Transactions of The Canadian Society for Mechanical Engineering, Sep 1, 2022
This study discusses the effectual variable parameters of multi-walled carbon nanotubes and titan... more This study discusses the effectual variable parameters of multi-walled carbon nanotubes and titanium oxide (MWCNT–TiO2) contents and welding current in obtaining a response on mechanical behavior. The experimental work involved three levels of both parameters, which included 1, 1.5, and 2 wt.% of MWCNTs–TiO2 and 160, 180, and 200 A of current by forming a full design that represented a 32 (3 k) factorial model. The results of an analysis of variance (ANOVA) were critically employed to assess the variation between the variables and within their levels for approaching the significant combination of parameters. The joints welded with MWCNT–TiO2-coated fillers tendered a significant reduction in grain size (GS) along with high values of tensile strength (TS). From the ANOVA, it was determined that both the investigated parameters and their combined effect created a significant response for GS reduction and increment in TS. The presented empirical regression quadratic model was validated for the adequacy of the projected results that were shown to be acceptable with the experimental investigated data. In addition, the desirability function approach was applied for a multiple response optimization in yielding the desired responses of GS and TS and simultaneously providing an optimized set of process parameters. Thus, the function declared 1.5 wt.% MWCNT–TiO2 and 180 A as the optimized process set for delivering the maximum TS at the designated range of GS for this system.
Purpose This study aims to describe the effects of capillary forces or action, viscosity, gravity... more Purpose This study aims to describe the effects of capillary forces or action, viscosity, gravity and inertia via the computational fluid dynamics (CFD) analysis. The study also includes distribution of the binder droplet over the powder bed after interacting from different heights. Design/methodology/approach Additive manufacturing (AM) has revolutionized many industries. Binder jetting (BJT) is a powder-based AM method that enables the production of complex components for a wide range of applications. The pre-densification interaction of binder and powder is vital among various parameters that can affect the BJT performance. In this study, BJT process is studied for the binder interaction with the powder bed of SS316L. The effect of the droplet-powder distance is thoroughly analysed. Two different droplet heights are considered, namely, h1 (zero) and h2 (9.89 mm). Findings The capillary and inertial effects are predominant, as the distance affects these parameters significantly. The binder spreading and penetration depth onto the powder bed is influenced directly by the distance of the binder droplet. The former increases with an increase in latter. The binder distribution over the powder bed, whether uniform or not, is studied by the stream traces. The penetration depth of the binder was also observed along the cross-section of the powder bed through the same. Originality/value In this work, the authors have developed a more accurate representative discrete element method of the powder bed and CFD analysis of binder droplet spreading and penetration inside the powder bed using Flow-3D. Moreover, the importance of the splashing due to the binder’s droplet height is observed. If splashing occurs, it will produce distortion in the powder, resulting in a void in the final part.
This article is an open access article distributed under the terms and conditions of the Creative... more This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY
The synthesis and manufacturing of polymer nanocomposites have garnered interest in recent resear... more The synthesis and manufacturing of polymer nanocomposites have garnered interest in recent research and development because of their superiority compared to traditionally employed industrial materials. Specifically, polymer nanocomposites offer higher strength, stronger resistance to corrosion or erosion, adaptable production techniques, and lower costs. The vat photopolymerization (VPP) process is a group of additive manufacturing (AM) techniques that provide the benefit of relatively low cost, maximum flexibility, high accuracy, and complexity of the printed parts. In the past few years, there has been a rapid increase in the understanding of VPP-based processes, such as high-resolution AM methods to print intricate polymer parts. The synergistic integration of nanocomposites and VPP-based 3D printing processes has opened a gateway to the future and is soon expected to surpass traditional manufacturing techniques. This review aims to provide a theoretical background and the engineering capabilities of VPP with a focus on the polymerization of nanocomposite polymer resins. Specifically, the configuration, classification, and factors affecting VPP are summarized in detail. Furthermore, different challenges in the
Herein, we demonstrate a facile approach in the fabrication of one-dimensional ZnO nanowires (NWs... more Herein, we demonstrate a facile approach in the fabrication of one-dimensional ZnO nanowires (NWs) from the vacuum die-casting method in assistance with anodic aluminum oxide (AAO) template. The casting method enables molten Zn to embed uniformly over the AAO nanomould under high pressure and temperature of 500 C. Besides, the significant influence of the oxidation time and temperature stimulates the ZnO NWs growth inside the AAO nanochannels. The oxidation in the nanochannels was profoundly controlled by the inward diffusion of oxygen atoms and the ZnO grows perpendicular towards the surface which obeys the parabolic law. The TEM and XRD results revealed the ZnO wurtzite crystalline structure with preferential orientation along the c-axis. The relationship between ZnO geometry and function of oxidation parameters is demonstrated by microscopic and spectroscopic analysis. The obtained NWs from the chemical etching process resulted in high crystalline, homogeneous, and high-aspect ratio ZnO NWs in relationship with the AAO pore dimension. Further, the as-prepared ZnO NWs electrical properties were measured in a four-electrode system through the single nanowire device fabricated by FIB. The obtained current-voltage characteristic curves exhibited hysterias loop in consequence with the space charge limited current effect of ZnO NW, which confirms its potential to be used in practical electronic applications.
