod. UDCa/EV, only): 1 Nm3/h @ 6 bar
(valve with connection of ¼” F)
• Water floor drain
• Fume suction system
ACCESSORIES (NOT INCLUDED)
• Analytical instruments for analyzing the composition of the
distilled mixture (e.g.: a refractometer)
Mod. UDCc/EV • Personal Computer running Windows (for mod. UDCc/EV
and mod. UDCa/EV, only)
Besides being provided with all the technical specifications of
mod. UDC/EV, this model also includes the following additional
items: SUPPLIED WITH
• Variable area flowmeter of AISI 304 stainless steel, with THEORETICAL – EXPERIMENTAL
range of 20 to 250 l/h and 4-20 mA output signal HANDBOOK
• Electronic residual pressure transmitter of stainless steel,
range of 0 to 1000 mbar, 4-20 mA output signal OPTIONAL
• Interface for the connection with the PC included in the • Electronic pressure transmitter for measurement of load
switchboard loss in the column
• Data acquisition software for Windows • Oil vacuum pump (mod. UDC/EV and UDCc/EV only)
• Borosilicate glass distillation column with sieve trays, DN 50
• Borosilicate glass distillation column with Raschig rings
packing, DN 50
24B-E-DS-UDC-1
VARIATIONS OF THE PLANT ON REQUEST
The equipment can be modified on request of the Customer.
DS 12 ELETTRONICA VENETA S.P.A. - 31045 Motta di Livenza (TV) Italy - Via Postumia 16 - Tel. +39 0422 765 802 - Fax +39 0422 861 901 - E-mail: [email protected]
