Scribd
Importer
26 vues1 page

Table

Transféré par

Muhammad Bilal
Copyright
© © All Rights Reserved
Nous prenons très au sérieux les droits relatifs au contenu. Si vous pensez qu’il s’agit de votre contenu, signalez une atteinte au droit d’auteur ici.
Formats disponibles
Téléchargez aux formats DOCX, PDF, TXT ou lisez en ligne sur Scribd
26 vues1 page

Table

Transféré par

Muhammad Bilal
Copyright
© © All Rights Reserved
Nous prenons très au sérieux les droits relatifs au contenu. Si vous pensez qu’il s’agit de votre contenu, signalez une atteinte au droit d’auteur ici.
Formats disponibles
Téléchargez aux formats DOCX, PDF, TXT ou lisez en ligne sur Scribd

Compound M.P.

(oC) Yield (%) FT-IR (cm-1)vmax / 1HNMR , C13NMR (500 MHz, CDCl3)/ MS (EI) (m/z)
1750 (C=O), 1323(C-N), / 3.91( 2H, OCCH2), 6.76 (1H, quinoline, Ar-H), 7.18 (3H, Ar-
5a 576.75 85 H), 7.29-7.37, ( 3H, Ar-H), 7.47 (1H, Pyridine), 7.82 (1H, quinolone), 8.74 (1H,pyridine)
8.89 (1H, pyridine)/ 35.5, 87.5,120, 124, 128.9, 134, 135, 154, 156.1,171
1650 (C=O), 3400 (N-H)/ 0.89 (6H, (CH3)2, 1.30 (4H, (CH2)2, 2.13 (2H, CH2), 3.73(2H,
5b 273.23 80 H-Ar), 5.92(1H, H-Ar), 6.82(1H, H-Ar), 6.92 (1H, N-H), 7.02 (1H, H-Ar)/ 0.89, 19.9,
34.8, 43.7, 124.01, 125.5, 135.2, 142.9, 154.9, 156.1, 76.9
1725 (C=O), 1250 (C-O), 808 (C-N),/ 1.64 (3H CH3), 3.71 (1H H-Ar), 3.81 ( 3H CH3),
5c 465.24 65 7.06 (1H H-Ar), 7.23 (1H H-Ar), 7.34 ( 1H H-Ar), 7.48-7.49 (2H, H-Ar), 7.73-7.82 (3H,
quinoline), 8.74 (1H, H-Ar), 8.89 (1H, N-H)/ 13.7, 40.4, 55.8, 87.5, 105.4, 124, 126.7,
128.5, 132.5, 133.5, 134.9, 135.2, 154.9, 156.1, 170.0
5d 363.82 80 1650 (C=O), 808 (C-N),/ 7.43-7.45 (2H H-Ar), 7.65-7.73 (3H, H-Ar), 8.12 (1H, H-Ar),
8.83 (1H, H-Ar), 8.97 (1H, N-H)/ 78.2, 124.1, 126.7, 130, 131.7, 131.8, 133.9, 134, 135.4,
140.5,154.8, 161, 165.2

5e 412.57 78 1675 (C=O), 808 (C-N),/ 4.14 (2H, COCH2), 7.47 (1H, H-Ar), 7.61-7.79 (5H, H-Ar),
8.85(1H, H-Ar), 8.96 (1H, N-H)/ 78.2 121.4, 124.1, 125.7, 126.7, 127.6, 130, 131.8, 133,
134, 135.4, 140.5,154.8, 161, 165.2