Purpose This study aims to describe the effects of capillary forces or action, viscosity, gravity... more Purpose This study aims to describe the effects of capillary forces or action, viscosity, gravity and inertia via the computational fluid dynamics (CFD) analysis. The study also includes distribution of the binder droplet over the powder bed after interacting from different heights. Design/methodology/approach Additive manufacturing (AM) has revolutionized many industries. Binder jetting (BJT) is a powder-based AM method that enables the production of complex components for a wide range of applications. The pre-densification interaction of binder and powder is vital among various parameters that can affect the BJT performance. In this study, BJT process is studied for the binder interaction with the powder bed of SS316L. The effect of the droplet-powder distance is thoroughly analysed. Two different droplet heights are considered, namely, h1 (zero) and h2 (9.89 mm). Findings The capillary and inertial effects are predominant, as the distance affects these parameters significantly. T...
The synergistic integration of nanocomposites and 3D printing has opened a gateway to the future ... more The synergistic integration of nanocomposites and 3D printing has opened a gateway to the future and is soon expected to surpass its rivalry with traditional manufacturing techniques. However, there is always a challenge associated with preparing a nanocomposite resin for polymerization-based 3D printing, which is the agglomeration of nanoparticles. Due to the high surface-area-to-volume ratio, the nanoparticles form clusters in the composite matrix, which affects the final properties. This paper aims to analyze the effects of graphene oxide (GO) dispersion on the mechanical and thermal properties of 3D-printed nanocomposites. In particular, a well-dispersed sonication dispersion route is employed for analyzing high and poor GO dispersions and their effects on different properties. After different microscopic analyses and testing, the optimum sonication condition was 30 min at an amplitude of 70%. In terms of mechanical properties, both tensile and compression strength first increas...
The synthesis and manufacturing of polymer nanocomposites have garnered interest in recent resear... more The synthesis and manufacturing of polymer nanocomposites have garnered interest in recent research and development because of their superiority compared to traditionally employed industrial materials.
Transactions of the Canadian Society for Mechanical Engineering
This study discusses the effectual variable parameters of multi-walled carbon nanotubes and titan... more This study discusses the effectual variable parameters of multi-walled carbon nanotubes and titanium oxide (MWCNT–TiO2) contents and welding current in obtaining a response on mechanical behavior. The experimental work involved three levels of both parameters, which included 1, 1.5, and 2 wt.% of MWCNTs–TiO2 and 160, 180, and 200 A of current by forming a full design that represented a 32 (3 k) factorial model. The results of an analysis of variance (ANOVA) were critically employed to assess the variation between the variables and within their levels for approaching the significant combination of parameters. The joints welded with MWCNT–TiO2-coated fillers tendered a significant reduction in grain size (GS) along with high values of tensile strength (TS). From the ANOVA, it was determined that both the investigated parameters and their combined effect created a significant response for GS reduction and increment in TS. The presented empirical regression quadratic model was validated...
