NSEC/Laboratory Manual/B.
Tech/1st Year/Chemistry
Experiment no: Date of Experiment:
Name:
Section: Stream: Roll No: Date of Submission:
Record of marks:
Division Attendence Data Graph Calculation Submission Total
recording in time
Full marks 1 2 - 1 1 5
Marks
obtained
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ACID BASE TITRATION
(Determination of strength of unknown HCl solution by NaOH solution)
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Theory:
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An acid–base titration is the determination of the concentration of an acid or base by
exactly neutralizing the acid or base with an acid or base of known concentration. This
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allows for quantitative analysis of the concentration of an unknown acid or base solution. It
makes use of the neutralization reaction that occurs between acids and bases.
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Apparatus:
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1. Burette
2. Pipette
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3. Indicator(Phenlopthalein, colourless in acid medium(PH<7) , pink in basic medium
(PH>7)
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4. Conical Flask
5. Beaker
6. Titrant or titrator (a standard solution of known concentration of sodium
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Hydroxide)
7. Analyte or titrand (solution of unknown concentration of HCl)
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Method:
Burette is filled up with given NaOH solution .10 ml of HCl solution is pipetted
out in each conical flask. One drop of phenolphthalein indicator is added in the
solution of conical flask. The solution of the conical remain colourless. It is titrated
with the NaOH solution. At the end point the colour will be light pink.
Reaction:
HCl (aq) + NaOH(aq)=NaCl + H2O
Table -1
Table for Temperature
Initial Temperature(0 C) Final Temperature(0 C) Mean Temperature(0 C)
Table -2
Table for Acid Base Titration
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No of Vol of HCl Burette Reading
Observation. solnTaken. (Vol of NaOH)
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(ml)
Initial Final Vol required Mean (ml)
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(ml)
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2.
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Calculation:
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Volume of HCl Taken= V1 ml= 10 ml
Strength of HCl = S1 (N) = ………………… (N)
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Volume of NaOH required =V2 ml=…………ml
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Strength of NaOH= S2 (N) = ………….............. (Given)
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We know,
V1 × S1 = V2 × S2
S1= V2 × S2/V1
Result:
The strength of unknown HCl solution is…………… (N) at ….........0C