1735 (C=O), 1250 (C-O), 808 (C-N), 700 ( C-Cl)/ 2.30 (S, 3H, H-CH3), 2.48 (S, 3H, Me),
5f 368.96 75 7.22 – 7.27 ( D, 2H ,H-Ar), 7.65-7.69 ( D, 2H, H-quinoline), 8.08 ( D, 1H, H-Ar), 8.83 (D,
1H, H-Ar), 8.97 ( D, 1H, C-N, quinoline)/ 21.6, 21.7 78.2, 124.1, 125.7, 128.7, 130.8,
134.0, 134,135.4, 139.8, 140.5, 143, 154, 161, 165.2
1740 (C=O), 1250 (C-O), 808 (C-N), 1100( C-Fl)/ 1.07 ( m, 1H, N-H), 1.33 ( m, 4H,
5g 778.9 70 (CH2)2), 2.78 (t, 4H, (CH2 )2), 3.46 (t, 2H, CH2), 4.12 (q, 1H, cyclopropane ), 6.01 (d, 1H,
H-Ar), 7.65-7.69 (q, 2H, H-Ar), 8.01 (d, 1H, H-Ar), 8.09 (s, 1H, H-Ar), 8.83 (d, 1H, H-
Ar), 8.97 (d, 1H, C-N)/ 7.7, 35.8, 45.8, 51.3, 78.2, 102.5, 109.3, 112.2, 124.1, 125.7,
130.5, 134, 135.4, 136.8, 140.5, 146.9, 152.5, 154.8, 161,162, 176.4
1735 (C=O), 1250 (C-O), 808 (C-N)/ 7.22 ( d, 1H, H-Ar), 7.57-7.60 (m, 2H, H-Ar),
5h 367 85 7.65-7.69 ( m, 2H, quinoline), 8.25 (d, 1H, H-Ar), 8.83 ( d, 1H, H-Ar), 8. 97 (d, 1H, H-
Ar)/ 55.8, 78.2, 114.2, 120.9, 124.1, 125.7,130, 131.3, 134,134.9, 140.5, 154.8, 158.5,
161, 169.1
1735, 1750 (C=O), 1250 (C-O), 808 (C-N)/ 1.9 ( d, 3H, Me), 2.21 (s, 3H, Me), 2.35 ( t,
5i 520.9 80 4H H-Ar), 3.23 ( t, 2H, CH2), 3.44 (s, 4H, H-Ar), 3.99-4.24 ( t, 2H, H2C-O), 7.69 (d, 1H,
H-Ar) 8.66 (s, 1H,H-Ar), 14.93 ( t, 1H, OH)/ 17.9, 46.6, 57.2, 59.4, 65.9, 71.1, 103.8,
109.3, 123.4, 126, 132.6, 143.1, 146.9, 158.2, 166.2, 170.4
1635 (C=O), 1250 (C-O)2, 808 (C-N)/ 3. 84- 3.90 ( s, 6H, (OCH3)2), 5.70 ( s, 2H, CH2),
5j 454.5 70 6.72-6.75 (d, 2H, H-Ar), 7.60, 7.62, 7.65 ( m, 3H, H-Ar), 8.70 ( d, 1H, H-Ar), 8.85 ( d,
1H, HC-N)/ 55.8, 73.1, 74.1, 96.8, 106.5, 112.5, 123.9, 129.5, 130.8, 133.7, 135.3, 141.7,
153.6, 162.2, 164,168, 198.3
1650 (C=O), 1250 (C-O), 808 (C-N)/ 3.32 (s, 3H, CH3), 7.65, 7.69 ( t, 2H, H-Ar), 8.83
5k 450 75 (d, 1H, quinoline) 8.97 ( d, 1H, H-Ar) 9.24 ( s, 1H, imidazole) 13.0 (d, 1H, N-H,
imidazole)/ 30.7,78.2, 124.7, 129, 130, 134, 135.4, 140.5,149, 150.8,154.8, 161, 162.8
1700 (C=O), 1200 (C-O), 808 (C-N)/1.18 ( t, 1H, 3H, CH3), 2.71 ( q, 2H, CH2), 5.70 ( s,
5l 397.5 80 2H, OCH2), 7.33 ( q, 1H, H-Ar), 7.60- 7.62 ( t, 3H, H-Ar), 7.80 ( d, 2H, H-Ar), 7.96 ( q,
1H, H-Ar), 8.70 ( d, 1H, H-Ar), 8.85 ( d, 1H, H-Ar)/ 74.1, 27.3, 73.1, 74.1, 123.9,
124.5,127.5, 127.6,129.4, 133, 133.7, 135.5, 135.7,141.7, 143.5, 153.6, 164.8, 198.3

Vous aimerez peut-être aussi