Transactions of the Canadian Society for Mechanical Engineering
In this study, we have developed a swift and well-ordered growth of the Anodic Aluminum Oxide (AA... more In this study, we have developed a swift and well-ordered growth of the Anodic Aluminum Oxide (AAO) nanoporous structure by two-step high temperature anodization of pure Aluminum substrate. The pre-anodization surface treatment of the aluminum substrate assists in the formation of well-organized nanoporous structures. The two-step anodization process was performed in 0.3 M of oxalic acid at 20 °C for 40 V and 45 V to obtain tunable pore diameters. The high temperature of the electrolyte solution helps in the rapid growth of the AAO nanoporous structure. The top surface image of AAO shows a well-ordered nanoporous structure with an average pore diameter of 70 nm at 40 V and 100 nm at 45 V. The SEM cross sectional view also illustrates the well-ordered nano channel and the elemental mapping elaborates the presence of aluminum and oxygen. The thickness of the AAO nanoporous structure was determined by using SEM for three anodization time spans (20, 24 and 28 hours), in which an increas...
Herein, we demonstrate a facile approach in the fabrication of one-dimensional ZnO nanowires (NWs... more Herein, we demonstrate a facile approach in the fabrication of one-dimensional ZnO nanowires (NWs) from the vacuum die-casting method in assistance with anodic aluminum oxide (AAO) template. The casting method enables molten Zn to embed uniformly over the AAO nanomould under high pressure and temperature of 500 °C. Besides, the significant influence of the oxidation time and temperature stimulates the ZnO NWs growth inside the AAO nanochannels. The oxidation in the nanochannels was profoundly controlled by the inward diffusion of oxygen atoms and the ZnO grows perpendicular towards the surface which obeys the parabolic law. The TEM and XRD results revealed the ZnO wurtzite crystalline structure with preferential orientation along the c-axis. The relationship between ZnO geometry and function of oxidation parameters is demonstrated by microscopic and spectroscopic analysis. The obtained NWs from the chemical etching process resulted in high crystalline, homogeneous, and high-aspect r...
Transactions of The Canadian Society for Mechanical Engineering, Sep 1, 2022
This study discusses the effectual variable parameters of multi-walled carbon nanotubes and titan... more This study discusses the effectual variable parameters of multi-walled carbon nanotubes and titanium oxide (MWCNT–TiO2) contents and welding current in obtaining a response on mechanical behavior. The experimental work involved three levels of both parameters, which included 1, 1.5, and 2 wt.% of MWCNTs–TiO2 and 160, 180, and 200 A of current by forming a full design that represented a 32 (3 k) factorial model. The results of an analysis of variance (ANOVA) were critically employed to assess the variation between the variables and within their levels for approaching the significant combination of parameters. The joints welded with MWCNT–TiO2-coated fillers tendered a significant reduction in grain size (GS) along with high values of tensile strength (TS). From the ANOVA, it was determined that both the investigated parameters and their combined effect created a significant response for GS reduction and increment in TS. The presented empirical regression quadratic model was validated for the adequacy of the projected results that were shown to be acceptable with the experimental investigated data. In addition, the desirability function approach was applied for a multiple response optimization in yielding the desired responses of GS and TS and simultaneously providing an optimized set of process parameters. Thus, the function declared 1.5 wt.% MWCNT–TiO2 and 180 A as the optimized process set for delivering the maximum TS at the designated range of GS for this system.
Purpose This study aims to describe the effects of capillary forces or action, viscosity, gravity... more Purpose This study aims to describe the effects of capillary forces or action, viscosity, gravity and inertia via the computational fluid dynamics (CFD) analysis. The study also includes distribution of the binder droplet over the powder bed after interacting from different heights. Design/methodology/approach Additive manufacturing (AM) has revolutionized many industries. Binder jetting (BJT) is a powder-based AM method that enables the production of complex components for a wide range of applications. The pre-densification interaction of binder and powder is vital among various parameters that can affect the BJT performance. In this study, BJT process is studied for the binder interaction with the powder bed of SS316L. The effect of the droplet-powder distance is thoroughly analysed. Two different droplet heights are considered, namely, h1 (zero) and h2 (9.89 mm). Findings The capillary and inertial effects are predominant, as the distance affects these parameters significantly. The binder spreading and penetration depth onto the powder bed is influenced directly by the distance of the binder droplet. The former increases with an increase in latter. The binder distribution over the powder bed, whether uniform or not, is studied by the stream traces. The penetration depth of the binder was also observed along the cross-section of the powder bed through the same. Originality/value In this work, the authors have developed a more accurate representative discrete element method of the powder bed and CFD analysis of binder droplet spreading and penetration inside the powder bed using Flow-3D. Moreover, the importance of the splashing due to the binder’s droplet height is observed. If splashing occurs, it will produce distortion in the powder, resulting in a void in the final part.
This article is an open access article distributed under the terms and conditions of the Creative... more This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY
The synthesis and manufacturing of polymer nanocomposites have garnered interest in recent resear... more The synthesis and manufacturing of polymer nanocomposites have garnered interest in recent research and development because of their superiority compared to traditionally employed industrial materials. Specifically, polymer nanocomposites offer higher strength, stronger resistance to corrosion or erosion, adaptable production techniques, and lower costs. The vat photopolymerization (VPP) process is a group of additive manufacturing (AM) techniques that provide the benefit of relatively low cost, maximum flexibility, high accuracy, and complexity of the printed parts. In the past few years, there has been a rapid increase in the understanding of VPP-based processes, such as high-resolution AM methods to print intricate polymer parts. The synergistic integration of nanocomposites and VPP-based 3D printing processes has opened a gateway to the future and is soon expected to surpass traditional manufacturing techniques. This review aims to provide a theoretical background and the engineering capabilities of VPP with a focus on the polymerization of nanocomposite polymer resins. Specifically, the configuration, classification, and factors affecting VPP are summarized in detail. Furthermore, different challenges in the
Herein, we demonstrate a facile approach in the fabrication of one-dimensional ZnO nanowires (NWs... more Herein, we demonstrate a facile approach in the fabrication of one-dimensional ZnO nanowires (NWs) from the vacuum die-casting method in assistance with anodic aluminum oxide (AAO) template. The casting method enables molten Zn to embed uniformly over the AAO nanomould under high pressure and temperature of 500 C. Besides, the significant influence of the oxidation time and temperature stimulates the ZnO NWs growth inside the AAO nanochannels. The oxidation in the nanochannels was profoundly controlled by the inward diffusion of oxygen atoms and the ZnO grows perpendicular towards the surface which obeys the parabolic law. The TEM and XRD results revealed the ZnO wurtzite crystalline structure with preferential orientation along the c-axis. The relationship between ZnO geometry and function of oxidation parameters is demonstrated by microscopic and spectroscopic analysis. The obtained NWs from the chemical etching process resulted in high crystalline, homogeneous, and high-aspect ratio ZnO NWs in relationship with the AAO pore dimension. Further, the as-prepared ZnO NWs electrical properties were measured in a four-electrode system through the single nanowire device fabricated by FIB. The obtained current-voltage characteristic curves exhibited hysterias loop in consequence with the space charge limited current effect of ZnO NW, which confirms its potential to be used in practical electronic applications.
Purpose This study aims to describe the effects of capillary forces or action, viscosity, gravity... more Purpose This study aims to describe the effects of capillary forces or action, viscosity, gravity and inertia via the computational fluid dynamics (CFD) analysis. The study also includes distribution of the binder droplet over the powder bed after interacting from different heights. Design/methodology/approach Additive manufacturing (AM) has revolutionized many industries. Binder jetting (BJT) is a powder-based AM method that enables the production of complex components for a wide range of applications. The pre-densification interaction of binder and powder is vital among various parameters that can affect the BJT performance. In this study, BJT process is studied for the binder interaction with the powder bed of SS316L. The effect of the droplet-powder distance is thoroughly analysed. Two different droplet heights are considered, namely, h1 (zero) and h2 (9.89 mm). Findings The capillary and inertial effects are predominant, as the distance affects these parameters significantly. T...
The synergistic integration of nanocomposites and 3D printing has opened a gateway to the future ... more The synergistic integration of nanocomposites and 3D printing has opened a gateway to the future and is soon expected to surpass its rivalry with traditional manufacturing techniques. However, there is always a challenge associated with preparing a nanocomposite resin for polymerization-based 3D printing, which is the agglomeration of nanoparticles. Due to the high surface-area-to-volume ratio, the nanoparticles form clusters in the composite matrix, which affects the final properties. This paper aims to analyze the effects of graphene oxide (GO) dispersion on the mechanical and thermal properties of 3D-printed nanocomposites. In particular, a well-dispersed sonication dispersion route is employed for analyzing high and poor GO dispersions and their effects on different properties. After different microscopic analyses and testing, the optimum sonication condition was 30 min at an amplitude of 70%. In terms of mechanical properties, both tensile and compression strength first increas...
The synthesis and manufacturing of polymer nanocomposites have garnered interest in recent resear... more The synthesis and manufacturing of polymer nanocomposites have garnered interest in recent research and development because of their superiority compared to traditionally employed industrial materials.
Transactions of the Canadian Society for Mechanical Engineering
This study discusses the effectual variable parameters of multi-walled carbon nanotubes and titan... more This study discusses the effectual variable parameters of multi-walled carbon nanotubes and titanium oxide (MWCNT–TiO2) contents and welding current in obtaining a response on mechanical behavior. The experimental work involved three levels of both parameters, which included 1, 1.5, and 2 wt.% of MWCNTs–TiO2 and 160, 180, and 200 A of current by forming a full design that represented a 32 (3 k) factorial model. The results of an analysis of variance (ANOVA) were critically employed to assess the variation between the variables and within their levels for approaching the significant combination of parameters. The joints welded with MWCNT–TiO2-coated fillers tendered a significant reduction in grain size (GS) along with high values of tensile strength (TS). From the ANOVA, it was determined that both the investigated parameters and their combined effect created a significant response for GS reduction and increment in TS. The presented empirical regression quadratic model was validated...
Transactions of the Canadian Society for Mechanical Engineering
In this study, we have developed a swift and well-ordered growth of the Anodic Aluminum Oxide (AA... more In this study, we have developed a swift and well-ordered growth of the Anodic Aluminum Oxide (AAO) nanoporous structure by two-step high temperature anodization of pure Aluminum substrate. The pre-anodization surface treatment of the aluminum substrate assists in the formation of well-organized nanoporous structures. The two-step anodization process was performed in 0.3 M of oxalic acid at 20 °C for 40 V and 45 V to obtain tunable pore diameters. The high temperature of the electrolyte solution helps in the rapid growth of the AAO nanoporous structure. The top surface image of AAO shows a well-ordered nanoporous structure with an average pore diameter of 70 nm at 40 V and 100 nm at 45 V. The SEM cross sectional view also illustrates the well-ordered nano channel and the elemental mapping elaborates the presence of aluminum and oxygen. The thickness of the AAO nanoporous structure was determined by using SEM for three anodization time spans (20, 24 and 28 hours), in which an increas...
Herein, we demonstrate a facile approach in the fabrication of one-dimensional ZnO nanowires (NWs... more Herein, we demonstrate a facile approach in the fabrication of one-dimensional ZnO nanowires (NWs) from the vacuum die-casting method in assistance with anodic aluminum oxide (AAO) template. The casting method enables molten Zn to embed uniformly over the AAO nanomould under high pressure and temperature of 500 °C. Besides, the significant influence of the oxidation time and temperature stimulates the ZnO NWs growth inside the AAO nanochannels. The oxidation in the nanochannels was profoundly controlled by the inward diffusion of oxygen atoms and the ZnO grows perpendicular towards the surface which obeys the parabolic law. The TEM and XRD results revealed the ZnO wurtzite crystalline structure with preferential orientation along the c-axis. The relationship between ZnO geometry and function of oxidation parameters is demonstrated by microscopic and spectroscopic analysis. The obtained NWs from the chemical etching process resulted in high crystalline, homogeneous, and high-aspect r...
Uploads
Papers by kashif azher